Startseite Solid-state synthesis and magnetic properties of rhombohedral phase Mg2SiNi3
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Solid-state synthesis and magnetic properties of rhombohedral phase Mg2SiNi3

  • Liangbiao Wang , Dejian Zhao , Juanjuan Lu , Weiqiao Liu und Quanfa Zhou
Veröffentlicht/Copyright: 29. Januar 2018
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Abstract

A solid-state route was developed to prepare rhombohedral phase Mg2SiNi3 with the dimensions of about 300 nm by using metallic magnesium, nickel oxide and silicon as starting materials at 700 °C in an autoclave reactor. The obtained product was investigated by means of X-ray diffraction, scanning electron microscopy and transmission electron microscopy. Magnetic measurement at room temperature indicated that the values of saturation magenetization and coercivity of the obtained Mg2SiNi3 were 0.31 emu g–1 and 65.20 Oe, respectively.


*Correspondence address, Dr. Liangbiao Wang and Prof. Qianfa Zhou, School of Chemistry and Environment Engineering, Jiangsu University of Technology, No. 1801 Zhongwu Road, Changzhou 213001, P.R. China, Tel.: +86-519-86953005, Fax: +86-519-86953005, E-mail:

References

[1] R.A.Varin, T.Czujko, J.Mizera: J. Alloys Compd.350 (2003) 332. 10.1016/S0925-8388(02)00984-2Suche in Google Scholar

[2] M.Shimada, E.Higuchi, H.Inoue: J. Alloys Compd.580 (2013) 153. 10.1016/j.jallcom.2013.01.191Suche in Google Scholar

[3] J.de Boor, C.Gloanec, H.Kolb, R.Sottong, P.Ziolkowski, E.Müller: J. Alloys Compd.632 (2015) 348. 10.1016/j.jallcom.2015.01.149Suche in Google Scholar

[4] H.L.Liu, T.T.Yu, D.Q.Su, Z.H.Tang, J.H.Zhang, Y.J.Liu, A.H.Yuan, Q.H.Kong: Ceram. Int.43 (2017) 14395. 10.1016/j.ceramint.2017.07.207Suche in Google Scholar

[5] X.Chen, J.C.Guan, G.Y.Sha, Z.M.Gao, C.T.Williams, C.H.Liang: RSC Adv.4 (2014) 653. 10.1039/C3RA43460ESuche in Google Scholar

[6] J.Y.Lin, H.M.Hsu, K.C.Lu: Cryst. Eng. Comm.17 (2015) 1911. 10.1039/C4CE02513JSuche in Google Scholar

[7] S.Y.Chen, P.H.Yeh, W.W.Wu, U.S.Chen, Y.L.Chueh, Y.C.Yang, S.Gwo, L.J.Chen: ACS Nano5 (2011) 9202. PMid:22010967; 10.1021/nn203445pSuche in Google Scholar PubMed

[8] Y.P.Liu, J.D.Livington, S.M.Allen: Metall. Mater. Trans.A 26 (1995) 1441. 10.1007/BF02647594Suche in Google Scholar

[9] S.T.Sabitu, G.Gallo, A.J.Goudy: J. Alloys Compd.499 (2010) 35. 10.1016/j.jallcom.2010.03.128Suche in Google Scholar

[10] Y.K.Song, R.A.Varin: Intermetallics6 (1998) 43. 10.1016/S0966-9795(97)00054-XSuche in Google Scholar

[11] D.Cracco, A.Percheron-Guegan: J. Alloys Compd.268 (1998) 248. 10.1016/S0925-8388(97)00552-5Suche in Google Scholar

[12] D.Noréus, L.Eriksson, L.Göthe, P.E.Werner: J. Less-Common Metals.107 (1985) 345. 10.1016/0022-5088(85)90093-1Suche in Google Scholar

[13] D.K.Yang, C.Wen, F.S.Han, Y.J.Yang: J. Non-Cryst. Solids352 (2006) 3244. 10.1016/j.jnoncrysol.2006.05.027Suche in Google Scholar

[14] K.Ozaki, T.Nishio, A.Matsumoto, K.Kobayashi: Mater. Sci. Eng.A 375–377 (2004) 857860. 10.1016/j.msea.2003.10.150Suche in Google Scholar

[15] J.H.Zhang, B.Yan, H.Wu, Q.H.Kong: RSC Adv.4 (2014) 6991. 10.1039/C3RA46764CSuche in Google Scholar

Received: 2017-07-08
Accepted: 2017-09-18
Published Online: 2018-01-29
Published in Print: 2018-02-12

© 2018, Carl Hanser Verlag, München

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