Solid-state synthesis and magnetic properties of rhombohedral phase Mg2SiNi3

Liangbiao Wang; Dejian Zhao; Juanjuan Lu; Weiqiao Liu; Quanfa Zhou

doi:10.3139/146.111588

Artikel

Solid-state synthesis and magnetic properties of rhombohedral phase Mg₂SiNi₃

Liangbiao Wang , Dejian Zhao , Juanjuan Lu , Weiqiao Liu und Quanfa Zhou

Veröffentlicht/Copyright: 29. Januar 2018

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Aus der Zeitschrift International Journal of Materials Research Band 109 Heft 2

Abstract

A solid-state route was developed to prepare rhombohedral phase Mg₂SiNi₃ with the dimensions of about 300 nm by using metallic magnesium, nickel oxide and silicon as starting materials at 700 °C in an autoclave reactor. The obtained product was investigated by means of X-ray diffraction, scanning electron microscopy and transmission electron microscopy. Magnetic measurement at room temperature indicated that the values of saturation magenetization and coercivity of the obtained Mg₂SiNi₃ were 0.31 emu g^–1 and 65.20 Oe, respectively.

Keywords: Solid-state route; Silicide; Mg2SiNi3; Magnetic properties

*Correspondence address, Dr. Liangbiao Wang and Prof. Qianfa Zhou, School of Chemistry and Environment Engineering, Jiangsu University of Technology, No. 1801 Zhongwu Road, Changzhou 213001, P.R. China, Tel.: +86-519-86953005, Fax: +86-519-86953005, E-mail: lbwang@jsut.edu.cnlabzqf@jsut.edu.cn

References

[1] R.A.Varin, T.Czujko, J.Mizera: J. Alloys Compd.350 (2003) 332. 10.1016/S0925-8388(02)00984-2Suche in Google Scholar

[2] M.Shimada, E.Higuchi, H.Inoue: J. Alloys Compd.580 (2013) 153. 10.1016/j.jallcom.2013.01.191Suche in Google Scholar

[3] J.de Boor, C.Gloanec, H.Kolb, R.Sottong, P.Ziolkowski, E.Müller: J. Alloys Compd.632 (2015) 348. 10.1016/j.jallcom.2015.01.149Suche in Google Scholar

[4] H.L.Liu, T.T.Yu, D.Q.Su, Z.H.Tang, J.H.Zhang, Y.J.Liu, A.H.Yuan, Q.H.Kong: Ceram. Int.43 (2017) 14395. 10.1016/j.ceramint.2017.07.207Suche in Google Scholar

[5] X.Chen, J.C.Guan, G.Y.Sha, Z.M.Gao, C.T.Williams, C.H.Liang: RSC Adv.4 (2014) 653. 10.1039/C3RA43460ESuche in Google Scholar

[6] J.Y.Lin, H.M.Hsu, K.C.Lu: Cryst. Eng. Comm.17 (2015) 1911. 10.1039/C4CE02513JSuche in Google Scholar

[7] S.Y.Chen, P.H.Yeh, W.W.Wu, U.S.Chen, Y.L.Chueh, Y.C.Yang, S.Gwo, L.J.Chen: ACS Nano5 (2011) 9202. PMid:22010967; 10.1021/nn203445pSuche in Google Scholar PubMed

[8] Y.P.Liu, J.D.Livington, S.M.Allen: Metall. Mater. Trans.A 26 (1995) 1441. 10.1007/BF02647594Suche in Google Scholar

[9] S.T.Sabitu, G.Gallo, A.J.Goudy: J. Alloys Compd.499 (2010) 35. 10.1016/j.jallcom.2010.03.128Suche in Google Scholar

[10] Y.K.Song, R.A.Varin: Intermetallics6 (1998) 43. 10.1016/S0966-9795(97)00054-XSuche in Google Scholar

[11] D.Cracco, A.Percheron-Guegan: J. Alloys Compd.268 (1998) 248. 10.1016/S0925-8388(97)00552-5Suche in Google Scholar

[12] D.Noréus, L.Eriksson, L.Göthe, P.E.Werner: J. Less-Common Metals.107 (1985) 345. 10.1016/0022-5088(85)90093-1Suche in Google Scholar

[13] D.K.Yang, C.Wen, F.S.Han, Y.J.Yang: J. Non-Cryst. Solids352 (2006) 3244. 10.1016/j.jnoncrysol.2006.05.027Suche in Google Scholar

[14] K.Ozaki, T.Nishio, A.Matsumoto, K.Kobayashi: Mater. Sci. Eng.A 375–377 (2004) 857–860. 10.1016/j.msea.2003.10.150Suche in Google Scholar

[15] J.H.Zhang, B.Yan, H.Wu, Q.H.Kong: RSC Adv.4 (2014) 6991. 10.1039/C3RA46764CSuche in Google Scholar

Received: 2017-07-08

Accepted: 2017-09-18

Published Online: 2018-01-29

Published in Print: 2018-02-12

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https://doi.org/10.3139/146.111588

Schlagwörter für diesen Artikel

Solid-state route; Silicide; Mg2SiNi3; Magnetic properties