Effect of Conditions of Cryogenic Treatment on the Properties of Selected Cold Work Tool Steels*
-
J. Sobotová
, M. Kuřík , Z. Kolář and P. Priknerová
Abstract
The paper evaluates the properties of two cold work tool steels which differ in the production process and content of carbon and vanadium. Both steels are characterized by their great hardenability, toughness, dimensional stability and wear resistance. They are a subledeburitic steel X63CrMoV5-1 produced by classical metallurgy and a ledeburitic steel Vanadis 6 produced by powder metallurgy. Different austenitizing temperatures in the range of recommended values for the material were used during the heat treatment. Both materials were tempered at a temperature of 530 °C. Also cryogenic treatment at temperatures of −196 °C and −180 ° C for 5 h and/or 4 h was inserted into the conventional heat treatment cycle. The effect of the timing of cryogenic treatment in the heat treatment cycle was observed. Hardness measurement, a three-point bending test and a wear resistance test by the pin-on-disk method were used to specify the effect of the conditions of heat treatment on the properties of the investigated materials.
Kurzfassung
Der Beitrag untersucht die Eigenschaften zweier Kaltarbeitsstähle, die sich durch den Herstellprozess und die Gehalte von Kohlenstoff und Vanadium unterscheiden. Beide Stähle zeichnen sich durch ihre große Härte, Zähigkeit, Formbeständigkeit und Verschleißfestigkeit aus. Es sind der subledeburitische Stahl X63CrMoV5-1, hergestellt durch klassische Metallurgie, und der ledeburitische Stahl Vanadis 6, hergestellt durch Pulvermetallurgie. Es wurden verschiedene Austenitisiertemperaturen entsprechend der empfohlenen Werte des Materials während der Wärmebehandlung angewendet. Beide Werkstoffe wurden bei 530 °C vergütet. Es wurde ebenfalls eine Tiefkühlbehandlung bei Temperaturen von −196 °C und −180 ° C für 5 h und/oder 4 h zum konventionellen Wärmebehandlungskreislauf hinzugefügt. Dabei wurde beobachtet, welchen Effekt der Zeitpunkt der Tieftemperaturbehandlung während des Wärmebehandlungszyklus hat. Mit einer Härtemessung, einem Dreipunkt-Biegeversuch und einem Verschleißtest, der Pin-on-Disk-Methode, wurde die Auswirkung der Wärmebehandlungsbedingungen auf die Eigenschaften des untersuchten Materials beschrieben.
References
1. Gill, S. S.; Singh, J.; Singh, R.; Singh, H.: Metallurgical Principles of Cryogenically Treated Tool Steels – a review on the current state of science. Int J. Adv. Manufact. Techn.54 (2011) 1–4, pp. 59–82, 10.1007/s00170-010-2935-5Search in Google Scholar
2. Baldissera, P.; Delprete, C.: Deep Cryogenic Treatment: A Bibliographic Review. The Open Mechanical Engineering Journal2 (2008), pp. 1–11, 10.2174/1874155X00802010001Search in Google Scholar
3. Yan, X. G.; Li, D. Y.: Effects of the Sub-zero Treatment Condition on Microstructure, Mechanical Behavior and Wear Resistance of W9Mo3Cr4 V High Speed Steel. Wear302 (2013) 1–2, pp. 854–862, 10.1016/j.wear.2012.12.037Search in Google Scholar
4. Kalsi, N. S.; Sehgal, R.; Sharma, V. S.: Cryogenic Treatment of Tool Materials: A Review. Mat. Manuf. Process.25 (2010) 10, pp. 1077–1100, 10.1080/10426911003720862Search in Google Scholar
5. Oppenkowski, A.; Weber, S.; Theisen, W.: Evaluation of Factors Influencing Deep Cryogenic Treatment that Affect the Properties of Tool Steels. J. Mat. Process. Technol.210 (2010) 14, pp. 1949–1955, 10.1016/j.jmatprotec.2010.07.007Search in Google Scholar
6. Molinari, A.; Pellizzari, M.; Gialanella, S.; Straffelini, G.; Stiasny, K. H.: Effect of Deep Cryogenic Treatment on the Mechanical Properties of Tool Steels. J. Mat. Process. Technol.118 (2001) 1–3, pp. 350–355, 10.1016/s0924-0136(01)00973-6Search in Google Scholar
7. Da Silva, F. J.; Franco, S. D.; Machado, Á. R.; Ezugwu, E. O.: Performance of Cryogenically Treated HSS Tools. Wear261 (2006) 5–6, pp. 674–685. 10.1016/j.wear.2006.01.017Search in Google Scholar
8. Sobotová, J.; Jurči, P.; Dlouhy, I.: The Effect of Subzero Treatment on Microstructure, Fracture Toughness and Wear Resistance of Vanadis 6 Tool Steel. Mat. Sci. Eng. A652 (2016), pp. 192–204, 10.1016/j.msea.2015.11.078Search in Google Scholar
9. Das, D.; Dutta, A. K.; Ray, K. K.: Sub-zero Treatments of AISI D2 Steel: Part I. Microstructure and Hardness. Mat. Sci. Eng. A527 (2010) 9, pp. 2182–2193, 10.1016/j.msea.2009.10.070Search in Google Scholar
10. Kamran, A.; Akhbarizadeh, A.; Javadpour, S.: Investigating the effect of holding duration on the microstructure of 1.2080 tool steel during the deep cryogenic heat treatment. Vacuum86 (2012) 10, pp. 1534–1540, 10.1016/j.vacuum.2012.02.013Search in Google Scholar
11. Jurči, P.; Janka, L.: Wear Resistance of Sub-zero Treatment Processed Cr-V Ledeburitic Steel Vanadis 6. Proc. 21st Int. Conf. on Metallurgy and Materials, Metal 2012, Brno: Tanger Ltd., 2012, pp. 634–639, ISBN 978-80-87294-31-4Search in Google Scholar
12. Jurči, P.; Dománková, M.; Sobotová, J.: Microstructure and Hardness of Sub-zero Treated and untempered P/M Vanadis 6 Lledeburitic Tool Steel. Vacuum111 (2015), pp. 92–101, 10.1016/j.vacuum.2014.10.004Search in Google Scholar
13. Sobotová, J.; Jurči, P.; Adámek, J.; Salabová, P.; Prikner, O.; Šuštaršič, B.; Jenko, D.: Diagnostics of the Microstructural Changes in Sub-zero Processed Vanadis 6 P/M Ledeburitic Tool Steel. Materiali in Tehonologije/Materials and Technology47 (2013) 1, pp. 93–98Search in Google Scholar
14. Sobotová, J.; Jurči, P.; Cejp, J.: Structure and Properties of Sub-zero Processed Vanadis 6. Proc. 20th Ann. Int. Conf. On Metallurgy and Materials, Metal 2011, Ostrava, Tanger Ltd., 2011, pp. 672–677, ISBN 978-80-87294-22-2Search in Google Scholar
15. Standard ASTM G99: Test Method for Wear Testing with a Pin-on-Disc Apparatus: G99-05. Reapproved, ASTM Int., USA, 2010Search in Google Scholar
© 2017, Carl Hanser Verlag, München
Articles in the same Issue
- Veranstaltungen/Events
- Veranstaltungen
- HTM-Praxis
- HTM-Praxis
- Kurzfassungen/Abstracts
- Kurzfassungen
- Inhalt/Contents
- Inhalt
- Fachbeiträge/Technical Contributions
- Development of an Energy-Efficient Burner for Heat Treatment Furnaces with a Reducing Gas Atmosphere*
- Einfluss der Temperatur und des Vergütungszustands auf die Wärmeleitfähigkeit von Warmarbeitsstählen für das Presshärten*
- Einfluss der Wärmebehandlung auf die Korrosionsbeständigkeit von Schneidwaren*
- Effect of Conditions of Cryogenic Treatment on the Properties of Selected Cold Work Tool Steels*
- Investigation of the Tribological Behaviour of HS6-5-3 type Tool Steels during High-Temperature Sliding Wear*
- Energy Resolved Residual Stress Analysis with Laboratory X-Ray Sources
Articles in the same Issue
- Veranstaltungen/Events
- Veranstaltungen
- HTM-Praxis
- HTM-Praxis
- Kurzfassungen/Abstracts
- Kurzfassungen
- Inhalt/Contents
- Inhalt
- Fachbeiträge/Technical Contributions
- Development of an Energy-Efficient Burner for Heat Treatment Furnaces with a Reducing Gas Atmosphere*
- Einfluss der Temperatur und des Vergütungszustands auf die Wärmeleitfähigkeit von Warmarbeitsstählen für das Presshärten*
- Einfluss der Wärmebehandlung auf die Korrosionsbeständigkeit von Schneidwaren*
- Effect of Conditions of Cryogenic Treatment on the Properties of Selected Cold Work Tool Steels*
- Investigation of the Tribological Behaviour of HS6-5-3 type Tool Steels during High-Temperature Sliding Wear*
- Energy Resolved Residual Stress Analysis with Laboratory X-Ray Sources