Startseite Transport phenomena in an agitated vessel with an eccentrically located impeller
Artikel
Lizenziert
Nicht lizenziert Erfordert eine Authentifizierung

Transport phenomena in an agitated vessel with an eccentrically located impeller

  • Magdalena Cudak EMAIL logo , Joanna Karcz und Anna Kiełbus-Rąpała
Veröffentlicht/Copyright: 26. Januar 2011
Veröffentlichen auch Sie bei De Gruyter Brill

Abstract

The paper presents results of an experimental analysis of the transport phenomena at the vicinity of the wall of an unbaffled agitated vessel with an eccentrically located impeller. Distributions of the transport coefficients were experimentally studied using an electrochemical method within the turbulent regime of the Newtonian liquid flow. Measurements were carried out in an agitated vessel with the inner diameter T = 0.3 m. Liquid height in the vessel was equal to the inner diameter, H = T. The agitated vessel was equipped with a Rushton or a Smith turbine or an A 315 impeller. Eccentricity of the impeller shaft was varied from 0 to 0.53. Local values of the dimensionless shear rate, shear stress, dynamic velocity and friction coefficient were integrated numerically for the whole surface area of the cylindrical wall of the vessel. Averaged values of these quantities were correlated with the impeller eccentricity and modified Reynolds number. The proposed Eqs. (5)–(8), with the coefficients given in Table 2, have no equivalent in open literature concerning this subject. Distributions of the shear rate, γ/n, and friction coefficient, f, at the vicinity of the cylindrical wall of the unbaffled vessel equipped with eccentric Rushton or Smith turbine or A 315 impeller are very uneven and they depend significantly on the impeller eccentricity, e/R. Maximum local values of these variables are located on the wall section closest to the impeller blades. From among the tested impellers, the greatest effects of the impeller eccentricity, e/R, and the liquid turbulence (described by the modified Reynolds number Re P,M) on the averaged dimensionless shear rate (γ/n)m and friction coefficient, f m, are found for the radial-flow Rushton turbine located eccentrically in an unbaffled agitated vessel.

[1] Cabaret, F., Fradette, L., & Tanguy, P. A. (2008a). Effect of shaft eccentricity on the laminar mixing performance of a radial impeller. The Canadian Journal of Chemical Engineering, 86, 971–977. DOI: 10.1002/cjce.20103. http://dx.doi.org/10.1002/cjce.2010310.1002/cjce.20103Suche in Google Scholar

[2] Cabaret, F., Fradette, L., & Tanguy, P. A. (2008b). Gas-liquid mass transfer in unbaffled dual-impeller mixers. Chemical Engineering Science, 63, 1636–1647. DOI: 10.1016/j.ces.2007.11.028. http://dx.doi.org/10.1016/j.ces.2007.11.02810.1016/j.ces.2007.11.028Suche in Google Scholar

[3] Cabaret, F., Rivera, C., Fradette, L., Heniche, M., & Tanguy, P. A. (2007). Hydrodynamics performance of a dual shaft mixer with viscous Newtonian liquids. Chemical Engineering Research and Design, 85, 583–590. DOI: 10.1205/cherd06175. http://dx.doi.org/10.1205/cherd0617510.1205/cherd06175Suche in Google Scholar

[4] Cudak, M. (2004). Heat and momentum transfer in a stirred tank with an eccentrically located impeller. PhD Thesis, Szczecin University of Technology, Poland. Suche in Google Scholar

[5] Cudak, M., & Karcz, J. (2009). The effects of eccentricity and diameter of HE 3 impeller on the momentum transfer process in an agitated vessel. In 13th European Conference on Mixing, 14–17 April 2009. London, UK. Suche in Google Scholar

[6] Cudak, M., & Karcz, J. (2008a). Distribution of local heat transfer coefficient values in the wall region of an agitated vessel. Chemical Papers, 62, 92–99. DOI: 10.2478/s11696-007-0084-6. http://dx.doi.org/10.2478/s11696-007-0084-610.2478/s11696-007-0084-6Suche in Google Scholar

[7] Cudak, M., & Karcz, J. (2008b). Momentum transfer in an agitated vessel equipped with an eccentrically located HE 3 impeller. Chemical and Process Engineering, 29, 1071–1082. Suche in Google Scholar

[8] Cudak, M., & Karcz, J. (2006). Momentum transfer in an agitated vessel with off-centred impellers. Chemical Papers, 60, 375–380. DOI: 10.2478/s11696-006-0068-y. http://dx.doi.org/10.2478/s11696-006-0068-y10.2478/s11696-006-0068-ySuche in Google Scholar

[9] Dyląg, M., & Brauer, H. (1976). Leistungsbedarf bei exzentrischer Anordnung des Ruehrers. Verfahrenstechnik, 10(10), 637–640. Suche in Google Scholar

[10] Galletti, C., & Brunazzi, E. (2008). On the main flow features and instabilities in an unbaffled vessel agitated with an eccentrically located impeller. Chemical Engineering Science, 63, 4494–4505. DOI: 10.1016/j.ces.2008.06.007. http://dx.doi.org/10.1016/j.ces.2008.06.00710.1016/j.ces.2008.06.007Suche in Google Scholar

[11] Galletti, C., Pintus, S., & Brunazzi, E. (2009a). Effect of shaft eccentricity and impeller blade thickness on the vortices features in an unbaffled vessel. Chemical Engineering Research and Design, 87, 391–400. DOI: 10.1016/j.cherd.2008.11.013. http://dx.doi.org/10.1016/j.cherd.2008.11.01310.1016/j.cherd.2008.11.013Suche in Google Scholar

[12] Galletti, C., Pintus, S., & Brunazzi, E. (2009b). Macroinstabilities in eccentrically agitated vessels. Chemical Engineering Transactions, 17, 483–488. DOI: 10.3303/CET0917081. Suche in Google Scholar

[13] Hall, J. F., Barigou, M., Simmons, M. J. H., & Stitt, E. H. (2005a). Comparative study of different mixing strategies in small high throughput experimentation reactors. Chemical Engineering Science, 60, 2355–2368. DOI: 10.1016/j.ces.2004.10.045. http://dx.doi.org/10.1016/j.ces.2004.10.04510.1016/j.ces.2004.10.045Suche in Google Scholar

[14] Hall, J. F., Barigou, M., Simmons, M. J. H., & Stitt, E. H. (2005b). A PIV study of hydrodynamics in gas-liquid high throughput experimentation (THE) reactors with eccentric impeller configurations. Chemical Engineering Science, 60, 6403–6413. DOI: 10.1016/j.ces.2005.03.044. http://dx.doi.org/10.1016/j.ces.2005.03.04410.1016/j.ces.2005.03.044Suche in Google Scholar

[15] Karcz, J. (1996). Momentum transfer in a region of an agitated vessel wall. Inżynieria Chemiczna i Procesowa, 17, 403–421. Suche in Google Scholar

[16] Karcz, J., & Abragimowicz, A. (2000). Local heat transfer in a liquid and gas — liquid system agitated by concave disc turbine. In H. E. A. van Akker, & J. J. Derksen (Eds.), 10th European Conference on Mixing, 2–5 July 2000 (pp. 493–500). Amsterdam, The Netherlands: Elsevier. DOI: 10.1016/B978-044450476-0/50062-5. 10.1016/B978-044450476-0/50062-5Suche in Google Scholar

[17] Karcz, J., & Cudak, M. (2006). An effect of the type of an eccentrically located impeller on the efficiency of heat transfer process. In 12th European Conference on Mixing, 27–30 June 2006. Bologna, Italy. Suche in Google Scholar

[18] Karcz, J., & Cudak, M. (2004). Experimental analysis of the transport phenomena in a stirred tank with an eccentrically located impeller. Inżynieria Chemiczna i Procesowa, 25, 1067–1073. Suche in Google Scholar

[19] Karcz, J., & Cudak, M. (2002). Efficiency of the heat transfer process in a jacketed agitated vessel equipped with an eccentrically located impeller. Chemical Papers, 56, 382–386. Suche in Google Scholar

[20] Karcz, J., Cudak, M., & Szoplik, J. (2005). Stirring of a liquid in a stirred tank with an eccentrically located impeller. Chemical Engineering Science, 60, 2369–2380. DOI: 10.1016/j.ces.2004.11.018. http://dx.doi.org/10.1016/j.ces.2004.11.01810.1016/j.ces.2004.11.018Suche in Google Scholar

[21] Karcz, J., & Szoplik, J. (2004). An effect of the eccentric position of the propeller agitator on the mixing time. Chemical Papers, 58, 9–14. Suche in Google Scholar

[22] Karcz, J., & Szoplik, J. (2001). Studies of mixing time in an agitated vessel with eccentric impeller. Inżynieria Chemiczna i Procesowa, 22, 651–656. (in Polish) Suche in Google Scholar

[23] King, R., & Muskett, J. (1985). Fluid loading and power measurements on an eccentrically mounted pitched blade impeller. In 5th European Conference on Mixing, 10–12 June 1985 (Paper 29, pp. 285–301). Wuerzburg, Germany. Suche in Google Scholar

[24] Medek, J., & Fort, I. (1985). Mixing in vessel with eccentric mixer. In 5th European Conference on Mixing, 10–12 June 1985 (Paper 27, pp. 263–271). Wuerzburg, Germany. Suche in Google Scholar

[25] Montante, G., Bakker, A., Paglianti, A., & Magelli, F. (2006). Effect of the shaft eccentricity on the hydrodynamics of unbaffled stirred tanks. Chemical Engineering Science, 61, 2807–2814. DOI: 10.1016/j.ces.2005.09.021. http://dx.doi.org/10.1016/j.ces.2005.09.02110.1016/j.ces.2005.09.021Suche in Google Scholar

[26] Seichter, P., Pesl, L., Slama, V., & Mazoch, J. (2000). Blending effect of excentric axial agitators. In 14th International Congress of Chemical and Process Engineering CHISA, 27–31 August 2000 (Paper E3.2). Prague, Czech Republic. Suche in Google Scholar

[27] Stręk, F. (1981). Agitation and agitated vessels (2nd ed.). Warszawa, Poland: WNT. Suche in Google Scholar

[28] Stręk, F., & Karcz, J. (1999). Application of an electrochemical method for the studies of a mass transfer process at the vicinity of a wall of an agitated vessel. Inżynieria Chemiczna i Procesowa, 20, 3–22. Suche in Google Scholar

[29] Szoplik, J., & Karcz, J. (2009). The efficiency of the homogenization of non-Newtonian liquid in an agitated vessel with an eccentric propeller. Chemical and Process Engineering, 30, 125–138. Suche in Google Scholar

[30] Szoplik, J., & Karcz, J. (2008). Mixing time of a non-Newtonian liquid in an unbaffled agitated vessel with an eccentric propeller. Chemical Papers, 62, 70–77. DOI: 10.2478/s11696-007-0081-9. http://dx.doi.org/10.2478/s11696-007-0081-910.2478/s11696-007-0081-9Suche in Google Scholar

[31] Szoplik, J., & Karcz, J. (2005). An efficiency of the liquid homogenization in agitated vessels equipped with off-centred impeller. Chemical Papers, 59, 373–379. Suche in Google Scholar

[32] Wichterle, K., Kadlec, M., Žák, L., & Mitschka, P. (1984). Shear rates on turbine impeller blades. Chemical Engineering Communications, 26, 25–32. DOI: 10.1080/00986448408940200. http://dx.doi.org/10.1080/0098644840894020010.1080/00986448408940200Suche in Google Scholar

[33] Wichterle, K., Mitschka, P., Hajek, J., & Žák, L. (1988). Shear stresses on the walls of vessels with axial impellers. Chemical Engineering Research and Design, 66, 102–106. Suche in Google Scholar

[34] Wichterle, K., Žák, L., & Mitschka, P. (1985). Shear stresses on the walls of agitated vessel. Chemical Engineering Communications, 32, 289–305. DOI: 10.1080/00986448508911652 http://dx.doi.org/10.1080/0098644850891165210.1080/00986448508911652Suche in Google Scholar

[35] Žák, L. (1986). Electrochemická diagnostika prenosových jevů na steně míchaných nádob (Electrochemical diagnostics of the transport phenomena on the agitated vessel wall). PhD Thesis, Czechoslovak Academy of Sciences, Prague, Czech Republic. Suche in Google Scholar

Published Online: 2011-1-26
Published in Print: 2011-4-1

© 2010 Institute of Chemistry, Slovak Academy of Sciences

Artikel in diesem Heft

  1. Mechanisms controlling lipid accumulation and polyunsaturated fatty acid synthesis in oleaginous fungi
  2. Predicting retention indices of aliphatic hydrocarbons on stationary phases modified with metallocyclams using quantitative structure-retention relationships
  3. New SPME fibre for analysis of mequinol emitted from DVDs
  4. Continuous production of citric acid from raw glycerol by Yarrowia lipolytica in cell recycle cultivation
  5. Enhancing the production of gamma-linolenic acid in Hansenula polymorpha by fed-batch fermentation using response surface methodology
  6. Process characteristics for a gas—liquid system agitated in a vessel equipped with a turbine impeller and tubular baffles
  7. Kinetic study of pyrolysis of waste water treatment plant sludge
  8. Transport phenomena in an agitated vessel with an eccentrically located impeller
  9. Membrane extraction of 1-phenylethanol from fermentation solution
  10. Theoretical study on transesterification in a combined process consisting of a reactive distillation column and a pervaporation unit
  11. Wall effects on terminal falling velocity of spherical particles moving in a Carreau model fluid
  12. The effect of the physical properties of the liquid phase on the gas-liquid mass transfer coefficient in two- and three-phase agitated systems
  13. Effectiveness of nitric oxide ozonation
  14. Modelling of nanocrystalline iron nitriding process — influence of specific surface area
  15. Effect of CeO2 and Sb2O3 on the phase transformation and optical properties of photostable titanium dioxide
  16. Carnauba wax microparticles produced by melt dispersion technique
  17. Complexation studies of 3-substituted β-diketones with selected d- and f-metal ions
  18. Influence of the solvent donor number on the O/W partition ratio of Cu(II) complexes of 1,2-dialkylimidazoles
  19. Continuous dialysis of sulphuric acid in the presence of zinc sulphate
  20. Differences in affinity of arylstilbazolium derivatives to tetraplex structures
  21. Fast ferritin immunoassay on PDMS microchips
Heruntergeladen am 27.11.2025 von https://www.degruyterbrill.com/document/doi/10.2478/s11696-010-0086-7/pdf?lang=de
Button zum nach oben scrollen