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Investigation of the solid samples evaporation from the auxiliary DC arc discharge in the atomic emission spectroscopy

  • S. Ružičková EMAIL logo , L. Koller und M. Matherny
Veröffentlicht/Copyright: 1. April 2006
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Abstract

Efficiency of the suggested tandem technique of Marinković burner was studied in terms of the influence of the PC-controlled DC arc of the different intensities (10 A, 15 A, 20 A, 25 A) on the evaporation process. Higher intensities than 25 A did not allow to use the given experimental equipment since they cause plasma instability and periodic plasma quenching. The suggested method was evaluated by the determination of the half (t 50%) and total (t 100%) evaporation time and by determination of the signal/background ratio for the chosen elements (Al, Ca, Cr, Fe, Mg, Ni, Si, and V) in the model graphite matrix.

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Published Online: 2006-4-1
Published in Print: 2006-4-1

© 2006 Institute of Chemistry, Slovak Academy of Sciences

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