Abstract
A quantitative relation between the linear attenuation coefficient (LAC) obtained by Synchrotron Radiation X-ray computed tomography (observed LAC) and the theoretically calculated LAC (theoretical LAC) of standard materials (minerals and metals) has been obtained for an X-ray microtomographic system at BL20B2 of SPring-8, Japan. This system, called SP-μCT, uses highly monochromatized and well-collimated X-ray beams produced by a synchrotron radiation source. Three-dimensional images were obtained for samples 0.4.4 mm in size at X-ray energies of 15.35 keV with a voxel size of 5.83 × 5.83 × 5.83 μm3. A histogram of the observed LAC for each sample was well-fitted by a Gaussian curve except for heavy metals whose X-ray transmittance was insufficient. The contrast resolution of CT images is best (within 5% of the LAC value) at LACs of about 10.30 cm-1. A garnet schist was imaged with SP-μCT to verify the observed-theoretical LAC relation for minerals contained in a rock sample. The result was consistent with the relation obtained for the standards. The CT and back-scattered electron images of the rock sample were compared. The present results put restrictions on discrimination of mineral phases and estimation of chemical compositions (e.g., Mg/Fe ratio) of certain minerals forming solid solutions based on CT values. The present quantitative relationship between observed and theoretical LACs enables us to obtain an absolute elemental concentration map by imaging just above and below the X-ray absorption edge energy of the element (subtraction method).
© 2015 by Walter de Gruyter Berlin/Boston
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Articles in the same Issue
- Contact metamorphism of the White Mountain Peak metavolcanic complex, eastern California
- Structure and luminescence characteristics of quartz from pegmatites
- Evidence for monazite-, barite-, and AgMnO4 (distorted barite)-type structures of CaSO4 at high pressure and temperature
- The “template” effect of the extra-framework content on zeolite compression: The case of yugawaralite
- The influence of OH in coesite on the kinetics of the coesite-quartz phase transition
- First-principles study of hydrogen bond symmetrization of phase D under high pressure
- First-principles study of OH-stretching modes in kaolinite, dickite, and nacrite
- A systematic study of OH in hydrous wadsleyite from polarized FTIR spectroscopy and single-crystal X-ray diffraction: Oxygen sites for hydrogen storage in Earthʼs interior
- Determination of the content and distribution of fixed ammonium in illite-smectite using a modified X-ray diffraction technique: Application to oil source rocks of western Greenland
- Determination of defect structures in kaolin minerals by high-resolution transmission electron microscopy (HRTEM)
- Mössbauer spectroscopy of omphacite and garnet pairs from eclogites: Application to geothermobarometry
- Allanite and epidote weathering at the Coweeta Hydrologic Laboratory, western North Carolina, U.S.A.
- Ca2SiO3OHFA high-pressure phase with dense calcium polyhedral packing and tetrahedral silicon
- Relationships between SEM-cathodoluminescence response and trace-element composition of hydrothermal vein quartz
- Quantitative evaluation of attenuation contrast of X-ray computed tomography images using monochromatized beams
- Biotic and abiotic products of Mn(II) oxidation by spores of the marine Bacillus sp. strain SG-1
- The Mn, Mg-intracrystalline exchange reaction in donpeacorite (Mn0.54Ca0.03Mg1.43Si2O6) and its relation to the fractionation behavior of Mn in Fe, Mg-orthopyroxene
- Crystal structures of chalcostibite (CuSbS2) and emplectite (CuBiS2): Structural relationship of stereochemical activity between chalcostibite and emplectite
- Hydration and swelling of synthetic Na-saponites: Influence of layer charge
- Dehydroxylation and CO2 incorporation in annealed mica (sericite): An infrared spectroscopic study
- Relict coesite exsolution in omphacite from Western Tianshan eclogites, China
- Hyperfine electric field gradients and local distortion environments of octahedrally coordinated Fe2+
- A synchrotron Mössbauer spectroscopy study of (Mg,Fe)SiO3 perovskite up to 120 GPa
- Temporal stability and pressure calibration of barium carbonate and talc/pyrex pressure media in a piston-cylinder apparatus
- Cation ordering in magnesioferrite, MgFe2O4, to 982 °C using in situ synchrotron X-ray powder diffraction
- Halite-sylvite thermoconsolution
- The role of water in the structures of synthetic hallimondite, Pb2[(UO2)(AsO4)2](H2O)n and synthetic parsonsite, Pb2[(UO2)(PO4)2](H2O)n, 0 ≤ n ≤ 0.5
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- Letter. The effect of zinc sulfide on phase transformations of ferrihydrite
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