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Structure of nanosized materials by high-energy X-ray diffraction: study of titanate nanotubes
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Milen Gateshki
Published/Copyright:
September 25, 2009
High-energy X-ray diffraction and atomic Pair Distribution Function analysis are employed to determine the atomic-scale structure of titanate nanotubes. It is found that the nanotube walls are built of layers of Ti–O6 octahedra simular to those observed in crystalline layered titanates. In the nanotubes, however, the layers are bent and not stacked in perfect registry as in the crystal.
:
Received: 2007-May-16
Accepted: 2007-August-17
Published Online: 2009-9-25
Published in Print: 2007-11-1
© Oldenbourg Wissenschaftsverlag
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Articles in the same Issue
- Preface: Nanocrystallography
- Characterization of defect structures in nanocrystalline materials by X-ray line profile analysis
- Application of the apparent lattice parameter to determination of the core-shell structure of nanocrystals
- The formation and characterization of three-dimensional gold nanocrystal superlattices
- Grazing exit small angle X-ray scattering on grain formation in polycrystalline metal films
- Solving the 3D structure of metal nanoparticles
- Structure of nanosized materials by high-energy X-ray diffraction: study of titanate nanotubes
- Local atomic structure in disordered and nanocrystalline catalytic materials
- Quantitative structural analysis of individual nanotubes by electron diffraction
- Structural fingerprinting in the transmission electron microscope: overview and opportunities to implement enhanced strategies for nanocrystal identification
- Vibrational properties of metallic nanoparticles
- X-ray computed tomography in Zernike phase contrast mode at 8 keV with 50-nm resolution using Cu rotating anode X-ray source
- Sol-gel synthesis of rodlike polysilsesquioxanes forming regular higher-ordered nanostructure
- Crystal growth from cluster to bulk materials via nanomaterials
Keywords for this article
Synchrotron X-ray diffraction;
High energy X-ray diffraction;
Nanotubes;
Titanate
Articles in the same Issue
- Preface: Nanocrystallography
- Characterization of defect structures in nanocrystalline materials by X-ray line profile analysis
- Application of the apparent lattice parameter to determination of the core-shell structure of nanocrystals
- The formation and characterization of three-dimensional gold nanocrystal superlattices
- Grazing exit small angle X-ray scattering on grain formation in polycrystalline metal films
- Solving the 3D structure of metal nanoparticles
- Structure of nanosized materials by high-energy X-ray diffraction: study of titanate nanotubes
- Local atomic structure in disordered and nanocrystalline catalytic materials
- Quantitative structural analysis of individual nanotubes by electron diffraction
- Structural fingerprinting in the transmission electron microscope: overview and opportunities to implement enhanced strategies for nanocrystal identification
- Vibrational properties of metallic nanoparticles
- X-ray computed tomography in Zernike phase contrast mode at 8 keV with 50-nm resolution using Cu rotating anode X-ray source
- Sol-gel synthesis of rodlike polysilsesquioxanes forming regular higher-ordered nanostructure
- Crystal growth from cluster to bulk materials via nanomaterials
