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Growth and characterization of the new double sulphate, Li3Rb(SO4)2 · H2O
Veröffentlicht/Copyright:
28. Juli 2010
Abstract
A new double lithium rubidium sulphate, Li3Rb(SO4)2 · H2O, was found. Single crystals were obtained by drowning out in a tetramethoxysilane gel medium. The compound crystallises in the space group P1 with parameters a = 5.1356(4) Å, b = 4.9853(4) Å, and c = 8.2712(9) Å, α = 90.032(7)°, β = 105.729(6)°, γ = 90.004(7)° and Z = 1. The crystal structure was determinated by X-ray diffraction; in addition the new double sulphate was characterized by IR-spectroscopy. The system Rb2SO4–Li2SO4–H2O at 323 K is given.
Published Online: 2010-7-28
Published in Print: 1998-12-1
© 2015 Oldenbourg Wissenschaftsverlag GmbH, Rosenheimer Str. 145, 81671 München
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Artikel in diesem Heft
- Surface crystallography by low energy electron diffraction
- Growth and characterization of the new double sulphate, Li3Rb(SO4)2 · H2O
- Crystal structure determination of Ag2Ga by single crystal X-ray diffraction
- Crystal chemistry of inorganic compounds based on chains of oxocentered tetrahedra
- Crystal chemistry of inorganic compounds based on chains of oxocentered tetrahedra
- Crystal structures of manganese hydrogen sulfates – Mn(HSO4)2, Mn(HSO4)2 · H2O and Mn(HSO4)2(H2SO4)2
- The low-temperature structure and phase transition of hemimorphite, Zn4Si2O7(OH)2 · H2O
- The crystal and molecular structures of R2SnCl2(1,10-phenanthroline), R = iPr, Cy, CH2Ph and R2 = Me, Ph: a comparison between solid state and theoretical structures
Artikel in diesem Heft
- Surface crystallography by low energy electron diffraction
- Growth and characterization of the new double sulphate, Li3Rb(SO4)2 · H2O
- Crystal structure determination of Ag2Ga by single crystal X-ray diffraction
- Crystal chemistry of inorganic compounds based on chains of oxocentered tetrahedra
- Crystal chemistry of inorganic compounds based on chains of oxocentered tetrahedra
- Crystal structures of manganese hydrogen sulfates – Mn(HSO4)2, Mn(HSO4)2 · H2O and Mn(HSO4)2(H2SO4)2
- The low-temperature structure and phase transition of hemimorphite, Zn4Si2O7(OH)2 · H2O
- The crystal and molecular structures of R2SnCl2(1,10-phenanthroline), R = iPr, Cy, CH2Ph and R2 = Me, Ph: a comparison between solid state and theoretical structures
