anti-3,7-Bis(methylbenzyl)-3,7-diaza-10-oxa[3.3.3]-propellanium diiodide monohydrate, C24H34I2N2O2 (1) and 3-benzyl-7,10-bis(methylbenzyl)-3,7,10-triaza[3.3.3]-propellanium diiodide · 0.5 CH3CN · 0.72 H2O, C32H42.9I2N3.5O0.72 (2). Moieties based on I−…H2O…I− interactions

doi:10.1524/zkri.1998.213.1.52

Home anti-3,7-Bis(methylbenzyl)-3,7-diaza-10-oxa[3.3.3]-propellanium diiodide monohydrate, C24H34I2N2O2 (1) and 3-benzyl-7,10-bis(methylbenzyl)-3,7,10-triaza[3.3.3]-propellanium diiodide · 0.5 CH3CN · 0.72 H2O, C32H42.9I2N3.5O0.72 (2). Moieties based on I−…H2O…I− interactions

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anti-3,7-Bis(methylbenzyl)-3,7-diaza-10-oxa[3.3.3]-propellanium diiodide monohydrate, C₂₄H₃₄I₂N₂O₂ (1) and 3-benzyl-7,10-bis(methylbenzyl)-3,7,10-triaza[3.3.3]-propellanium diiodide · 0.5 CH₃CN · 0.72 H₂O, C₃₂H_42.9I₂N_3.5O_0.72 (2). Moieties based on I⁻…H₂O…I⁻ interactions

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From the journal Zeitschrift für Kristallographie - Crystalline Materials Volume 213 Issue 1

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"anti-3,7-Bis(methylbenzyl)-3,7-diaza-10-oxa[3.3.3]-propellanium diiodide monohydrate, C₂₄H₃₄I₂N₂O₂ (1) and 3-benzyl-7,10-bis(methylbenzyl)-3,7,10-triaza[3.3.3]-propellanium diiodide · 0.5 CH₃CN · 0.72 H₂O, C₃₂H_42.9I₂N_3.5O_0.72 (2). Moieties based on I⁻…H₂O…I⁻ interactions" Zeitschrift für Kristallographie - Crystalline Materials, vol. 213, no. 1, 1998, pp. 52-61. https://doi.org/10.1524/zkri.1998.213.1.52

(1998). anti-3,7-Bis(methylbenzyl)-3,7-diaza-10-oxa[3.3.3]-propellanium diiodide monohydrate, C₂₄H₃₄I₂N₂O₂ (1) and 3-benzyl-7,10-bis(methylbenzyl)-3,7,10-triaza[3.3.3]-propellanium diiodide · 0.5 CH₃CN · 0.72 H₂O, C₃₂H_42.9I₂N_3.5O_0.72 (2). Moieties based on I⁻…H₂O…I⁻ interactions. Zeitschrift für Kristallographie - Crystalline Materials, 213(1), 52-61. https://doi.org/10.1524/zkri.1998.213.1.52

(1998) anti-3,7-Bis(methylbenzyl)-3,7-diaza-10-oxa[3.3.3]-propellanium diiodide monohydrate, C₂₄H₃₄I₂N₂O₂ (1) and 3-benzyl-7,10-bis(methylbenzyl)-3,7,10-triaza[3.3.3]-propellanium diiodide · 0.5 CH₃CN · 0.72 H₂O, C₃₂H_42.9I₂N_3.5O_0.72 (2). Moieties based on I⁻…H₂O…I⁻ interactions. Zeitschrift für Kristallographie - Crystalline Materials, Vol. 213 (Issue 1), pp. 52-61. https://doi.org/10.1524/zkri.1998.213.1.52

"anti-3,7-Bis(methylbenzyl)-3,7-diaza-10-oxa[3.3.3]-propellanium diiodide monohydrate, C₂₄H₃₄I₂N₂O₂ (1) and 3-benzyl-7,10-bis(methylbenzyl)-3,7,10-triaza[3.3.3]-propellanium diiodide · 0.5 CH₃CN · 0.72 H₂O, C₃₂H_42.9I₂N_3.5O_0.72 (2). Moieties based on I⁻…H₂O…I⁻ interactions" Zeitschrift für Kristallographie - Crystalline Materials 213, no. 1 (1998): 52-61. https://doi.org/10.1524/zkri.1998.213.1.52

anti-3,7-Bis(methylbenzyl)-3,7-diaza-10-oxa[3.3.3]-propellanium diiodide monohydrate, C₂₄H₃₄I₂N₂O₂ (1) and 3-benzyl-7,10-bis(methylbenzyl)-3,7,10-triaza[3.3.3]-propellanium diiodide · 0.5 CH₃CN · 0.72 H₂O, C₃₂H_42.9I₂N_3.5O_0.72 (2). Moieties based on I⁻…H₂O…I⁻ interactions. Zeitschrift für Kristallographie - Crystalline Materials. 1998;213(1): 52-61. https://doi.org/10.1524/zkri.1998.213.1.52

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Abstract

The cations of the diazapropellanium salt 1 ([C₂₄H₃₂N₂O²⁺ · 2I⁻ · H₂O]) and the triazapropellanium salt 2 ([C₃₁H₃₉N₃²⁺ · 2I⁻ · 0.5(CH₃CN) · 0.72 H₂O]) have analogous configurations and conformations. Compound 2 decomposes in the MoK_α X-ray beam. Both compounds contain the known (but rather rare) I⁻…H₂O…I⁻ anion; previously reported manifestations of such interactions are classified in detail.

Published Online: 2010-7-28

Published in Print: 1998-1-1

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https://doi.org/10.1524/zkri.1998.213.1.52

Articles in the same Issue

A grid search procedure of positioning a known molecule in an unknown crystal structure with the use of powder diffraction data
On the indexing of 3T mica polytype
Symmetry analysis and the atomic distortions of the phase transitions in CsZnPO₄
The magnetic structure of braunite Mn²⁺Mn³⁺₆O₈/SiO₄
Amplitude sine modulated magnetic structures of DyPtGe₂
Crystal structures of di-tin-hexa(seleno)hypodiphosphate, Sn₂P₂Se₆, in the ferroelectric and paraelectric phase
Structure investigations of Tl(I)-arsenates(V): Tl₃(AsO₄), Tl₂Cu(I)(AsO₄) and TlCu(II)₂(AsO₄)(AsO₃OH)
Pulverdiffraktometrische Untersuchungen am System Sr_3−xCa_xAl₂O₆ sowie Einkristallstrukturanalysen für die Fälle x = 1,395(8), 1,62(1) und 2,12(1)
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The crystal and molecular structures of R₂Sn(O₂CR¹)Cl: R = Me, tBu and Ph; ⁻O₂CR¹ = o-(2-hydroxy-5-methylphenylazo)benzoate
Crystal structure of a benzene solvate of N-(4-methoxycarbonylphenylOoxycarbonylaziridino-[2′,3′: 1,2]-[60]fullerene