Startseite Crystal and molecular structure of C.I. Solvent Brown 1, 1,3-diamino phenyl azo-2-naphthalene
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Crystal and molecular structure of C.I. Solvent Brown 1, 1,3-diamino phenyl azo-2-naphthalene

Veröffentlicht/Copyright: 28. Juli 2010
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Zeitschrift für Kristallographie - Crystalline Materials
Aus der Zeitschrift Zeitschrift für Kristallographie - Crystalline Materials Band 209 Heft 8

Abstract

The crystal structure of C.I. Solvent Brown 1, C16H14N4, has been determined by single crystal X-ray diffraction techniques. It crystallises in the orthorhombic system with a = 12.771(1) Å, b = 13.021(1) Å, c = 16.244(3) Å, space group Pcab, (No. 61), Z = 8. The structure has been solved by direct methods and least-squares refinement has been completed on three dimensional data (2561 reflections, MoKα, radiation). The hydrogen atoms have been found but only their positional parameters refined. Final residual 0.096 (all intensity data). The molecule exists as an azo-compound in the trans configuration. The molecules are packed in columns parallel to the a axis, but, unusually, the molecular plane is almost parallel to the column axis. The molecules are linked by one hydrogen bond per molecule almost parallel to the b axis.

Published Online: 2010-7-28
Published in Print: 1994-8-1

© 2015 Oldenbourg Wissenschaftsverlag GmbH, Rosenheimer Str. 145, 81671 München

Artikel in diesem Heft

  1. Proportional colored symmetry of friezes
  2. Neutron microfocusing with bent crystals
  3. Structural phase transitions in the superionic conductors Na9{Fe2[PO4]4(O, F)2} and Na8{Ti2[PO4]4O2} in the temperature range 520–540 K
  4. Crystal structure of Nd3Au4 and Nd17Au36
  5. Crystal structure of MgAlPO5
  6. X-ray powder crystal structure analysis of high pressure tungsten dioxide. On the information in weak reflections
  7. Crystal structure of Z-2-(6,7-dimethoxytetrahydroisoquino-1-ylidene)-[2-(3,4-dimethoxyphenyl)-ethyl]-acetamide 1
  8. Synthesis and structural characterization of 1-[1-(naphthalenyl)]-3-(4-nitrophenyl)-2-propen-1-one1
  9. Structure of [4.4]paracyclophane and three [m.n]paracyclophane derivatives
  10. Crystal and molecular structure of C.I. Solvent Brown 1, 1,3-diamino phenyl azo-2-naphthalene
  11. An example of water forming double three-center hydrogen bonds. Crystal structure of bis(aquadichloromethylphenyltin) · 18-crown-6
  12. Crystal structure of tricopper tetraselenoantimonate (V), Cu3SbSe4
  13. Crystal structure of ammonium tetraiodoindate (III), NH4InI4
  14. Crystal structure of dicopper titanium tritelluride, Cu2TiTe3
  15. Crystal structure of cis-bis(diphenylphosphino)ethene, ((C6H5)2P)2C2H2
  16. Crystal structure of bis(triphenylphosphine)iminium tetrakis(pentafluorophenyl)aurate(III), [((C6H5)3P)2N]+[Au(C6F5)4]−
  17. Crystal structure of di(2-methoxy-3-t-butyl-5-methyl phenyl)methyl methyl ether, (H3COCH3C4H9C6H2)2HCOCH3
  18. Crystal structure of catena{bis[μ-(2-pyridinecarboxilato-μ-O2,O1,N)] mercury(II)}, Hg((C5H4N)(CO2))2
  19. Crystal structure of N,N-dimethylurea, (CH3)2NOCNH2
  20. Crystal structure of N,N-dimethylselenourea, (CH3)2NSeCNH2
  21. Crystal structure of N,N-dimethylthiourea, (CH3)2NSCNH2
  22. Crystal structure of μ-hydrido-μ-methylphenylphosphido-octacarbonyl-dirhenium, C15H9O8PRe2
  23. Crystal structure of μ-hydrido-μ-di-parafluorophenyl-phosphido-octacarbonyl-dirhenium, C20H9F2O8PRe2
  24. Crystal structure of μ-hydrido-μ-diphenylphosphido-octacarbonyl-dirhenium, C20H11O8PRe2
  25. Crystal structure of μ-hydrido-μ-di-paramethoxyphenyl-phosphido-octacarbonyl-dirhenium, C22H15O10PRe2
  26. Crystal structure of μ-hydrido-μ-bis(pentafluorophenyl)-phosphido-octacarbonyl-dirhenium, C20HF10O8PRe2
  27. Crystal structure of cerium dipalladium gallide, CePd2Ga
  28. Crystal structure of platinum silicon telluride, PtSiTe
https://doi.org/10.1524/zkri.1994.209.8.677

Artikel in diesem Heft

  1. Proportional colored symmetry of friezes
  2. Neutron microfocusing with bent crystals
  3. Structural phase transitions in the superionic conductors Na9{Fe2[PO4]4(O, F)2} and Na8{Ti2[PO4]4O2} in the temperature range 520–540 K
  4. Crystal structure of Nd3Au4 and Nd17Au36
  5. Crystal structure of MgAlPO5
  6. X-ray powder crystal structure analysis of high pressure tungsten dioxide. On the information in weak reflections
  7. Crystal structure of Z-2-(6,7-dimethoxytetrahydroisoquino-1-ylidene)-[2-(3,4-dimethoxyphenyl)-ethyl]-acetamide 1
  8. Synthesis and structural characterization of 1-[1-(naphthalenyl)]-3-(4-nitrophenyl)-2-propen-1-one1
  9. Structure of [4.4]paracyclophane and three [m.n]paracyclophane derivatives
  10. Crystal and molecular structure of C.I. Solvent Brown 1, 1,3-diamino phenyl azo-2-naphthalene
  11. An example of water forming double three-center hydrogen bonds. Crystal structure of bis(aquadichloromethylphenyltin) · 18-crown-6
  12. Crystal structure of tricopper tetraselenoantimonate (V), Cu3SbSe4
  13. Crystal structure of ammonium tetraiodoindate (III), NH4InI4
  14. Crystal structure of dicopper titanium tritelluride, Cu2TiTe3
  15. Crystal structure of cis-bis(diphenylphosphino)ethene, ((C6H5)2P)2C2H2
  16. Crystal structure of bis(triphenylphosphine)iminium tetrakis(pentafluorophenyl)aurate(III), [((C6H5)3P)2N]+[Au(C6F5)4]−
  17. Crystal structure of di(2-methoxy-3-t-butyl-5-methyl phenyl)methyl methyl ether, (H3COCH3C4H9C6H2)2HCOCH3
  18. Crystal structure of catena{bis[μ-(2-pyridinecarboxilato-μ-O2,O1,N)] mercury(II)}, Hg((C5H4N)(CO2))2
  19. Crystal structure of N,N-dimethylurea, (CH3)2NOCNH2
  20. Crystal structure of N,N-dimethylselenourea, (CH3)2NSeCNH2
  21. Crystal structure of N,N-dimethylthiourea, (CH3)2NSCNH2
  22. Crystal structure of μ-hydrido-μ-methylphenylphosphido-octacarbonyl-dirhenium, C15H9O8PRe2
  23. Crystal structure of μ-hydrido-μ-di-parafluorophenyl-phosphido-octacarbonyl-dirhenium, C20H9F2O8PRe2
  24. Crystal structure of μ-hydrido-μ-diphenylphosphido-octacarbonyl-dirhenium, C20H11O8PRe2
  25. Crystal structure of μ-hydrido-μ-di-paramethoxyphenyl-phosphido-octacarbonyl-dirhenium, C22H15O10PRe2
  26. Crystal structure of μ-hydrido-μ-bis(pentafluorophenyl)-phosphido-octacarbonyl-dirhenium, C20HF10O8PRe2
  27. Crystal structure of cerium dipalladium gallide, CePd2Ga
  28. Crystal structure of platinum silicon telluride, PtSiTe
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