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Crystal and molecular structure of N-p-fluorobenzoyl-l-valine
Published/Copyright:
August 25, 2010
Abstract
The title compound, (C12H14NO3F), N-p-fluorobenzoyl-l-valine, crystallizes in the orthorhombic space group P212121 with unit cell parameters a = 10.743(1), b = 11.534(1), c = 20.013(5) Å, Z = 8; Dx = 1.281 Mg m−3. The structure was solved by direct-methods and refined by a full-matrix least-squares procedure on 2757 reflections to final R = 0.045. The two molecules comprising the crystallographic asymmetric unit differ from each other as a result of a rotation about the C(2) – C(3) bond. All potential hydrogen bonding sites on each molecule participate in a complicated, three-dimensional hydrogen bonding network which is described in detail.
Published Online: 2010-08-25
Published in Print: 1989
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- An uncommon Cu[2+4]O6 coordination polyhedron in the crystal structure of KCu3(OH)2[(AsO4)H(AsO4)] (with a comparison to related structure types)
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- The crystal structure of hexaaquacopper(II) bis(7-oxabicyclo[2.2.1]heptane-2,3-dicarboxylato)cuprate(II)
- Crystal and molecular structure of an isostere of purine ring system: 7-benzylamino-2-methylmercaptothiazolo [5,4-d] pyrimidine
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