Startseite Accurate Bragg intensities for uracil: a thermal parameter refinement
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Accurate Bragg intensities for uracil: a thermal parameter refinement

Veröffentlicht/Copyright: 28. Juli 2010
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Abstract

Accurate and extensive three-dimensional intensity data for a single crystal of uracil have been collected by diffractometry using MoK[unk] x-radiation. The average precision in the Bragg intensities is less than 2%. Secondary extinction was eliminated by powder-diffraction measurements. Multiple diffraction could not be detected. The interaction of thermal parameters with scattering factors is analyzed with a simple model. A refinement of the anisotropic thermal parameters, based on reflections for which (sinθ)/λ exceeds.648 Å−1, led to values which are significantly different from refinement based on all data. The carbon-atom parameter differences are consistent with recent studies of combined x-ray and neutron-diffraction analysis.

Published Online: 2010-07-28
Published in Print: 1969-02
Heruntergeladen am 14.10.2025 von https://www.degruyterbrill.com/document/doi/10.1524/zkri.1969.128.1-2.133/html?lang=de
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