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Studies on etching of neutron-irradiated calcium fluoride single crystals

Published/Copyright: July 28, 2010
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Abstract

Good quality natural crystals of calcium fluoride obtained from Amba Dungar mines of Chhota Udepur, Gujarat State, India, were cleaved, and a number of matched pairs were obtained. One piece from each pair was irradiated with different doses of neutrons in the swimming-pool Aspara Reactor at Trombay, India. After irradiation, the irradiated and their non-irradiated counterparts were matched. They were then etched simultaneously in 0.28 N perchloric acid for the same period. The etch patterns produced were studied optically. They were successively etched for three different periods, and the sizes and the depths of the pits on the nonirradiated and irradiated cleavages were measured. It is observed that (i) the irradiated cleavages etch at a faster rate than non-irradiated cleavages and, (ii) the rate of etching increases with increase in the dose of irradiation.

A crystal plate 3.86 mm thick, irradiated with a dose of 1.3 · 1010 n/cm2, was selected and cleaved into five thinner plates. All of them were etched simultaneously for the same period and the etch rate measured on them. As one proceeds within the body of the crystal it is observed that the etch rates on the faces increase with increase in the distance from the outer surface. The implications are discussed.

Published Online: 2010-07-28
Published in Print: 1968-01

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