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Single crystals grown from small droplets
Veröffentlicht/Copyright:
28. Juli 2010
Abstract
Single crystal droplets of Au, Cu, Ag, Pb, In, Cu3Au, and Ge have been grown in vacuum by two simple methods. In each case graphite crucibles were employed and served as a surface for point contact so that the droplets could solidify in the absence of a containment shell, free of mechanical and thermal stresses. The crystals approximate spheres ranging from 50 to 600 microns in diameter and are thus ideally suited for x-ray diffraction studies in transmission. Although the surface tension properties of the materials were important to the successful growth characteristics, it was also observed that exclusion of foreign nuclei and elimination of mechanical and thermal stresses were equally significant.
Published Online: 2010-07-28
Published in Print: 1963-11
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Artikel in diesem Heft
- Kristallstrukturbestimmung von Imidazol (C3N2H4) mit Faltmolekülen*
- Die Kristallstruktur einiger Alkohol-Halbhydrate
- Applications of Fourier-transform theory to electron-density extraction of Patterson functions
- Single crystals grown from small droplets
- The crystal structure of dachiardite
- Structure, growth and morphology of crystals*
- A back-reflection x-ray camera for thermal-expansion studies and the thermal expansion of NaCl from −180°C to 200°C
- High-pressure scheelite-structure polymorphs of rare-earth vanadates and arsenates
- The redetermination and refinement of the crystal structure of rhodonite, (Mn,Ca)SiO3
- The crystal structure of hodgkinsonite Zn2Mn [(OH)2|SiO4]
- Atomic radii in metals
- Derivation of the two-sided, two-colored, band groups with their associated point groups and a numerical correction
- Some crystallographic properties of CaSeO4 and its hydrates
- Space group of biguanide acid sulphate
- The unit-cell of freudenbergite
Artikel in diesem Heft
- Kristallstrukturbestimmung von Imidazol (C3N2H4) mit Faltmolekülen*
- Die Kristallstruktur einiger Alkohol-Halbhydrate
- Applications of Fourier-transform theory to electron-density extraction of Patterson functions
- Single crystals grown from small droplets
- The crystal structure of dachiardite
- Structure, growth and morphology of crystals*
- A back-reflection x-ray camera for thermal-expansion studies and the thermal expansion of NaCl from −180°C to 200°C
- High-pressure scheelite-structure polymorphs of rare-earth vanadates and arsenates
- The redetermination and refinement of the crystal structure of rhodonite, (Mn,Ca)SiO3
- The crystal structure of hodgkinsonite Zn2Mn [(OH)2|SiO4]
- Atomic radii in metals
- Derivation of the two-sided, two-colored, band groups with their associated point groups and a numerical correction
- Some crystallographic properties of CaSeO4 and its hydrates
- Space group of biguanide acid sulphate
- The unit-cell of freudenbergite
