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Synthesis and Liquid Crystalline Properties of Novel Imides and Thioimides with Chiral Aliphatic Tails

  • Andrzej Orzeszko EMAIL logo , Dorota Melon-Ksyta , Ewa Kowalczyk and Krzysztof Czupryński
Published/Copyright: June 2, 2014
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Zeitschrift für Naturforschung B
From the journal Zeitschrift für Naturforschung B Volume 58 Issue 10

Three chiral compounds (R)-octan-2-ol, (S)-citronellol and (S)-citronellyl bromide were used for the synthesis of novel ester imides with biphenyl moieties as mesogenic units. Observations by means of polarising microscopy as well as DSC measurements revealed the presence of SmC* and/or SmA phases for all the compounds examined. It was found that the biphenyl units with long chiral alkoxy substituents induce smectic C phases.

Keywords: Imides; Thioimides; Liquid Crystals
Received: 2003-5-2
Published Online: 2014-6-2
Published in Print: 2003-10-1

© 1946 – 2014: Verlag der Zeitschrift für Naturforschung

Articles in the same Issue

  1. Non-Stoichiometric Monoclinic Cr5Se8 Prepared at High-Pressure and High-Temperature and the Crystal Structure Refined from Rietveld Data
  2. SiF-NH-Funktionelle Cyclodisilazane – Synthese und Reaktivität / SiF-NH-Functional Cyclodisilazane – Synthesis and Reactivity
  3. Synthesis, Electronic Spectra and Solvent-Induced Reversible Dissociation of Diphosphine(hexafluoroacetylacetonato)copper(I) Complexes
  4. Synthesis, Crystal Structure and Spectroscopic Properties of a Dinuclear Nickel(II) Complex Bridged by an Alkoxide and a μ-Pyrazolate Ligand
  5. Formation and Structural Characterization of [RuCl2(CO)2(SPh2)2], [RuCl2(CO)3(OH2)], and [Ru(OH2)6][RuCl3(CO)3]2 · 2H2O
  6. Is 2-D Graphite an Ultimate Large Hydrocarbon? IV. Structure and Energy Spectra of Large Polycyclic Aromatic Hydrocarbons with Different Symmetry
  7. Crystal Structure of Eu2PdSi3
  8. Darstellung und 51V-NMR-spektroskopische Untersuchungen von η5-Cyclopentadienyl-tert-butylimidovanadium(III)-Komplexen mit σ-Donator, π-Akzeptor-Liganden / Synthesis and 51V NMR Spectroscopic Studies of η5 -Cyclopentadienyl-tert-butylimidovanadium( III) Complexes with σ -Donor, π -Acceptor Ligands
  9. Reduktion von Isochinolin und Indol mit Cäsium in flüssigem Ammoniak / Reduction of Isoquinoline and Indole with Cesium in Liquid Ammonia
  10. Synthesis of trans-Configurated Spacered Nucleoside Analogues Comprising a Difluorocyclopropane Moiety
  11. Generation and Structural Characterization of an [(Imidazol-2-ylidene)HfCl5]-Anion/Imidazolium Cation Salt
  12. Synthesis and Characterization of Copper(II) and Zinc(II) Complexes Containing 1-Phenyl-3-methyl-4-benzoyl-5-pyrazolone
  13. Synthesis and Liquid Crystalline Properties of Novel Imides and Thioimides with Chiral Aliphatic Tails
  14. Note: Synthesis of the Dinuclear Halogeno-Bridged Complexes [Re2(μ-X)2(CO)6(CH3CN)2], (X = Cl, Br)
  15. Dawenol, a New Polyene Metabolite from the Myxobacterium
  16. A Novel Methylene Dithioether as a Ligand: Synthesis and Molecular Structure of a Zinc(II) Complex with N4S2 Coordination Environment
  17. Synthesis and Tin(IV) Coordination Chemistry of the Novel Tripod N(CH2CH2CH2SH)3
https://doi.org/10.1515/znb-2003-1013
Keywords for this article
Imides; Thioimides; Liquid Crystals

Articles in the same Issue

  1. Non-Stoichiometric Monoclinic Cr5Se8 Prepared at High-Pressure and High-Temperature and the Crystal Structure Refined from Rietveld Data
  2. SiF-NH-Funktionelle Cyclodisilazane – Synthese und Reaktivität / SiF-NH-Functional Cyclodisilazane – Synthesis and Reactivity
  3. Synthesis, Electronic Spectra and Solvent-Induced Reversible Dissociation of Diphosphine(hexafluoroacetylacetonato)copper(I) Complexes
  4. Synthesis, Crystal Structure and Spectroscopic Properties of a Dinuclear Nickel(II) Complex Bridged by an Alkoxide and a μ-Pyrazolate Ligand
  5. Formation and Structural Characterization of [RuCl2(CO)2(SPh2)2], [RuCl2(CO)3(OH2)], and [Ru(OH2)6][RuCl3(CO)3]2 · 2H2O
  6. Is 2-D Graphite an Ultimate Large Hydrocarbon? IV. Structure and Energy Spectra of Large Polycyclic Aromatic Hydrocarbons with Different Symmetry
  7. Crystal Structure of Eu2PdSi3
  8. Darstellung und 51V-NMR-spektroskopische Untersuchungen von η5-Cyclopentadienyl-tert-butylimidovanadium(III)-Komplexen mit σ-Donator, π-Akzeptor-Liganden / Synthesis and 51V NMR Spectroscopic Studies of η5 -Cyclopentadienyl-tert-butylimidovanadium( III) Complexes with σ -Donor, π -Acceptor Ligands
  9. Reduktion von Isochinolin und Indol mit Cäsium in flüssigem Ammoniak / Reduction of Isoquinoline and Indole with Cesium in Liquid Ammonia
  10. Synthesis of trans-Configurated Spacered Nucleoside Analogues Comprising a Difluorocyclopropane Moiety
  11. Generation and Structural Characterization of an [(Imidazol-2-ylidene)HfCl5]-Anion/Imidazolium Cation Salt
  12. Synthesis and Characterization of Copper(II) and Zinc(II) Complexes Containing 1-Phenyl-3-methyl-4-benzoyl-5-pyrazolone
  13. Synthesis and Liquid Crystalline Properties of Novel Imides and Thioimides with Chiral Aliphatic Tails
  14. Note: Synthesis of the Dinuclear Halogeno-Bridged Complexes [Re2(μ-X)2(CO)6(CH3CN)2], (X = Cl, Br)
  15. Dawenol, a New Polyene Metabolite from the Myxobacterium
  16. A Novel Methylene Dithioether as a Ligand: Synthesis and Molecular Structure of a Zinc(II) Complex with N4S2 Coordination Environment
  17. Synthesis and Tin(IV) Coordination Chemistry of the Novel Tripod N(CH2CH2CH2SH)3
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