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Analytical and experimental investigation of tensile properties of cross-ply and angle-ply GFRP composite laminates

  • Mostefa Bourchak EMAIL logo and Wail Harasani
Published/Copyright: December 13, 2013

Abstract

The static tensile properties in the form of ultimate failure stress, ultimate failure strain and Young’s modulus of a cross-ply glass fiber-reinforced polymer (GFRP) composite laminate [904, 04]s and an unconventional angle-ply GFRP composite laminate [+67.54, -67.54]s were investigated using the netting analysis, the laminate mixture rule (Hart-Smith 10% rule) and the classical laminate theory (CLT). The findings were then compared to experimental results to determine the accuracy of each analytical technique. It was found that the netting analysis was the best overall method for estimating the cross-ply laminate tensile properties, whereas neither the CLT nor the 10% rule were appropriate for estimating the tensile properties of the unconventional ply angle laminate.

1 Introduction

It is well known that for better structural design analysis, composite laminate mechanical properties are best derived experimentally. However, due to the large number of possible composite laminate configurations (through changing ply angle and stacking sequences), relying on experiments to estimate the failure properties would be time-consuming and costly. Consequently, many theoretical composite laminate failure theories have been proposed [1] to assist designers in estimating the tensile properties. The netting analysis [2–4] and the rule of mixtures such as the Hart-Smith 10% rule [4] are empirical laminate analysis methods for the first estimate of stiffness and strength. They are both related to in-plane extensional loading/deformation only, fiber-dominated properties only and final ply fiber failure mode only. They are also both based on rules of fiber-dominated 0°, 45° and 90° layups. Whereas the netting analysis assumes only lamina fiber direction to provide stiffness and strength (i.e., no stiffness and strength contribution from off-axis plies), the laminate mixture rule assumes empirical contribution from off-axis plies, e.g., the aerospace widely used 10% off-axis contribution Hart-Smith rule [5]. Although the latter was originally derived for 0°, 45° and 90° ply laminates, it has been reported in the literature that an extended version includes other nonconventional angles [6] such as the one used in this work ([+67.54, -67.54]s). Moreover, CLT is an analytical method used to estimate composite laminate stiffness and strength based on the summation of transformed lamina in-plane linear elastic stiffness and in-plane intralaminar failure mode [7].

In this work, conventional netting analysis, 10% rule and CLT were used to estimate the tensile properties of two glass fiber-reinforced polymer (GFRP) composite laminates ([904, 04]s and [+67.54, -67.54]s). These theoretical outcomes were then compared to experimental findings.

2 Material preparation

The specimens were made using unidirectional Interglas 92145 glass filament fabrics (INTERGLAS, Erbach, Germany) and EPOLAM 2063 (AXSON TECHNOLOGIES, Cergy cedex, France) two-component epoxy matrix system. Two GFRP composite laminates were manufactured: one laminate having a [904, 04]s layup, and the other a [+67.54, -67.54]s layup. Both were made using the resin infusion technique and then post-cured in an oven according to the resin manufacturer’s recommended cure cycle and temperature. Laminates were made with a fiber volume fraction of approximately 40%. Specimens were then cut according to the ASTM standard for polymer matrix composite tensile properties [8]. The specimens were 2.4 mm thick, 20 mm wide and 105 mm in gauge length. Tensile static tests were then carried out using an MTS 809 axial/torsional servohydraulic test system (MTS, MN, USA) at a load displacement rate of 2 mm/min. A single ply of the GFRP material used when mixed with the EPOLAM 2063 two-component epoxy matrix system has mechanical properties as shown in Table 1.

Table 1

Interglas 92145/EPOLAM 2063 mechanical properties.

PropertySymbolValue
Fiber volume fractionVf0.45
Longitudinal tensile elastic modulusE11T33 GPa
Longitudinal compression elastic modulusE11C28 GPa
Transverse elastic modulusE223.1 GPa
Shear modulusG123 GPa
Ultimate longitudinal tensile strength(σ11T)ult630 MPa
Ultimate longitudinal compression strength(σ11C)ult510 MPa
Ultimate transverse tensile strength(σ22T)ult57 MPa
Ultimate in-plane shear strength12)ult50 MPa
Ultimate longitudinal tensile strain(ε11T)ult1.91%
Ultimate longitudinal compression strain(ε11C)ult1.82%
Ultimate transverse tensile strain(ε22T)ult1.84%
Ultimate in-plane shear strain(ε12)ult1.67%
Poisson’s ratioN0.26
Ply thicknessT0.15 mm

3 Results and discussion

3.1 Netting analysis

Netting analysis is an empirical composite laminate analysis method. It assumes that only lamina fiber direction provides stiffness or strength, i.e., no contribution from off-axis plies. The composite laminate tensile mechanical properties can be derived as follows:

(1)Ultimate tensile strength:(σxT)ult=t0tt×(σ11T)ult (1)
(2)Ultimate tensile strain:(εxT)ult=t0tt×(ε11T)ult (2)
(3)Young'smodulus:Ex=t0tt×E11 (3)

where t0 is the 0° ply total thickness and tt is the laminate total thickness.

However, because there are no 0° plies in the [+67.54, -67.54]s laminate, the conventional netting analysis is unable to predict any of the tensile mechanical properties for this specific laminate.

3.2 Laminate mixture rule

The laminate mixture rule is also an empirical composite laminate analysis method. It assumes an empirical contribution from off-axis plies, e.g., 10% off-axis contribution (Hart-Smith rule). The composite laminate tensile mechanical properties can be derived as follows:

(4)(σxT)ult=(t0tt×(σ11T)ult)+0.1×(tθtt×(σ11T)ult) (4)
(5)(εxT)ult=(t0tt×(ε11T)ult)+0.1×(tθtt×(ε11T)ult) (5)
(6)Ex=(t0tt×E11)+0.1×(tθtt×E11) (6)

where t0 is the 0° ply total thickness, tθ is the θ° ply total thickness and tt is the laminate total thickness.

3.3 Classical laminate theory (CLT)

CLT is a linear elastic ply constitutive relations method at the macroscopic level. It works for plane stress cases to derive in-plane laminate mechanical properties. Tensile tests are considered to be a linear-elastic stress-strain analysis load configuration, which can be numerically investigated using CLT. The latter temperature thermoelastic analysis is not considered for this case. CLT uses the maximum strain failure criterion, which accounts for:

  • Ply transverse, shear and fiber failure modes in tension or compression

  • Partial ply failure with transverse and shear property degradation

  • Last ply failure at fiber failure

Generally, CLT is applicable to symmetric balanced laminates with multiple orthotropic or isotropic plies such as the unidirectional glass used in this work. CLT also accounts for different material properties, thicknesses and fiber angles. In a composite laminate, stresses are generally different on plies with different orientation (as in this work) or different material properties. Consequently, some plies are bound to fail first before others, which is generally referred to as first-ply failure [9]. The tensile properties are estimated using the following equation:

(7){NxNyNxy}=[A11A12A16A12A22A26A16A26A66]{εxεyγxy} (7)

where the Ni vector represents the loading intensities, and

(8)Aij=k=1n[Q¯ij]k(tk-tk-1) (8)

where t is the laminate thickness and tk is the kth laminate thickness.

Because the laminates used in this work are symmetric and only longitudinal loading is considered, Eq. (7) reduces to:

(9){Nx00}=[A11A120A12A22000A66]{εxεy0} (9)

which gives

(10)Ex=1t[A11-A122A22] (10)
(11)σx=Nxt (11)
(12)εx=σxEx (12)

The rest of the ply failure calculations are carried out using one of the many freely available CLT software packages. These programs initially perform laminate analysis for given loading (axial in this case), and then they obtain stresses and strains in each layer in 1-2 ply axes, which are checked against the failure criteria for each mode (1-1 fiber failure, 2-2 transverse failure and 1-2 shear matrix failure). If a ply fails in matrix-dominated mode (i.e., 2-2 or 1-2), then the code degrades layer stiffness properties (E2 and G12) and it repeats analysis. If, however, a ply has failed in fiber-dominated mode, i.e., 1-1, then the code assumes final failure and the code stops analysis.

3.4 Experimental results

Figures 1 and 2 show the tensile test results of three specimens, each of both laminates considered for this work. The achieved stress and strain values for each specimen are very consistent with each other, i.e., with little scatter. The obtained ultimate values are summarized in Tables 1 and 2 for [904, 04]s and [+67.54, -67.54]s laminates, respectively. From Figure 1, it can be seen that the slope was linear up to around 150 MPa, when a visible change in slope occurred, with the rest of the curve showing linear variation to final failure. Rusnáková et al. [10] used similar glass fibers (Fiberglas 92145) and reported lower ultimate failure stresses and strains for 0/90 cross-ply laminates compared to the findings of this work. They reported a maximum failure stress of 371 MPa and a maximum failure strain of 0.0548. However, it should be noted that the matrix system they used is different from the one used for this work. Moreover, Figure 2 shows that the strength of [+67.54, -67.54]s laminates is considerably weaker compared to that of [904, 04]s laminates due to mainly the matrix taking the tensile load and not much being carried by the fibers. It is also noted that the stress/strain curve starts to change its slope just after the 30-MPa mark, indicating the onset of matrix failure.

Table 2

Summary of [904, 04]s specimen tensile results.

Analysis methodEx (GPa)Ultimate failure stress (MPa)Ultimate failure strain (mm/mm)
Netting (error % compared to experiment)16.5 (11)315 (-35)0.019 (-53)
10% Rule (error % compared to experiment)18.5 (21)346.5 (-22)0.0187 (-56)
CLA (error % compared to experiment)18.13 (19)767.8 (44)0.042 (30)
Experiment14.64260.0292
Figure 1 Stress vs. strain curves for [904, 04]s specimens.
Figure 1

Stress vs. strain curves for [904, 04]s specimens.

Figure 2 Stress vs. strain curves for [+67.54, -67.54]s specimens.
Figure 2

Stress vs. strain curves for [+67.54, -67.54]s specimens.

3.5 Comparison between all methods

Tables 2 and 3 and Figures 3 and 4 summarize the results of all methods used in this work and how they compare to experimental data. The conventional netting analysis is unable to estimate the [+67.54, -67.54]s laminate properties because this method does not account for any off-axis plies.

Figure 3 Summary of [+904, -904]s comparison results.
Figure 3

Summary of [+904, -904]s comparison results.

Figure 4 Summary of [+67.54, -67.54]s comparison results.
Figure 4

Summary of [+67.54, -67.54]s comparison results.

Table 3

Summary of [+67.54, -67.54]s specimen tensile results.

Analysis methodEx (GPa)Ultimate failure stress (MPa)Ultimate failure strain (mm/mm)
Netting (error % compared to experiment)N/AN/AN/A
10% Rule (error % compared to experiment)3.3 (-121)63 (-26)0.02 (+45)
CLA (error % compared to experiment)4.175 (-74)32.14 (-148)0.008 (-37)
Experiment7.3800.011

N/A, Not Applicable

For the [904, 04]s laminate, it can be seen from the summary of results that for the ultimate failure stress, the 10% rule gave the lowest error (-22%) compared to experimental data, with the netting analysis underestimating the ultimate tensile strength by 35% and the CLT overestimating it by 44%. In terms of Young’s modulus, the netting analysis gave the lowest error (11%), whereas the 10% rule and CLT gave comparable overestimates of around 20% compared to the experimental data. However, for ultimate failure strain predictions, the CLT produced the lowest error of 30%, whereas both the netting analysis and the 10% rule underestimated the ultimate failure strain by around 50%.

For the [+67.54, -67.54]s laminate, it can be seen from the summary of results in Table 3 that for ultimate failure stress the 10% rule gave the lowest error (-26%) compared to experimental data, with the CLT underestimating it by almost three times. In terms of Young’s modulus, the CLT underestimated it by 74%, and the 10% rule underestimated it by more than 100%. However, for ultimate failure strain predictions, the CLT produced the lowest error of -37%, whereas the CLT overestimated the ultimate failure strain by around 45%.

4 Conclusion

Two GFRP laminates were manufactured using liquid resin infusion technique. Specimens were cut from these laminates and tested under static tensile loading using a universal test machine. One laminate had a cross-ply stacking sequence, [+904, -904]s, and another had an unconventional angle-ply stacking sequence, [+67.54, -67.54]s. The tensile properties of each laminate were initially estimated using three analytical techniques, namely, the netting analysis, the laminate mixture rule (Hart-Smith 10% rule) and the classical laminate theory. The obtained results were compared to experimental data. Experimental results contained very little scatter in data. The results indicated that the netting analysis performed better for estimating the cross-ply laminate tensile properties, whereas for the unconventional angle-ply laminates neither the empirical nor the CLT methods were able to produce acceptable results compared to the experimental findings. The implication is that the CLT as well as other conventional empirical methods should only be used for conventional ply angles of 0°, 45° and 90° unless modifications are made to allow for nonconventional angle-ply laminates such as the one studied in this work.


Corresponding author: Mostefa Bourchak, Faculty of Engineering, Department of Aeronautical Engineering, King Abdulaziz University, PO Box 80204, Jeddah Makkah 21589, Saudi Arabia, Phone: +966 2 6402000 Ext.: 66031, Fax: +966 2 695 2944, e-mail:

Acknowledgments

The authors would like to thank Dr. Ian Farrow from Bristol University Aerospace Engineering Department for the use of his CLT program.

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Received: 2013-4-22
Accepted: 2013-10-26
Published Online: 2013-12-13
Published in Print: 2015-5-1

©2015 by De Gruyter

This article is distributed under the terms of the Creative Commons Attribution Non-Commercial License, which permits unrestricted non-commercial use, distribution, and reproduction in any medium, provided the original work is properly cited.

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