Home Production and characterization of waste walnut shell powder that can be used as a sustainable eco-friendly reinforcement in biocomposites
Article
Licensed
Unlicensed Requires Authentication

Production and characterization of waste walnut shell powder that can be used as a sustainable eco-friendly reinforcement in biocomposites

  • Bekir Çevik

    Assoc. Prof. Dr. Bekir Çevik, born in 1983, Mechanical Engineer, received his BSc degree from Gazi University and Düzce University, Turkey, in 2006 and 2021. He received his MSc degree in Institute of Science and Technology, Gazi University, in 2009 and completed his PhD at the same university and in the same science fields in 2014. He has been working in the Department of Biosystems Engineering of Düzce University, Turkey. His research interests include materials science, mainly residual stress, welding, and biocomposites.

    ORCID logo EMAIL logo
    and Yücel Avşar

    Research Assistant Yücel Avşar graduated from Çukurova University, Faculty of Agriculture, Department of Agricultural Machinery, in 2018. In 2020, he started working as a research assistant at the Düzce University Faculty of Agriculture, Department of Biosystems Engineering. He completed his master’s degree at Çukurova University, Department of Agricultural Machinery and Technologies Engineering, in 2022. He is currently continuing his PhD education in the same department.

Published/Copyright: May 22, 2024
Become an author with De Gruyter Brill

Abstract

The rapid depletion of natural resources and the increase of environmental problems due to production-related waste necessitate sustainable waste management. In particular, reintroducing by-products and waste generated by agricultural activities into the economy is critical to reduce environmental pollution, solve the storage problem, and promote sustainability. Agricultural wastes such as fiber, husks, cobs, stalks, straw, dust, and particles are recyclable and can be innovatively reused in various sectors. One of the innovative fields where sustainable agricultural waste management can be implemented is the development of biocomposites. One of the most important steps in the production of biocomposites reinforced with agricultural waste is processing the waste biomass and making it usable as a reinforcing element. This study investigated the production of powder reinforcements for biocomposite material from the biomass of walnut shells using a ring mill. The walnut shells, mechanically reduced in size, were first dried at 100 °C for 3 h and ground at four different grinding times (10, 20, 30, and 40 min). Afterward, the waste walnut shell powders were subjected to sieve analysis and precise weight measurements. Then, the waste walnut shell powders, which were dried at 100 °C for 3 h and ground for 40 min, were subjected to a second drying process at 100 °C (60, 180, and 300 min) and ground again for 40 min. Then, the resulting waste walnut shell powders were subjected to sieve analysis, precision weight measurements, and microscopic, and SEM analyses to determine the characterization of the powders.


Corresponding author: Bekir Çevik and Yücel AvŞar, Department of Biosystems Engineering, 121595 Düzce University , Düzce, Türkiye, E-mail: (B. Çevik), (Y. AvŞar)

Funding source: Düzce University Research Fund.

Award Identifier / Grant number: 2022.11.01.1369

About the authors

Bekir Çevik

Assoc. Prof. Dr. Bekir Çevik, born in 1983, Mechanical Engineer, received his BSc degree from Gazi University and Düzce University, Turkey, in 2006 and 2021. He received his MSc degree in Institute of Science and Technology, Gazi University, in 2009 and completed his PhD at the same university and in the same science fields in 2014. He has been working in the Department of Biosystems Engineering of Düzce University, Turkey. His research interests include materials science, mainly residual stress, welding, and biocomposites.

Yücel Avşar

Research Assistant Yücel Avşar graduated from Çukurova University, Faculty of Agriculture, Department of Agricultural Machinery, in 2018. In 2020, he started working as a research assistant at the Düzce University Faculty of Agriculture, Department of Biosystems Engineering. He completed his master’s degree at Çukurova University, Department of Agricultural Machinery and Technologies Engineering, in 2022. He is currently continuing his PhD education in the same department.

  1. Research ethics: The author declares no conflicts of interest. This article does not contain any studies involving animals or human participants performed by the author.

  2. Author contributions: All the authors have accepted responsibility for the entire content of this submitted manuscript and approved submission.

  3. Competing interests: The authors declare that there are no financial or commercial conflicts of interest.

  4. Research funding: This study is supported by Düzce University Research Fund Project Number: 2022.11.01.1369.

  5. Data availability: All data generated or analyzed during this study are included in this published article.

References

[1] M. Balat and G. Ayar, “Biomass energy in the world, use of biomass and potential trends,” Energy Sources, vol. 27, no. 10, pp. 931–940, 2005, https://doi.org/10.1080/00908310490449045.Search in Google Scholar

[2] A. Fitzgerald, ., “A life cycle engineering perspective on biocomposites as a solution for a sustainable recovery,” Sustainability, vol. 13, no. 3, p. 1160, 2021, https://doi.org/10.3390/su13031160.Search in Google Scholar

[3] S. Gairola, T. P. Naik, S. Sinha, and I. Singh, “Corncob waste as a potential filler in biocomposites: a decision towards sustainability,” Compos Part C: Open Access, vol. 9, 2022, Art. no. 100317, https://doi.org/10.1016/j.jcomc.2022.100317.Search in Google Scholar

[4] G. Açıkbaş, “Interfacial and physico-mechanical properties of walnut shell fiber reinforced polyester matrix composites,” Mater. Test., vol. 60, no. 5, pp. 510–518, 2018, https://doi.org/10.3139/120.111176.Search in Google Scholar

[5] M. Núñez-Decap, A. Wechsler-Pizarro, and M. Vidal-Vega, “Mechanical, physical, thermal and morphological properties of polypropylene composite materials developed with particles of peach and cherry stones,” Sustain. Mater. Technol., vol. 29, 2021, Art. no. e00300, https://doi.org/10.1016/j.susmat.2021.e00300.Search in Google Scholar

[6] B. Koul, M. Yakoob, and M. P. Shah, “Agricultural waste management strategies for environmental sustainability,” Environ. Res., vol. 206, 2022, Art. no. 112285, https://doi.org/10.1016/j.envres.2021.112285.Search in Google Scholar PubMed

[7] C. Koçhan, “Mechanical properties of waste mussel shell particles reinforced epoxy composites,” Mater. Test., vol. 61, no. 2, pp. 149–154, 2019, https://doi.org/10.3139/120.111298.Search in Google Scholar

[8] A. Kaab, M. Sharifi, H. Mobli, A. Nabavi-Pelesaraei, and K. Chau, “Combined life cycle assessment and artificial intelligence for prediction of output energy and environmental impacts of sugarcane production,” Sci. Tot. Environ., vol. 664, pp. 1005–1019, 2019, https://doi.org/10.1016/j.scitotenv.2019.02.004.Search in Google Scholar PubMed

[9] O. Das, ., “Natural and industrial wastes for sustainable and renewable polymer composites,” Renew. Sustain. Energy Rev., vol. 158, 2022, Art. no. 120054, https://doi.org/10.1016/j.rser.2021.112054.Search in Google Scholar

[10] P. Young, A. Luch, and P. Laux, “Impact of phosphine and of sulfuryl fluoride fumigation on walnut quality,” J. Stored Products Res., vol. 100, 2023, Art. no. 102059, https://doi.org/10.1016/j.jspr.2022.102059.Search in Google Scholar

[11] I. Domingos, J. Ferreira, L. Cruz-Lopes, and B. Esteves, “Liquefaction and chemical composition of walnut shells,” Open Agric., vol. 7, no. 1, pp. 249–256, 2022, https://doi.org/10.1515/opag-2022-0072.Search in Google Scholar

[12] Z. Qin, ., “A sensitive sandwich enzyme-linked immunosorbent assay (sELISA) for the detection of walnut residues in processed food,” J. Food Composit. Anal., vol. 119, 2023, Art. no. 105221, https://doi.org/10.1016/j.jfca.2023.105221.Search in Google Scholar

[13] J. Nicolás-Bermúdez, ., “Characterization of the hierarchical architecture and micromechanical properties of walnut shell (Juglans regia L.),” J. Mech. Behav. Biomed. Mater., vol. 130, 2022, Art. no. 105190, https://doi.org/10.1016/j.jmbbm.2022.105190.Search in Google Scholar PubMed

[14] C. S. G. P. Queirós, ., “Characterization of walnut, almond, and pine nut shells regarding chemical composition and extract composition,” Biomass Convers. Biorefinery, vol. 10, pp. 175–188, 2020, https://doi.org/10.1007/s13399-019-00424-2.Search in Google Scholar

[15] H. Albatrni, H. Qiblawey, and M. J. Al-Marri, “Walnut shell based adsorbents: a review study on preparation, mechanism, and application,” J. Water Process Eng., vol. 45, 2022, Art. no. 102527, https://doi.org/10.1016/j.jwpe.2021.102527.Search in Google Scholar

[16] M. Kizatova, M. Sultanova, A. Baikenov, A. Saduakas, and N. Akzhanov, “Revealing the features of the composition of the walnut shell from the point of view of the possibility of its use in the food industry,” Eastern Eur. J. Enterprise Technol., vol. 1, no. 11, pp. 49–55, 2022, https://doi.org/10.15587/1729-4061.2022.252315.Search in Google Scholar

[17] Ş. Yıldızhan, A. Çalık, M. Özcanlı, and H. Serin, “Bio-composite materials: a short review of recent trends, mechanical and chemical properties, and applications,” Eur. Mech. Sci., vol. 2, no. 3, pp. 83–91, 2018, https://doi.org/10.26701/ems.369005.Search in Google Scholar

[18] T. Singh, S. Tejyan, A. Patnaik, V. Singh, I. Zsoldos, and G. Fekete, “Fabrication of waste bagasse fiber-reinforced epoxy composites: study of physical, mechanical, and erosion properties,” Polym. Compos., vol. 40, no. 9, pp. 3777–3786, 2019, https://doi.org/10.1002/pc.25239.Search in Google Scholar

[19] S. N. Mohd Bakhori, ., “Physical, mechanical and perforation resistance of natural-synthetic fiber interply laminate hybrid composites,” Polymers, vol. 14, no. 7, p. 1322, 2022, https://doi.org/10.3390/polym14071322.Search in Google Scholar PubMed PubMed Central

[20] A. K. J. Al-Shamary, R. Karakuzu, H. Kandas, and O. Ozdemir, “Experimental investigation of the impact behavior of glass/epoxy composite materials with the natural fiber layer,” Mater. Test., vol. 64, no. 6, pp. 780–786, 2022, https://doi.org/10.1515/mt-2021-2133.Search in Google Scholar

[21] R. M. Government, K. A. Ani, T. O. Azeez, and O. D. Onukwuli, “Effects of the chemical treatment of avocado pear wood filler on the properties of LDPE composites,” Mater. Test., vol. 61, no. 12, pp. 1209–1214, 2019, https://doi.org/10.3139/120.111441.Search in Google Scholar

[22] H. Kandas and O. Ozdemir, “Investigation of glass/epoxy laminate composites reinforced with bio-particles under mechanical loading,” Mater. Test., vol. 65, no. 3, pp. 444–452, 2023, https://doi.org/10.1515/mt-2022-0289.Search in Google Scholar

[23] A. Karimah, ., “A review on natural fibers for development of eco-friendly bio-composite: characteristics, and utilizations,” J. Mater. Res. Technol., vol. 13, pp. 2442–2458, 2021, https://doi.org/10.1016/j.jmrt.2021.06.014.Search in Google Scholar

[24] Z. Wang, X. Zhu, and P. J. Deuss, “The effect of ball milling on birch, pine, reed, walnut shell enzymatic hydrolysis recalcitrance and the structure of the isolated residual enzyme lignin,” Ind. Crops Prod., vol. 167, 2021, Art. no. 113493, https://doi.org/10.1016/j.indcrop.2021.113493.Search in Google Scholar

[25] K. Salasinska, M. Barczewski, R. Górny, and A. Kloziński, “Evaluation of highly filled epoxy composites modified with walnut shell waste filler,” Polym. Bull., vol. 75, pp. 2511–2528, 2018, https://doi.org/10.1007/s00289-017-2163-3.Search in Google Scholar

[26] R. Avolio, I. Bonadies, D. Capitani, M. E. Errico, G. Gentile, and M. Avella, “A multitechnique approach to assess the effect of ball milling on cellulose,” Carbohydr. Polym., vol. 87, no. 1, pp. 265–273, 2012, https://doi.org/10.1016/j.carbpol.2011.07.047.Search in Google Scholar PubMed

[27] S. Liu, H. Wang, and H. Wang, “Effect of grinding time on the particle size distribution characteristics of tuff powder,” Mater. Sci., vol. 27, no. 2, pp. 205–209, 2021, https://doi.org/10.5755/j02.ms.23526.Search in Google Scholar

[28] H. Nakamura, H. Kan, H. Takeuchi, and S. Watano, “Effect of stator geometry of impact pulverizer on its grinding performance,” Chem. Eng. Sci., vol. 122, pp. 565–572, 2015, https://doi.org/10.1016/j.ces.2014.10.011.Search in Google Scholar

[29] H. Jung, Y. Lee, and W. Yoon, “Effect of moisture content on the grinding process and powder properties in food: a review,” Processes, vol. 6, no. 6, 2018, Art. no. 69, https://doi.org/10.3390/pr6060069.Search in Google Scholar

[30] S. G. Walde, K. Balaswamy, V. Velu, and D. G. Rao, “Microwave drying and grinding characteristics of wheat (Triticum aestivum),” J. Food Eng., vol. 55, pp. 271–276, 2002, https://doi.org/10.1016/S0260-8774(02)00101-2.Search in Google Scholar

[31] A. Akdoğan and S. Güleç, “Sustainable solid waste management and a research on the analysis of managers’ thoughts and attitudes in respect to solid waste management in municipalities,” Hacettepe Univ. J. Econ. Admin. Sci., vol. 25, no. 1, pp. 39–69, 2007.Search in Google Scholar

[32] G. Özkan, B. Gültekin Subaşı, S. Kamiloğlu Beştepe, and E. Çapanoğlu Güven, “Food sustainability and agricultural waste management,” Çevre İklim ve Sürdürülebilirlik, vol. 23, no. 2, pp. 145–160, 2022.Search in Google Scholar

[33] A. Georganas, ., “Bioactive compounds in food waste: a review on the transformation of food waste to animal feed,” Foods, vol. 9, no. 3, 2020, Art. no. 291, https://doi.org/10.3390/foods9030291.Search in Google Scholar PubMed PubMed Central

[34] E. Güneş and T. Karakaş, “Sustainability approaches in agriculture and food system,” J. Acad. Value Stud., vol. 8, no. 3, pp. 304–316, 2022. https://doi.org/10.29228/javs.63757.Search in Google Scholar

Published Online: 2024-05-22
Published in Print: 2024-08-27

© 2024 Walter de Gruyter GmbH, Berlin/Boston

Articles in the same Issue

  1. Frontmatter
  2. An improved white shark optimizer algorithm used to optimize the structural parameters of the oil pad in the hydrostatic bearing
  3. Microstructure and oxidation of a Ni–Al based intermetallic coating formation on a Monel-400 alloy
  4. Friction, wear, and hardness properties of hybrid vehicle brake pads and effects on brake disc roughness
  5. Development of sinter linings for high-speed trains
  6. Wear resistance optimized by heat treatment of an in-situ TiC strengthened AlCoCrFeNi laser cladding coating
  7. Mechanical analysis of hybrid structured aircraft wing ribs with different geometric gaps
  8. Thermo-mechanical characteristics of spent coffee grounds reinforced bio-composites
  9. Compositional zoning and evolution of symplectite coronas in jadeitite
  10. Effect of niobium addition on the microstructure and wear properties of mechanical alloyed Cu–Al–Ni shape memory alloy
  11. Optimization of electric vehicle design problems using improved electric eel foraging optimization algorithm
  12. Effects of infill pattern and compression axis on the compressive strength of the 3D-printed cubic samples
  13. Microstructure and tribological properties of aluminum matrix composites reinforced with ZnO–hBN nanocomposite particles
  14. Marathon runner algorithm: theory and application in mathematical, mechanical and structural optimization problems
  15. Parameter identification of Yoshida–Uemori combined hardening model by using a variable step size firefly algorithm
  16. Identification of the tip mass parameters in a beam-tip mass system using response surface methodology
  17. Production and characterization of waste walnut shell powder that can be used as a sustainable eco-friendly reinforcement in biocomposites
  18. Anticorrosion performance of a zinc-rich cycloaliphatic epoxy resin coating containing CeO2 nanoparticle
Downloaded on 25.10.2025 from https://www.degruyterbrill.com/document/doi/10.1515/mt-2024-0018/pdf?lang=en
Scroll to top button