Home Technology Effect of austempering treatment on metallurgical structure of Ce inoculated X210Cr12 cold work tool steel
Article
Licensed
Unlicensed Requires Authentication

Effect of austempering treatment on metallurgical structure of Ce inoculated X210Cr12 cold work tool steel

  • Tanju Teker

    Tanju Teker born in Sivas in 1971, works in the University of Sivas Cumhuriyet, Faculty of Technology, Department of Manufacturing Engineering, Sivas, Turkey. He graduated in Metallurgy Education from Gazi University, Ankara, Turkey, in 1997. He received his MSc and PhD degrees from Firat University, Elazig, Turkey in 2004 and 2010, respectively. His research interests are metal coating techniques, casting, fusion, and solid-state welding methods.

    EMAIL logo
    , S. Osman Yilmaz

    S. Osman Yilmaz born in Elazig in 1966, works at the University of Namık Kemal, Faculty of Engineering, Department of Mechanical Engineering, Corlu, Tekirdağ, Turkey. He received his BSc from METU University, Ankara, Faculty of Engineering, Metallurgy and Materials Engineering Department in 1989, his MSc from the Institute of Science and Technology, Metallurgy Department in 1992, and his PhD from the University of Firat, Institute of Science and Technology, Metallurgy Department, Elazig in 1998. He studied metal coating techniques, surface modification, welding, casting, and wear.

    and S. Özmen Eruslu

    S. Özmen Eruslu born in 1977, works at the University of Namık Kemal, Faculty of Engineering, Department of Mechanical Engineering, Corlu, Tekirdağ, Turkey. He graduated in Mechanical Engineering from Süleyman Demirel University, Isparta, Turkey, in 1999. He received his MSc and PhD degrees from Trakya University, Edirne, Turkey and Dokuz Eylül University, İzmir, Turkey in 2002 and 2008, respectively. His research interests are material design and behaviors, finite element analysis, and composite materials.

Published/Copyright: February 21, 2022
Become an author with De Gruyter Brill

Abstract

The effect of austempering treatment on metallurgical structure of X210Cr12 cold work tool steel inoculated with Ce was researched. Microstructural changes, elemental characterizations, and phase formations of the samples were examined by using scanning electron microscopy, energy dispersive spectroscopy, X-ray diffraction, elemental mapping, and microhardness test. Ce inoculation reduced the grain size, and the austenitizing temperature had a huge effect on the austenitizing process. The austenitizing process increased the hardness by reducing the retained austenite, but the degree was dependent on the austenitization temperature. The austempering treatment improved the hardness resistance by depositing more equal carbides composed of nano-sized carbides. High austempering period and increase of austempering temperature decreased the homogeneity and hardness of the microstructure.


Corresponding author: Tanju Teker, Department of Manufacturing Engineering, Faculty of Technology, University of Sivas Cumhuriyet, Sivas, Turkey, E-mail:

About the authors

Tanju Teker

Tanju Teker born in Sivas in 1971, works in the University of Sivas Cumhuriyet, Faculty of Technology, Department of Manufacturing Engineering, Sivas, Turkey. He graduated in Metallurgy Education from Gazi University, Ankara, Turkey, in 1997. He received his MSc and PhD degrees from Firat University, Elazig, Turkey in 2004 and 2010, respectively. His research interests are metal coating techniques, casting, fusion, and solid-state welding methods.

S. Osman Yilmaz

S. Osman Yilmaz born in Elazig in 1966, works at the University of Namık Kemal, Faculty of Engineering, Department of Mechanical Engineering, Corlu, Tekirdağ, Turkey. He received his BSc from METU University, Ankara, Faculty of Engineering, Metallurgy and Materials Engineering Department in 1989, his MSc from the Institute of Science and Technology, Metallurgy Department in 1992, and his PhD from the University of Firat, Institute of Science and Technology, Metallurgy Department, Elazig in 1998. He studied metal coating techniques, surface modification, welding, casting, and wear.

S. Özmen Eruslu

S. Özmen Eruslu born in 1977, works at the University of Namık Kemal, Faculty of Engineering, Department of Mechanical Engineering, Corlu, Tekirdağ, Turkey. He graduated in Mechanical Engineering from Süleyman Demirel University, Isparta, Turkey, in 1999. He received his MSc and PhD degrees from Trakya University, Edirne, Turkey and Dokuz Eylül University, İzmir, Turkey in 2002 and 2008, respectively. His research interests are material design and behaviors, finite element analysis, and composite materials.

Acknowledgement

This work was supported by the Domeks machine and Turaş gas armature company. The authors are grateful to thank the companies for their assistance in conducting the experiments.

  1. Author contributions: All the authors have accepted responsibility for the entire content of this submitted manuscript and approved submission.

  2. Research funding: None declared.

  3. Conflict of interest statement: The authors declare no conflicts of interest regarding this article.

References

[1] A. Molinari, M. Pellizzari, S. Gialanella, G. Straffelini, and K. H. Stiasny, “Effect of deep cryogenic treatment on the mechanical properties of tool steels,” J. Mater. Process. Technol., vol. 118, nos. 1–3, pp. 350–355, 2001, https://doi.org/10.1016/S0924-0136(01)00973-6.Search in Google Scholar

[2] J. Y. Huang, Y. T. Zhu, X. Z. Liao, I. J. Beyerlein, M. A. Bourke, and T. E. Mitchell, “Microstructure of cryogenic treated M2 tool steel,” Mater. Sci. Eng., vol. 339, nos. 1–2, pp. 241–244, 2003, https://doi.org/10.1016/S0921-5093(02)00165-X.Search in Google Scholar

[3] A. Kokosza and J. Pacyna, “Evaluation of retained austenite stability in heat treated cold work tool steel,” J. Mater. Process. Technol., vol. 162, no. 163, pp. 327–331, 2005, https://doi.org/10.1016/j.jmatprotec.2005.02.068.Search in Google Scholar

[4] T. Večko Pirtovšek, G. Kugler, M. Godec, and M. Terčelj, “Microstructural characterization during the hot deformation of 1.17C–11.3Cr–1.48V–2.24W–1.35Mo ledeburitic tool steel,” Mater. Char., vol. 62, no. 2, pp. 189–197, 2011, https://doi.org/10.1016/j.matchar.2010.11.016.Search in Google Scholar

[5] V. Firouzdor, E. Nejati, and F. Khomamizaheh, “Effect of deep cryogenic treatment on wear resistance and tool life of M2 HSS drill,” J. Mater. Process. Technol., vol. 206, nos. 1–3, pp. 467–472, 2008, https://doi.org/10.1016/j.jmatprotec.2007.12.072.Search in Google Scholar

[6] A. Akhbarizadeh, A. M. A. Shafyei, and M. A. Golozar, “Effects of cryogenic treatment on wear behaviour of D6 tool steel,” Mater. Des., vol. 30, no. 8, pp. 3259–3264, 2009, https://doi.org/10.1016/j.matdes.2008.11.016.Search in Google Scholar

[7] N. B. Dhokey and S. Nirbhavane, “Dry sliding wear of cryo-treated multiple tempered D3 tool steel,” J. Mater. Process. Technol., vol. 209, no. 3, pp. 1484–1490, 2009, https://doi.org/10.1016/j.jmatprotec.2008.03.069.Search in Google Scholar

[8] S. S. Grill, J. Singh, R. Sigh, and H. Sigh, “Metallurgical principals of cryogenically treated tool steels – a review on the current state of science,” Int. J. Adv. Manuf. Technol., vol. 54, pp. 59–82, 2011, https://doi.org/10.1007/s00170-010-2935-5.Search in Google Scholar

[9] Ö. M. Murathan, K. Davut, and V. Kilicli, “Effect of austenitizing temperatures on the microstructure and mechanical properties of AISI 9254 steel,” Mater. Test., vol. 63, no. 1, pp. 48–54, 2021, https://doi.org/10.1515/mt-2020-0007.Search in Google Scholar

[10] C. H. Surberg, P. F. Stratton, and K. Lingenhole, “The effect of cryogenic treatment on the properties of AISI D2,” Mater. Manuf. Process., vol. 24, nos 7–8, pp. 863–867, 2009, https://doi.org/10.1080/10426910902917421.Search in Google Scholar

[11] A. Oppenkowski, S. Weber, and W. Theisen, “Evaluation of factors influencing deep cryogenic treatment that affect the properties of tool steels,” J. Mater. Process. Technol., vol. 210, no. 14, pp. 1949–1955, 2010, https://doi.org/10.1016/j.jmatprotec.2010.07.007.Search in Google Scholar

[12] X. Chen and Y. Li, “Fracture toughness improvement of austempered high silicon steel by titanium, vanadium and rare earth elements modification,” Mater. Sci. Eng., vol. 444, nos. 1–2, pp. 298–305, 2007, https://doi.org/10.1016/j.msea.2006.08.113.Search in Google Scholar

[13] Y. Qu, J. Xing, X. Zhi, J. Peng, and H. Fu, “Effect of cerium on the as-casted microstructure of a hypereutectic high chromium cast iron,” Mater. Lett., vol. 62, nos. 17–18, pp. 3024–3027, 2008, https://doi.org/10.1016/j.matlet.2008.01.129.Search in Google Scholar

[14] K. Amini, S. Nategh, and A . Shafyei, “Influence of different cryotreatments on tribological behavior of 80CrMo12 5 cold work tool steel,” Mater. Des., vol. 3, no. 10, pp. 4666–4675, 2010, https://doi.org/10.1016/j.matdes.2010.05.028.Search in Google Scholar

[15] Y. M. Rhyim, S. H. Han, Y. S. Na, and J. H. Lee, “Effect of deep cryogenic treatment on carbide precipitation and mechanical properties of tool steel,” Solid State Phenom., vol. 118, pp. 9–14, 2006, https://doi.org/10.1016/j.matlet.2008.01.129.Search in Google Scholar

[16] D. Das, A. K. Dutta, V. Toppo, and K. K. Ray, “Effect of deep cryogenic treatment on the carbide precipitation and tribological behavior of D2 steel,” Mater. Manuf. Process., vol. 22, no. 4, pp. 474–480, 2007, https://doi.org/10.1080/10426910701235934.Search in Google Scholar

[17] T. Teker, I. S. Dalmış, and R. Yılmaz, “Effect of heat treatment on wear behavior of GX200Cr13Ni6WMoMn,” Mater. Test., vol. 61, no. 5, pp. 441–447, 2019, https://doi.org/10.3139/120.111339.Search in Google Scholar

[18] D. Mohan Lal, S. Renganarayanan, and A. Kalanidhi, “Cryogenic treatments to augment wear resistance of tool and die steels,” Cryogenics, vol. 41, no. 3, pp. 149–155, 2001, https://doi.org/10.1016/S0011-2275(01)00065-0.Search in Google Scholar

[19] K. D. Timmerhaus and R. P. Reed, Cryogenic Engineering, New York, USA, Springer, 2007, pp. 3–37.10.1007/0-387-46896-XSearch in Google Scholar

[20] V. Leskovsek, M. Kalin, and J. Vizintin, “Influence of deep cryogenic treatment on wear resistance of vacuum heat-treated HSS,” Vacuum, vol. 80, no. 6, pp. 507–518, 2006, https://doi.org/10.1016/j.vacuum.2005.08.023.Search in Google Scholar

[21] T. Engelke and A. Esderts, “Analytical strength assessments of austempered ductile iron components,” Mater. Test., vol. 60, no. 10, pp. 940–944, 2018, https://doi.org/10.3139/120.111235.Search in Google Scholar

Published Online: 2022-02-21
Published in Print: 2022-01-27

© 2021 Walter de Gruyter GmbH, Berlin/Boston

Downloaded on 1.1.2026 from https://www.degruyterbrill.com/document/doi/10.1515/mt-2021-2014/pdf
Scroll to top button