Preparation and characterization of dried cellulose nanofibrils

Jianping Ni; Chen Gong; Zhenghua Su; Chao Tian

doi:10.1515/ijmr-2020-8119

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Preparation and characterization of dried cellulose nanofibrils

Jianping Ni , Chen Gong , Zhenghua Su und Chao Tian

Veröffentlicht/Copyright: 18. August 2021

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Aus der Zeitschrift International Journal of Materials Research Band 112 Heft 8

Abstract

One of the main manufacturing challenges is to obtain dried cellulose nanofibrils (CNFs) so that they can be cost effectively transported to customers. This work presents a study on using two methods of drying: freeze drying and spray drying; these dried CNFs were then characterized. The dried CNFs from either freeze drying or spray drying could not recover their original state after simple re-dispersion in water. Compared to spray dried CNFs, the microstructure of the freeze dried CNFs remained in a better shape. This was because the packing of nanofibrils as a result of freeze drying was not as tight as that from spray drying. It was demonstrated by the lower final mass residue and crystallinity of the freeze-dried CNFs, which led to better re-dispersion in water. X-ray diffractometry proved the occurrence of aggregation/hornification of the dried CNFs with increased crystallinity. Time-dependent sedimentation confirmed that the dried CNFs were incapable of forming stable water-re-dispersible suspensions.

Keywords: Cellulose nanofibrils; Properties; Freeze drying; Spray drying

Chao Tian, Ph D China National Pulp and Paper Research Institute Co., LTD Building 2, No. 4, Qiyang Road Chaoyang District Beijing, 100102 P. R. China Tel.: +86-10-64778086 Fax: +86-10-64778084 Web: www.cnppri.com

Funding statement: The authors gratefully acknowledge financial support from Demonstration of Hemicellulose Extraction Technology from Pulping Hydrolysate and Xylose Preparation (2017YFB0307904), the team project of Pulp and Environment Technology R&D Center at China National Pulp and Paper Research Institute Co., Ltd.

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Received: 2020-10-16

Accepted: 2021-04-21

Published Online: 2021-08-18

Published in Print: 2021-08-31

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https://doi.org/10.1515/ijmr-2020-8119

Schlagwörter für diesen Artikel

Cellulose nanofibrils; Properties; Freeze drying; Spray drying