Abstract
A continuous S2 silicide ([Ti,Zr]xSiy) segregation layer was found in the fibre matrix interface of SCS6-SiC/Ti-5.8Al-4Sn-3.5Zr-0.7Nb-0.5Mo-0.35Si (IMI834) composites (composition in wt.%). The S2 layer separates completely the titanium matrix from the reaction layer. It was shown that the S2 layer stabilises the interface during thermal treatment. The thermal stability of composites was tested in which artificial coatings were introduced into the interface. For the artificial coatings a composition and structure of the S2 silicides were aspired. The interface of the composites was investigated with analytical transmission electron microscope in the as-processed condition and annealed at 700 °C for 3 000 h and at 800 °C for 1000 h. The coatings of the same composition and structure can be introduced into the interface of SiC-SCS6/IMI834 composites as those of the S2 silicide obtained by self-segregation. The composites with the artificial coatings have a similar interface stability at 700 °C as those obtained by self-segregation.
The authors greatly thank Manfred Klaukien (DLR) for the TEM preparation of the composites.
References
1 Dudek, H.J.; Borath, R.; Leucht, R.; Kaysser, W.A.: J. Mater. Sci. 32 (1997) 5355.10.1023/A:1018623012948Search in Google Scholar
2 Sridhar, G.; Sarma, S.S.: Met. Trans. A 19 (1988) 3025.10.1007/BF02647729Search in Google Scholar
3 Ghosal, P.; Prasad, R.; Ramachandra, C.: Met. Trans. A 26(1995) 2751.10.1007/BF02669431Search in Google Scholar
4 Flower, H.M.; Swann, P.R.; West, D.R.F.: Met. Trans. 2 (1971) 3289.10.1007/BF02811609Search in Google Scholar
5 Ramachandra, C.; Singh, V.: Met. Trans. A 19 (1988) 389.10.1007/BF02652553Search in Google Scholar
6 Ramachandra, C.; Singh, A.K.; Sarma, G.M.K.: Met. Trans. A 24 (1993) 1273.10.1007/BF02668196Search in Google Scholar
7 Salpadoru, N.H.; Flower, H.M.: Metall. Trans. A 26 (1995) 243.10.1007/BF02664663Search in Google Scholar
8 Leucht, R.; Dudek, H.J.: Mater. Sci. Eng. A 188 (1994) 201.10.1016/0921-5093(94)90373-5Search in Google Scholar
9 Leucht, R.: Dudek, H.J.: Weber, K.: A. Werner, Z. Metallkd. 87 (1996) 424.10.1515/ijmr-1996-870515Search in Google Scholar
10 Yang, Y.Q.; Dudek, H.J.; Kumpfert, J.: Composites A 29 (1998) 1235.10.1016/S1359-835X(97)00127-9Search in Google Scholar
11 Dudek, H.J.; Weber, K.: submitted to J. Mater. Sci. Lett.Search in Google Scholar
12 Dudek, H.J.; Weber, K.: submitted to Scripta Metall. Mater. Lett.Search in Google Scholar
© 2002 Carl Hanser Verlag, München
Articles in the same Issue
- Frontmatter
- Aufsätze/Articles
- Dilatometric study of the effect of soluble boron on the continuous and isothermal austenite decomposition in 0.15C–1.6Mn steel
- Use of duplex microstructures in steel for estimation of plastic deformation in high-speed machining chips
- Stability of strengthened niobium alloys in long-term high-temperature loading conditions
- Effect of rare-earth metals on the hot strength of HSLA steels
- Wear behaviour of Ni–Cr–Mo–V steel under dry sliding
- Thermodynamic calculation of the phase diagram of the Co–Nb–Ta system
- Peritectic equilibrium in Fe-Co alloys
- A thermodynamic description of the B–Co system: modeling and experiment
- Thermodynamic interpretation of thermoelectric phenomena
- Unit cell volumes of the silicon- and germanium-containing solid solutions based on the 3d bcc transition metals
- Artificial silicide barrier coatings in titanium matrix composites
- Notifications/Mitteilungen
- Personal/Personelles
- DGM Training/DGM Fortbildung
- Conferences/Konferenzen
Articles in the same Issue
- Frontmatter
- Aufsätze/Articles
- Dilatometric study of the effect of soluble boron on the continuous and isothermal austenite decomposition in 0.15C–1.6Mn steel
- Use of duplex microstructures in steel for estimation of plastic deformation in high-speed machining chips
- Stability of strengthened niobium alloys in long-term high-temperature loading conditions
- Effect of rare-earth metals on the hot strength of HSLA steels
- Wear behaviour of Ni–Cr–Mo–V steel under dry sliding
- Thermodynamic calculation of the phase diagram of the Co–Nb–Ta system
- Peritectic equilibrium in Fe-Co alloys
- A thermodynamic description of the B–Co system: modeling and experiment
- Thermodynamic interpretation of thermoelectric phenomena
- Unit cell volumes of the silicon- and germanium-containing solid solutions based on the 3d bcc transition metals
- Artificial silicide barrier coatings in titanium matrix composites
- Notifications/Mitteilungen
- Personal/Personelles
- DGM Training/DGM Fortbildung
- Conferences/Konferenzen