Study of the textural properties of non-ionic resins and their influence on polyphenol adsorption and desorption
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Nils L. Huamán-Castilla
,
Olivia M. Luque-Vilca
,
Gregorio Arroyo-Japura
,
Marcos L. Quispe-Pérez
,
Nilton C. León-Calvo
,
José R. Pérez-Correa
Abstract
Macroporous resins are employed for the purification of polyphenolic extracts. However, the relationship between the adsorption and desorption and the textural properties remains unexplored. Thus, we evaluated the textural properties of HP-20, XAD-16 and SP-825 resins and their impact on adsorption and desorption of specific polyphenols like gallic acid, epigallocatechin, and procyanidin B2. The HP-20 resin exhibited a type II isotherm with macroporous structure, while XAD-16 and SP-825 resins displayed type IV isotherms, typically associated with mesoporous materials. The HP-20 resin demonstrated superior adsorption capacity and rupture points for epigallocatechin (2.37 mg/g, 124 min) and procyanidin B2 (1.29 mg/g, 136 min) compared to SP-825 and XAD-16. Contrary, the SP-825 resin exhibited the highest adsorption capacity (5.34 mg/g) and rupture point (68 min) for gallic acid. However, the desorption was more efficient when HP-20 resin was used for all specific polyphenols. Therefore, for an efficient purification process is necessary to consider the chemical structure of the polyphenol and the textural properties.
Acknowledgments
To Professor Nestor Escalona (PhD) for his support in the analysis of the textural properties.
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Research ethics: Not applicable.
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Author contributions: Nils L. Huamán-Castilla: project administration, investigation, methodology, analysis and writing – review final; José R. Perez Correa and María S. Mariotti Celis: methodology, supervision during the data acquisition process and original draft preparation; Nestor Escalona: analysis of textural properties of the resins investigated; Olivia M. Luque-Vilca: validation and formal analysis, as well as writing – original draft preparation; Gregorio Arroyo-Japura: writing – original draft preparation and editing; Marcos L. Quispe-Pérez: formal analysis, and writing – original draft preparation; Nilton C. León-Calvo: statistic analysis and writing – original draft preparation.
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Competing interests: The authors state no conflict of interest.
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Research funding: None declared.
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Data availability: Not applicable.
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Artikel in diesem Heft
- Frontmatter
- Critical Review
- Preparation of solution blow spinning nanofibers and its application in the food field: a review
- Articles
- Structural identification, stability and combination mechanism of calcium-chelating wheat gluten peptides
- Increased reactive carboxyl and free alfa-amino groups from fish type I collagen peptides by Alcalase® hydrolysis exhibit higher antibacterial and antioxidant activities
- Comparative study on enzyme activity, microstructure, drying kinetics, and physicochemical properties of apple slices affected by microwave and steam blanching
- Acerola byproducts microencapsulated by spray and freeze-drying: the effect of carrier agent and drying method on the production of bioactive powder
- Study of the textural properties of non-ionic resins and their influence on polyphenol adsorption and desorption
- Fabrication of palm carotene-based emulsion stabilized by rice protein isolate-flaxseed gum complex
- Physicochemical properties, the digestible and resistant starch content of chestnut flour with different particle sizes
Artikel in diesem Heft
- Frontmatter
- Critical Review
- Preparation of solution blow spinning nanofibers and its application in the food field: a review
- Articles
- Structural identification, stability and combination mechanism of calcium-chelating wheat gluten peptides
- Increased reactive carboxyl and free alfa-amino groups from fish type I collagen peptides by Alcalase® hydrolysis exhibit higher antibacterial and antioxidant activities
- Comparative study on enzyme activity, microstructure, drying kinetics, and physicochemical properties of apple slices affected by microwave and steam blanching
- Acerola byproducts microencapsulated by spray and freeze-drying: the effect of carrier agent and drying method on the production of bioactive powder
- Study of the textural properties of non-ionic resins and their influence on polyphenol adsorption and desorption
- Fabrication of palm carotene-based emulsion stabilized by rice protein isolate-flaxseed gum complex
- Physicochemical properties, the digestible and resistant starch content of chestnut flour with different particle sizes
