Startseite Hetero-structured Iron Molybdate Nanoparticles: Synthesis, Characterization and Photocatalytic Application
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Hetero-structured Iron Molybdate Nanoparticles: Synthesis, Characterization and Photocatalytic Application

  • Jan Nisar , Sohaib Hassan , Muhammad Iftikhar Khan , Munawar Iqbal , Arif Nazir EMAIL logo , Ahsan Sharif und Ejaz Ahmed
Veröffentlicht/Copyright: 23. Januar 2020
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Abstract

This study focuses on the synthesis of iron molybdate [Fe2(MoO4)3] nanoparticles (NPs) using simple co-precipitation process. The catalyst synthesized was characterized by advanced instrumental techniques such as XRD, SEM, EDX, TGA and FTIR, which confirmed the successful synthesis of NPs. Organic compound Rhodamine B (Rh. B) dye was selected for photo-degradation due to its complex structure and carcinogenic nature. Results exhibited that at neutral pH, the synthesized catalyst is highly effective for the degradation of Rh. B. For 20 mg/L initial concentration with an initial pH of 6.7, the degradation efficiency of Rh. B reaches 98  % within 180 min. Furthermore, the solution pH (1 to 11) affects the catalytic activity. This indicates that at neutral and/or alkaline pH, the usage of iron molybdate overwhelms the efficiency of Fenton-like reaction. It has been observed that Fe2(MoO4)3 showed excellent stability as after recycling it for 9 times its performance remained effective. Based on these data, the synthesized catalyst could be conveniently employed for degradation of toxic pollutants.

  1. Conflict of Interest: The authors declare that they have no conflict of interest.

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Received: 2019-06-26
Revised: 2019-10-12
Accepted: 2019-10-18
Published Online: 2020-01-23

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