Home Experimental Study on Atomizing and Reaction Performance of Pressure Swirl Nozzles in Ethoxylation Reactor
Article
Licensed
Unlicensed Requires Authentication

Experimental Study on Atomizing and Reaction Performance of Pressure Swirl Nozzles in Ethoxylation Reactor

  • Zhongjing Shi , Xuesheng Wang EMAIL logo , Qinzhu Chen , Yuanyuan Xiong , Shuo Chen and Xiangyu Meng
Published/Copyright: April 16, 2016

Abstract

Spray Tower Loop Reactors is one of the most advanced ethoxylation reactors in the world. The special pressure swirl nozzles are the core component and important for production efficiency and product quality. A test rig was established, which was divided into four parts: spray system, laser measurement system, photographic system and flux distribution test system. An experimental study on the atomizing performances was conducted, including discharge coefficient, spray cone angle, spray flux distribution, Sauter mean droplets size and droplets size distribution. According to the measurement data, the correlation of volume flow rate, discharge coefficient, spray cone angle and Sauter mean droplets size versus pressure drop were respectively gained. The spray flow distributions of all measured nozzles are classified as a unimodal、bimodal and trimodal distribution due to the different structure. And the experimental Probability Density Function (PDF) of the droplets size was gained by a split-type spray laser droplets size analyzer and compared with five empirical distributions. The log-hyperbolic distribution has a most agreement with the measured PDF. At same time, reaction performance of the special nozzles was measured in the industrial STLR ethoxylation reactor. It is indicated that Sauter mean diameter determines the number of EO and the width of droplets size distribution determines the width of the molecular weight distributions. The present paper exhibits the measurement way and outcomes of spray characteristics of the nozzles in ethoxylation reaction and it is instructive for the optimization design of SPLT ethoxylation reaction.

References

1. Babinsky, E., Sojka, P.E., 2002. Modeling Drop Size Distributions. Prog. Energ. Combust. 28, 303–329.10.1016/S0360-1285(02)00004-7Search in Google Scholar

2. Bhatia, J.C., Dominick, J., Durst, F., 1988. Phase-Doppler-Anemometry and the Log-Hyperbolic Distribution Applied to Liquid Sprays. Part. Part. Syst. Char. 5, 153–164.10.1002/ppsc.19880050401Search in Google Scholar

3. Bhatia, J.C., Durst, F., 1989. Comparative Study of Some Probability Distributions Applied to Liquid Sprays. Part. Part. Syst. Char. 6, 151–162.10.1002/ppsc.19890060126Search in Google Scholar

4. Dimiccoli, A., Di Serio, M., Santacesaria, E., 2000. Mass Transfer and Kinetics in Spray-Tower-Loop Absorbers and Reactors. Ind. Eng. Chem. Res. 39, 4082–4093.10.1021/ie000137ySearch in Google Scholar

5. Di Serio, M., Tesser R., Santacesaria, E., 2005. Comparison of Different Reactor Types Used in the Manufacture of Ethoxylated, Propoxylated Products. Ind. Eng. Chem. Res. 44, 9482–9489.10.1021/ie0502234Search in Google Scholar

6. Duan, Y., Han, D., Li, P., Wang, C., Lin, H., Huang, Z., 2015. Experimental Study on Injection and Macroscopic Spray Characteristics of Ethyl Oleate, Jet Fuel, and Their Blend on a Diesel Engine Common Rail System. Atomization Sprays 25, 777–793.10.1615/AtomizSpr.2015011145Search in Google Scholar

7. Gong, J. S., Fu, W. B., 2007. The Experimental Study on the Flow Characteristics for a Swirling Gas-Liquid Spray Atomizer. Appl. Therm. Eng. 27, 2886–2892.10.1016/j.applthermaleng.2007.04.006Search in Google Scholar

8. Guo, L., Yan, Y.Y., Maltson, J.D., 2011. Numerical Study on Discharge Coefficients of a Jet in Crossflow. Comput. Fluids 49, 323–332.10.1016/j.compfluid.2011.06.022Search in Google Scholar

9. Kim, W.T., Mitra, S.K., Li, X., Prociw, L.A., Hu, T.C.J., 2003. A Predictive Model for the Initial Droplet Size and Velocity Distributions in Sprays and Comparison with Experiments. Part. Part. Syst. Char. 20, 135–149.10.1002/ppsc.200390011Search in Google Scholar

10. Lan, Z., Zhu, D., Tian, W., Su, G., Qiu, S., 2014. Experimental Study on Spray Characteristics of Pressure-Swirl Nozzles in Pressurizer. Ann. Nucl. Energy. 63, 215–227.10.1016/j.anucene.2013.07.048Search in Google Scholar

11. Salzano, E., Di Serio, M., Santacesaria, E., 2007. The Role of Recirculation Loop on the Risk of Ethoxylation Processes. J. Loss. Prevent. Proc. 20, 238–250.10.1016/j.jlp.2007.03.016Search in Google Scholar

12. Santacesaria, E., Di Serio, M., Tesser, R., 2005. Gas-Liquid and Gas-Liquid-Solid Reaction Performed in Spray Tower Loop Reactors. Ind. Eng. Chem. Res 44, 9461–9472.10.1021/ie050222bSearch in Google Scholar

13. Santacesaria, E., Di Serio, M., Lisi, L., 1990. Kinetics of Nonylphenol Polyethoxylation Catalyzed by Potassium Hydroxide. Ind. Eng. Chem. Res. 29, 719–725.10.1021/ie00101a002Search in Google Scholar

14. Santacesaria, E., Di Serio, M., Iengo P., 1999. Mass Transfer and Kinetics in Ethoxylation Spray Tower Loop Reactors. Chem. Eng. Sci. 54, 1499–1504.10.1016/S0009-2509(99)00042-1Search in Google Scholar

15. Tratnig, A., Brenn, G., 2010. Drop Size Spectra in Sprays From Pressure-Swirl Atomizers. Int. J. Multiphase Flow 36, 349–363.10.1016/j.ijmultiphaseflow.2010.01.008Search in Google Scholar

16. Vijay, G.A., Moorthi, N.S.V., Manivannan, A., 2015. Internal and External Flow Characteristics of Swirl Atomizers: A Review. Atomization Sprays 25, 153–188.10.1615/AtomizSpr.2014010219Search in Google Scholar

17. Weber, C., 1931. Zum Zerfall eines Flüssigkeitsstrahles. ZAMM-J. Appl. Math. Mech. 11, 136–154.10.1002/zamm.19310110207Search in Google Scholar

18. Yan, Y., Zhang, L., Pan, W., Pu, G., 2014. Experimental Investigation of Atomizing Performance of Low Pressure Swirl Nozzle. Adv. Mech. Eng. 6, 1–1010.1155/2014/782064Search in Google Scholar

Published Online: 2016-4-16
Published in Print: 2016-10-1

©2016 by De Gruyter

Articles in the same Issue

  1. Frontmatter
  2. Catalytic Activity of Bimetallic Cu-Ag/MgO-SiO2 Toward the Conversion of Ethanol to 1,3-Butadiene
  3. Heat Transfer Studies in Ejector-induced Downflow Bubble Column
  4. Experimental Study on Atomizing and Reaction Performance of Pressure Swirl Nozzles in Ethoxylation Reactor
  5. Study of the Hydrodynamics and Mass Transfer Coefficient in a 2D Mimicked FT Slurry Bubble Columns for Alternative Clean Energy and Chemical Production
  6. Simultaneous Removal of Organic and Inorganic Pollutants From Landfill Leachate Using Sea Mango Derived Activated Carbon via Microwave Induced Activation
  7. Computational Fluid Dynamics Simulations of Lean Premixed Methane-Air Flame in a Micro-Channel Reactor Using Different Chemical Kinetics
  8. Membrane Aerated Biofilm Reactors for Thermomechanical Pulping Pressate Treatment
  9. Mixing of Shear Thinning Fluids in Cylindrical Tanks: Effect of the Impeller Blade Design and Operating Conditions
  10. Influence of Support Structural Characteristics on Long-term Performance of Pd-Ag/α-Al2O3 Catalyst for Tail-end Acetylene Selective Hydrogenation
  11. Investigation of Key Factors and Their Interactions in MTO Reaction by Statistical Design of Experiments
  12. Hydrogen Production via Glycerol Reforming over Pt/SiO2 Nanocatalyst in a Spiral-Shaped Microchannel Reactor
  13. Experimental Design-Assisted Investigation of Light Olefins Production Over Ceria-Altered HZSM-5 Catalysts by Naphtha Catalytic Steam Cracking
  14. Investigation of α-Amylase Production with Bacillus amyloliquefaciens in a Cocurrent Downflow Contacting Reactor
  15. Gaseous Hydrocarbon Synfuels from Renewable Electricity via H2/CO2-Flexibility of Fixed-Bed Catalytic Reactors
  16. Natural Convective Flow Analysis For Nanofluids With Reynold,s Model of Viscosity
Downloaded on 16.11.2025 from https://www.degruyterbrill.com/document/doi/10.1515/ijcre-2015-0148/html
Scroll to top button