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The crystal structure of lintisite, Na3LiTi2[Si2O6]2O2 · 2H2O, a new titanosilicate from Lovozero (USSR)
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August 25, 2010
Abstract
Lintisite is a new titanosilicate with ideal chemical composition Na3LiTi2Si4O14 · 2H2O, found at Lovozero, Kola peninsula, USSR. The mineral is monoclinic, space group C2/c, with a = 28.583(4), b = 8.600(1), c = 5.219(1) Å, β = 91.03(2)°. The crystal structure of lintisite has been refined to R = 0.033, Rw = 0.028 for 1095 reflections collected with MoKα radiation. The structure is formed by pyroxene-like chains of [SiO4] tetrahedra, chains of edge-sharing [TiO6] and [Na(O, H2O)6] octahedra, columns of edge-sharing [LiO4] tetrahedra, and distorted [NaO8] cubes. The modular relationships among lintisite, vinogradovite and ramsayite are discussed. Finally the thermal behaviour of lintisite is explained in the light of the structural results.
Published Online: 2010-08-25
Published in Print: 1990
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Articles in the same Issue
- The solid phases of deuterium sulphide by powder neutron diffraction
- Crystal and molecular structure of a manganese complex of trans-1,2-diaminocyclohexane-N,N,N′,N′-tetraacetic acid (CDTA): Mn4(CDTA)2(H2O)9(CH3COCH3)0.5 · Evidence for a Mn7(CDTA)4(H2O)8 unit
- X-ray and electron microscopic determination of Debye characteristic temperature, stacking fault energy and other microstructural parameters in zinc telluride films
- A simple formula for the morphological axial ratio and for indexing
- A neutron powder diffraction study of the β to γ phase transformation in NaFeO2
- Neutron diffraction study of Sr(BrO3)2 · H2O: Statistical tests of intensity variances, refinement including weak and negative intensities
- Crystal structure of N-(1-ethylcarbamoyl-tetrazol-5-yl)-O-(4-tolyl)-isourea
- Analysis of the distribution of impurities in crystals by anomalous X-ray scattering
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