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Synthesis and X-ray structure of trimethyl[2,4,6-tri(1,1-dimethylethyl)benzene] 1,3,5-tricarboxylate

Published/Copyright: August 25, 2010
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Zeitschrift für Kristallographie
From the journal Zeitschrift für Kristallographie Volume 193 Issue 1-2

Abstract

The crystal structure of the fully substituted benzene compound, trimethyl-[2,4,6-tri(1,1-dimethylethyl)benzene] 1,3,5-tricarboxylate C24H36O6 has been determined at 298 K and refined to R = 0.054 for 2201 observed reflections. Crystals are monoclinic, space group P21/n with Z = 4 in a cell of dimensions a = 10.910(4), b = 22.186(8), c = 10.518(3) Å and β = 115.58(2)°. The benzene ring is nonplanar while the angles about the ring are also distorted, [mean 122.1(3)° and 116.0(3)° about the ester and t-butyl groups respectively].

Published Online: 2010-08-25
Published in Print: 1990

Articles in the same Issue

  1. The solid phases of deuterium sulphide by powder neutron diffraction
  2. Crystal and molecular structure of a manganese complex of trans-1,2-diaminocyclohexane-N,N,N′,N′-tetraacetic acid (CDTA): Mn4(CDTA)2(H2O)9(CH3COCH3)0.5 · Evidence for a Mn7(CDTA)4(H2O)8 unit
  3. X-ray and electron microscopic determination of Debye characteristic temperature, stacking fault energy and other microstructural parameters in zinc telluride films
  4. A simple formula for the morphological axial ratio and for indexing
  5. A neutron powder diffraction study of the β to γ phase transformation in NaFeO2
  6. Neutron diffraction study of Sr(BrO3)2 · H2O: Statistical tests of intensity variances, refinement including weak and negative intensities
  7. Crystal structure of N-(1-ethylcarbamoyl-tetrazol-5-yl)-O-(4-tolyl)-isourea
  8. Analysis of the distribution of impurities in crystals by anomalous X-ray scattering
  9. Crystal structure and spectra of Trichloro-p-chlorobenzoyl-2-furaldehydohydrazono bismuth(III)
  10. Polarity determination in (001)-oriented AIII – Bv compound semiconductors by the Kossel technique and chemical etching
  11. Crystal and molecular structure of 3-nitro-4-hydroxy-phenylalanine nitrate
  12. The crystal structure of lintisite, Na3LiTi2[Si2O6]2O2 · 2H2O, a new titanosilicate from Lovozero (USSR)
  13. Synthesis and X-ray structure of trimethyl[2,4,6-tri(1,1-dimethylethyl)benzene] 1,3,5-tricarboxylate
  14. Crystal growth and structure determination of potassium zirconium phosphate K2Zr(PO4)2
https://doi.org/10.1524/zkri.1990.193.1-2.149

Articles in the same Issue

  1. The solid phases of deuterium sulphide by powder neutron diffraction
  2. Crystal and molecular structure of a manganese complex of trans-1,2-diaminocyclohexane-N,N,N′,N′-tetraacetic acid (CDTA): Mn4(CDTA)2(H2O)9(CH3COCH3)0.5 · Evidence for a Mn7(CDTA)4(H2O)8 unit
  3. X-ray and electron microscopic determination of Debye characteristic temperature, stacking fault energy and other microstructural parameters in zinc telluride films
  4. A simple formula for the morphological axial ratio and for indexing
  5. A neutron powder diffraction study of the β to γ phase transformation in NaFeO2
  6. Neutron diffraction study of Sr(BrO3)2 · H2O: Statistical tests of intensity variances, refinement including weak and negative intensities
  7. Crystal structure of N-(1-ethylcarbamoyl-tetrazol-5-yl)-O-(4-tolyl)-isourea
  8. Analysis of the distribution of impurities in crystals by anomalous X-ray scattering
  9. Crystal structure and spectra of Trichloro-p-chlorobenzoyl-2-furaldehydohydrazono bismuth(III)
  10. Polarity determination in (001)-oriented AIII – Bv compound semiconductors by the Kossel technique and chemical etching
  11. Crystal and molecular structure of 3-nitro-4-hydroxy-phenylalanine nitrate
  12. The crystal structure of lintisite, Na3LiTi2[Si2O6]2O2 · 2H2O, a new titanosilicate from Lovozero (USSR)
  13. Synthesis and X-ray structure of trimethyl[2,4,6-tri(1,1-dimethylethyl)benzene] 1,3,5-tricarboxylate
  14. Crystal growth and structure determination of potassium zirconium phosphate K2Zr(PO4)2
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