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Reaction of N-Methylimidazole and Dimethyl Acetylenedicarboxylate in the Presence of N-Phenyl Carbamate under Solvent-free Conditions
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June 2, 2014
An efficient synthesis of 1,2,3-functionalized imidazoles and dimethyl-2-[(alkoxycarbonyl)- anilino]-2-butenedioate derivatives via one-pot reactions between N-methylimidazole, dimethyl acetylenedicarboxylate and N-phenylcarbamates under solvent-free conditions is described. The mild reaction conditions and good yields exhibit the synthetic advantage of this method.
Graphical Abstract
Reaction of N-Methylimidazole and Dimethyl Acetylenedicarboxylate in the Presence of N-Phenyl Carbamate under Solvent-free Conditions
Received: 2013-11-28
Published Online: 2014-6-2
Published in Print: 2014-4-1
© 1946 – 2014: Verlag der Zeitschrift für Naturforschung
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Keywords for this article
N-Methylimidazole;
Solvent-free;
N-Phenylcarbamate 1,2,3-Functionalized Imidazoles
Articles in the same Issue
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- Strontium-Metallide im Bereich des Schnitts SrIn4 – SrHg4 / Strontium Metallides along the Section SrIn4 – SrHg4
- CeNi1-xSb1+yBi1-y Phases with ZrCuSiAs-type and CeNi1.26Sb2 with CaBe2Ge2-type Structure
- Synthesis and Crystal Structure of Pd5InSe
- Syntheses, Structures and Properties of a Cobalt(II) and a Cadmium(II) Complex Based on 1-((Benzotriazol-1-yl)methyl)-1H-1,3-imidazole and 1,3-Benzenedicarboxylate Ligands
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