The Effect of Bead Vacuum on Slot Die Coating
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H.-M. Chang
, C.-C. Lee and T.-J. Liu
Abstract
The effect of bead vacuum on the minimum wet thickness obtained on horizontal and vertical slot die coatings was experimentally examined using a flow visualization technique. The commercial software package FLOW3D was used to simulate the two-dimensional coating flow. Macroscopic material balances were applied to estimate the effect of bead vacuum. Applying vacuum on the coating bead was found to reduce the minimum wet thickness and increase the maximum coating speed, with the effect on horizontal slot die coating being more pronounced. Visual observations revealed that with increasing vacuum, the upstream meniscus against the moving web was pulled back significantly for a low-viscosity solution, and the dynamic contact angle was reduced for a high-viscosity solution. The observed upstream wetting length for a low-viscosity solution subject to bead vacuum was consistent with the prediction using macroscopic balances. The sizes of coating beads predicted by FLOW3D were generally larger than those observed from flow visualization. Coating failures caused by high bead vacuum could be predicted with the aid of numerical simulations.
References
Beguin, A. E., U.S. Patent 2681694 (1954)Search in Google Scholar
Brethour, J., “Simulation of Viscoelastic Coating Flows with a Volume-of-fluid Technique”, Proceedings of the 6th European Coating Symposium (2005)Search in Google Scholar
Brown, O. D., Maier, G. W., U.S. Patent 5639305 (1997)Search in Google Scholar
Carvalho, M. S., Kheshgi, H. S., “Low-Flow Limit in Slot Coating: Theory and Experiments”, AIChE J., 46, 1907–1917(2000)10.1002/aic.690461003Search in Google Scholar
Chang, H. M., et al., “Comparison of Vertical and Horizontal Slot Die Coatings”, Polym. Eng. Sci., 47, 1927–1936(2007a)10.1002/pen.20910Search in Google Scholar
Chang, Y. R., et al., “Three Minimum Wet Thickness Regions of Slot Die Coating”, J. Colloid Interface Sci., 308, 222–230(2007b)10.1016/j.jcis.2006.11.054Search in Google Scholar
Feng, J. Q., “Computational Analysis of Slot Coating on a Tensioned Web”, AIChE., 44, 2137–2143(1998)10.1002/aic.690441002Search in Google Scholar
Gutoff, E. B., CohenE.D.: Coating and Drying Defects, 2nd Edition, Wiley Interscience, New Jersey(2006)10.1002/0470044136Search in Google Scholar
Gutoff, E. B., Kendrick, C. E., “Low Flow Limits of Coatability on a Slide Coater”, AIChE J., 33, 141–145(1987)10.1002/aic.690330116Search in Google Scholar
Higgins, B. G., Scriven, L. E., “Capillary Pressure and Viscous Pressure Drop Set bounds on Coating Bead Operability”, Chem. Eng. Sci., 35, 673–682(1980)10.1016/0009-2509(80)80018-2Search in Google Scholar
Hirt, C. W., Nicols, B. D., “Volume of Fluid (VOF) Method for the Dynamics of Free Boundaries”, J. Comp. Phys., 39, 201–225(1981)10.1016/0021-9991(81)90145-5Search in Google Scholar
Hirt, C. W., et al., “Simulation of Transient and Three-Dimensional Coating Flows Using a Volume-of-Fluid Technique”, Proceedings of 50th Annual Conference of the Society for Imaging and Science Technology (1997)Search in Google Scholar
Hirt, C. W., “Direct Computation of Dynamic Contact Angles and Contact Lines”, ECC99 Coating Conference (1999)Search in Google Scholar
Lee, K. Y., et al., “Minimum Wet Thickness in Extrusion Slot Coating”, Chem. Eng. Sci., 47, 1703–1713(1992)10.1016/0009-2509(92)85018-7Search in Google Scholar
Lin, F. H., et al., “Experimental Study on Tensioned-Web Slot Coating”, Polym. Eng. Sci., 47, 841–851(2007)10.1002/pen.20764Search in Google Scholar
Lu, S. Y., et al., “Coating Window for Double Layer Extrusion Slot Coating of Poly(Vinyl-Alcohol) Solutions”, Polym. Eng. Sci., 41, 1823–1829(2001)10.1002/pen.10879Search in Google Scholar
Ruschak, K. J., “Low Flow in a Pre-Metered Coating Device”, Chem. Eng. Sci., 31, 1057–1060(1976)10.1016/0009-2509(76)87026-1Search in Google Scholar
Shibata, N., Sato, T., U.S. Patent 5108795 (1992)Search in Google Scholar
Takahashi, S., Shibata, N., U.S. Patent 5202164 (1993)Search in Google Scholar
Tanwar, J., et al., “Design Principles of Integrated Vacuum Slot Arrangement”, AIChE, 53, 572–578(2007)10.1002/aic.11112Search in Google Scholar
© 2009, Carl Hanser Verlag, Munich
Articles in the same Issue
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- Modeling the Temperature Development of Wall-slipping Polymers in Single-screw Channels
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Articles in the same Issue
- Contents
- Contents
- Regular Contributed Articles
- Modeling the Temperature Development of Wall-slipping Polymers in Single-screw Channels
- A Novel Dilatometer for PVT Measurements of Polymers at High Cooling – and Shear Rates
- Analysis of Heat Transfer in PVC Profiles during the Extrusion Calibration/Cooling Step
- Study on the Bleeding Mechanism of Slip Agents in a Polypropylene Film using Molecular Dynamics
- A Direct 3D Numerical Simulation Code for Extrusion and Mixing Processes
- The Resarch for Asphalt Modified with Phosphorus Trichloride/SBS
- The Effect of Bead Vacuum on Slot Die Coating
- Predicting the Yield Stress of Polymer Glasses Directly from Processing Conditions: Application to Miscible Systems
- Numerical Simulation of a Thermoviscoelastic Frictional Problem with Application to the Hot-Embossing Process for Manufacturing of Microcomponents
- A Design to Study Flow Induced Crystallization in a Multipass Rheometer
- Modeling of Melt Conveying in a Novel Screw-Nested Extruder
- Rheological and Thermal Properties of a Model System for PIM
- PPS-News
- PPS News
- Seikei Kakou Abstracts
- Seikei-Kakou Abstracts