Solid-state synthesis and magnetic properties of rhombohedral phase Mg2SiNi3

Liangbiao Wang; Dejian Zhao; Juanjuan Lu; Weiqiao Liu; Quanfa Zhou

doi:10.3139/146.111588

Article

Solid-state synthesis and magnetic properties of rhombohedral phase Mg₂SiNi₃

Liangbiao Wang , Dejian Zhao , Juanjuan Lu , Weiqiao Liu and Quanfa Zhou

Published/Copyright: January 29, 2018

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From the journal International Journal of Materials Research Volume 109 Issue 2

Abstract

A solid-state route was developed to prepare rhombohedral phase Mg₂SiNi₃ with the dimensions of about 300 nm by using metallic magnesium, nickel oxide and silicon as starting materials at 700 °C in an autoclave reactor. The obtained product was investigated by means of X-ray diffraction, scanning electron microscopy and transmission electron microscopy. Magnetic measurement at room temperature indicated that the values of saturation magenetization and coercivity of the obtained Mg₂SiNi₃ were 0.31 emu g^–1 and 65.20 Oe, respectively.

Keywords: Solid-state route; Silicide; Mg2SiNi3; Magnetic properties

*Correspondence address, Dr. Liangbiao Wang and Prof. Qianfa Zhou, School of Chemistry and Environment Engineering, Jiangsu University of Technology, No. 1801 Zhongwu Road, Changzhou 213001, P.R. China, Tel.: +86-519-86953005, Fax: +86-519-86953005, E-mail: lbwang@jsut.edu.cnlabzqf@jsut.edu.cn

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Received: 2017-07-08

Accepted: 2017-09-18

Published Online: 2018-01-29

Published in Print: 2018-02-12

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https://doi.org/10.3139/146.111588

Keywords for this article

Solid-state route; Silicide; Mg2SiNi3; Magnetic properties