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The crystal structure of synthetic CuBi5S8*

Published/Copyright: July 28, 2010
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Zeitschrift für Kristallographie - Crystalline Materials
From the journal Zeitschrift für Kristallographie - Crystalline Materials Volume 137 Issue 5-6

Abstract

The crystal structure of CuBi5S8 has been determined using three-dimensional intensity data. The unit cell, with dimensions a = 13.214 ± 0.001, b = 4.025 ± 0.003, c = 14.087 ± 0.001 Å and β = 115.6° ± 0.03° contains two formula units. The space group is C2h3–C2/m. The structure was derived from the Patterson, Fourier and difference Fourier diagrams. The final discrepancy index R is 8.5%.

The coordinations around the three independent Bi atoms are octahedral, trigonal pyramidal and square pyramidal. Two Cu atoms in the unit cell are distributed statistically in the fourfold position h (0,y,1/2) and their coordination polyhedra are distorted tetrahedra.

Published Online: 2010-7-28
Published in Print: 1973-10-1

© 2015 Oldenbourg Wissenschaftsverlag GmbH, Rosenheimer Str. 145, 81671 München

Articles in the same Issue

  1. Vacancy distribution in synthetic spinels of the series Fe304–γ-Fe2O3
  2. Structure and growth of an unusual silicon carbide polytype 147R
  3. Die Verfeinerung der Kristallstruktur eines lunaren Pigeonits
  4. Structure refinement of a barium mica
  5. Die Kristallstruktur von Bariumazidmonohydrat Ba(N3)2 · H2O
  6. The crystal structure of monoclinic CaAl2Si2O8: a case of monoclinic structure closely simulating orthorhombic symmetry
  7. On the application of a minimum residual method to the structure determination of superstructures*
  8. Symmetrie von KJO3 und die Struktur der Zimmertemperaturphase
  9. The crystal structure of synthetic CuBi5S8*
  10. Existenznachweis für eine Lösung des Phasenproblems für nichtperiodische Verteilungen*
  11. Hydroxyl orientation in muscovite polymorphs
  12. 14. Diskussionstagung der Arbeitsgemeinschaft Kristallographie der Deutschen Mineralogischen Gesellschaft, der Deutschen Physikalischen Gesellschaft und der Gesellschaft Deutscher Chemiker
  13. Berichtigung
  14. Berichtigung
https://doi.org/10.1524/zkri.1973.137.5-6.422

Articles in the same Issue

  1. Vacancy distribution in synthetic spinels of the series Fe304–γ-Fe2O3
  2. Structure and growth of an unusual silicon carbide polytype 147R
  3. Die Verfeinerung der Kristallstruktur eines lunaren Pigeonits
  4. Structure refinement of a barium mica
  5. Die Kristallstruktur von Bariumazidmonohydrat Ba(N3)2 · H2O
  6. The crystal structure of monoclinic CaAl2Si2O8: a case of monoclinic structure closely simulating orthorhombic symmetry
  7. On the application of a minimum residual method to the structure determination of superstructures*
  8. Symmetrie von KJO3 und die Struktur der Zimmertemperaturphase
  9. The crystal structure of synthetic CuBi5S8*
  10. Existenznachweis für eine Lösung des Phasenproblems für nichtperiodische Verteilungen*
  11. Hydroxyl orientation in muscovite polymorphs
  12. 14. Diskussionstagung der Arbeitsgemeinschaft Kristallographie der Deutschen Mineralogischen Gesellschaft, der Deutschen Physikalischen Gesellschaft und der Gesellschaft Deutscher Chemiker
  13. Berichtigung
  14. Berichtigung
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