Artikel
Lizenziert
Nicht lizenziert
Erfordert eine Authentifizierung
Americium, curium and neodymium analysis in ECRIX-H irradiated pellet: sample preparation for TIMS measurements
-
Eric Esbelin
Veröffentlicht/Copyright:
22. April 2013
Abstract
This paper concerns quantitative isotopic analysis of Am, Cm and Nd contained in an irradiated AmO1.62/MgO pellet. The complete analysis protocol is described, from dissolution of the pellets in a shielded line to the laboratory glove separation processes box for TIMS analysis. Emphasis is placed on the separation processes: by ion exchange resin in a hot cell and by HPLC in the laboratory. Intermediate measurements by X-ray fluorescence, alpha spectrometry, and ICP-AES are described.
Published Online: 2013-04-22
Published in Print: 2013-05
© by Oldenbourg Wissenschaftsverlag, München, Germany
Sie haben derzeit keinen Zugang zu diesem Inhalt.
Sie haben derzeit keinen Zugang zu diesem Inhalt.
Artikel in diesem Heft
- Absence of 232,230,228Th enhancement decay by ultrasound exposure
- Complexation of Cm(III) and Eu(III) with 2,6-bis(5-(2,2-dimethylpropyl)-1H-pyrazol-3-yl)pyridine and 2-bromohexanoic acid studied by time-resolved laser fluorescence spectroscopy
- Americium, curium and neodymium analysis in ECRIX-H irradiated pellet: sample preparation for TIMS measurements
- Co-extraction and stripping behavior of trivalent actinides and fission products in N,N-di-2-ethylhexyl-N´,N´-dioctyl-diglycolamide
- Mass spectrometric characterization and quantification of Pu(VI) hydrolysis products
- Effects of aging on PuO2·xH2O particle size in alkaline solution
- Redox behavior of Tc(VII)/Tc(IV) under various reducing conditions in 0.1 M NaCl solutions
- Cyclotron production of 44Sc for clinical application
- Proton irradiation parameters and chemical separation procedure for the bulk production of high-specific-activity 186gRe using WO3 targets
Artikel in diesem Heft
- Absence of 232,230,228Th enhancement decay by ultrasound exposure
- Complexation of Cm(III) and Eu(III) with 2,6-bis(5-(2,2-dimethylpropyl)-1H-pyrazol-3-yl)pyridine and 2-bromohexanoic acid studied by time-resolved laser fluorescence spectroscopy
- Americium, curium and neodymium analysis in ECRIX-H irradiated pellet: sample preparation for TIMS measurements
- Co-extraction and stripping behavior of trivalent actinides and fission products in N,N-di-2-ethylhexyl-N´,N´-dioctyl-diglycolamide
- Mass spectrometric characterization and quantification of Pu(VI) hydrolysis products
- Effects of aging on PuO2·xH2O particle size in alkaline solution
- Redox behavior of Tc(VII)/Tc(IV) under various reducing conditions in 0.1 M NaCl solutions
- Cyclotron production of 44Sc for clinical application
- Proton irradiation parameters and chemical separation procedure for the bulk production of high-specific-activity 186gRe using WO3 targets
