Tenth European Powder Diffraction Conference: Geneva, September 1-4, 2006

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Tenth European Powder Diffraction Conference

Geneva, September 1-4, 2006

Language: English

Published/Copyright: 2007

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Volume 26 | Zeitschrift für Kristallographie / Supplemente

About this book

Zeitschrift für Kristallographie. Supplement Volume 26 presents the complete Proceedings of all contributions to the X European Powder Diffraction Conference in Geneva 2006:

Method Development and Application
Instrumental
Software Development
Materials

Supplement Series of Zeitschrift für Kristallographie publishes Proceedings and Abstracts of international conferences on the interdisciplinary field of crystallography.

Topics

Frontmatter Publicly Available Download PDF	I
Preface Publicly Available Download PDF	IX
Editorial Notes Publicly Available Download PDF	XIII
European Powder Diffraction Conference Award Publicly Available Download PDF	XV
Table of Contents Publicly Available Download PDF	XVII
Powder diffraction studies on proteins: An overview of data collection approaches I. Margiolaki, J. P. Wright, A. N. Fitch, G. C. Fox, A. Labrador, R. B. Von Dreele, K. Miura, F. Gozzo, M. Schiltz, C. Besnard, F. Camus, P. Pattison, D. Beckers and T. Degen Publicly Available Download PDF	1
I. METHOD DEVELOPMENT AND APPLICATION
I.1 Determination of Crystal Structure
Nanostructure studied using the atomic pair distribution function S. J. L. Billinge Publicly Available Download PDF	17
Likelihood methods with protein powder diffraction data J. P. Wright, A. J. Markvardsen and I. Margiolaki Publicly Available Download PDF	27
The complementary use of solid state NMR and XRD to solve zeolite structures A. Russell and E. Morris Publicly Available Download PDF	33
Exploiting X-ray induced anisotropic lattice changes to improve intensity extraction in protein powder diffraction: Application to heavy atom detection C. Besnard, F. Camus, M. Fleurant, A. Dahlström, J. P. Wright, I. Margiolaki, P. Pattison and M. Schiltz Publicly Available Download PDF	39
Aspects of validation in the structure determination of organic materials from powder X-ray diffraction data Kenneth D.M. Harris Publicly Available Download PDF	45
Validation of magnetic structures A.S. Wills Publicly Available Download PDF	53
I.2 Qualitative and Quantitative Phase Analysis
New horizons for the structural characterization of stainless steel slags by X-ray powder diffraction B. Peplinski, B. Adamczyk, G. Kley, K. Adam, F. Emmerling and F.G. Simon Publicly Available Download PDF	61
Method for quick estimation of the Sb³⁺/Sb⁵⁺ content ratio in ATO B. Gržeta, E. Tkalčec, C. Goebbert, M. Takeda and M. Takahashi Publicly Available Download PDF	67
Evaluation of the phase detection limit on filter-deposited dust particles from Antarctic ice cores M. Dapiaggi, M. Sala, G. Artioli and M. J. Fransen Publicly Available Download PDF	73
I.3 Analysis of Microstructure and Macrostress
I.3.1 Residual Stresses
In-situ investigation by X-ray diffraction and wafer curvature of phase formation and stress evolution during metal thin film – silicon reactions O. Thomas Publicly Available Download PDF	81
Residual stress profile in ceramic laminates M. Ortolani, M. Leoni, P. Scardi and M. Golshan Publicly Available Download PDF	91
I.3.2 Line Broadening Analysis
Powder diffraction characterization of stacking disorder E. Estevez-Rams, A. Penton Madrigal, P. Scardi and M. Leoni Publicly Available Download PDF	99
A Debye function based powder diffraction data analysis method C. Giannini, A. Cervellino, A. Guagliardi, F. Gozzo, D. Zanchet, T. Rocha and M. Ladisa Publicly Available Download PDF	105
Illite crystallinity: Instrumental effect and its relation to crystallite size and lattice distortion Salah Shata Publicly Available Download PDF	111
Size-related diffraction anomalies from strongly distorted nano-crystals M.B. Shevchenko Publicly Available Download PDF	117
I.4 Texture
Rietveld texture analysis from diffraction images L. Lutterotti, M. Bortolotti, G. Ischia, I. Lonardelli and H.-R. Wenk Publicly Available Download PDF	125
Secondary extinction correction used in a novel method for improved XRD characterizations of textured materials: The case of thin films I. Tomov Publicly Available Download PDF	131
II. INSTRUMENTAL
In-situ powder diffraction in high magnetic fields V.K. Pecharsky, Ya. Mudryk and K.A. Gschneidner Publicly Available Download PDF	139
Characterization of a high performance laboratory parallel-beam diffractometer – bridging the gap to the synchrotron M. Wohlschlögel, T.U. Schülli, G. Maier, U. Welzel and E.J. Mittemeijer Publicly Available Download PDF	147
Design of powder diffraction beamline (BL-I11) at Diamond C.C. Tang, S.P. Thompson, T.P. Hill, G.R. Wilkin and U.H. Wagner Publicly Available Download PDF	153
In-situ analysis of crystallographic texture using high-energy X-rays H.-G. Brokmeier, S.B. Yi, B. Schwebke and J. Homeyer Publicly Available Download PDF	159
Installation of the high resolution TOF diffractometer at the Budapest Research Reactor Gy. Káli, Zs. Sánta, H. J. Bleif, F. Mezei, L. Rosta and M. Szalók Publicly Available Download PDF	165
Stress and local texture measurements at the materials science diffractometer STRESS-SPEC at FRM-II U. Garbe, M. Hofmann and H.-G. Brokmeier Publicly Available Download PDF	171
Versatile IBARAKI materials design neutron diffractometer at J-PARC T. Ishigaki, A. Hoshikawa, M. Yonemura, T. Kamiyama, S. Harjo, K. Aizawa, T. Sakuma, Y. Tomota, Y. Morii, M. Arai, M. Hayashi, K. Ebata, Y. Takano and T. Kasao Publicly Available Download PDF	177
From powder diffraction to structure resolution of nanocrystals by precession electron diffraction S. Nicolopoulos, J.P. Morniroli and M. Gemmi Publicly Available Download PDF	183
III. SOFTWARE
Powder pattern indexing and the dichotomy algorithm D. Louër and A. Boultif Publicly Available Download PDF	191
EFLECH/INDEX – Another try of whole pattern indexing J. Bergmann Publicly Available Download PDF	197
Predicted corner-sharing titanium silicates A. Le Bail Publicly Available Download PDF	203
Using the Cambridge Structural Database to validate powder structures G. Barr, W. Dong, C.J. Gilmore, A. Kern, A. Parkin and C.C. Wilson Publicly Available Download PDF	209
Two-dimensional powder diffraction B. Hinrichsen, R. E. Dinnebier and M. Jansen Publicly Available Download PDF	215
IV. MATERIALS
IV.1 Thin Layers
X-ray diffraction analysis of an ε/γʹ – ironnitride compound double layer T. Gressmann, A. Leineweber, E.J. Mittemeijer and M. Knapp Publicly Available Download PDF	223
Texture of submicron Ni-Mn-Ga films studied by X-ray diffraction at the ANKA synchrotron source V.A. Chernenko, S. Doyle, M. Kohl, P. Müllner, S. Besseghini and M. Ohtsuka Publicly Available Download PDF	229
Texture and stress in nickel layers with incorporated zirconia particles P. Angerer, P. Pessenda-Garcia, E. Neubauer and G. E. Nauer Publicly Available Download PDF	235
Growth of magnetron sputtered TiO₂ thin films studied by X-ray scattering R. Kužel, L. Nichtová, D. Heřman, J. Šícha and J. Musil Publicly Available Download PDF	241
Study of crystallization of magnetron sputtered TiO₂ thin films by X-ray scattering R. Kužel, L. Nichtová, Z. Matěj, D. Heřman, J. Šícha and J. Musil Publicly Available Download PDF	247
IV.2 Nanocrystalline and Amorphous Materials
Transition of nc-SiC powder surface into grain boundaries during sintering by molecular dynamics simulation and neutron powder diffraction M. Wojdyr, Y. Mo, E. Grzanka, S. Stelmakh, S. Gierlotka, Th. Proffen, T.W. Zerda, B. Palosz and I. Szlufarska Publicly Available Download PDF	255
Evolution of the microstructure in nanocrystalline copper electrodeposits during room temperature storage Karen Pantleon and Marcel A.J. Somers Publicly Available Download PDF	261
Melting of small silver clusters investigated by HT-GIXRD M. Quaas, I. Shyjumon, R. Hippler and H. Wulff Publicly Available Download PDF	267
The use of RDF analysis in the study of powder samples: Zirconia complex supported by clay and pseudoboehmite E.M. Moroz and D.A. Zuyzin Publicly Available Download PDF	273
RDF method application to phase analysis of X-ray amorphous products of gibbsite thermal activation K.I. Shefer, E.M. Moroz, L.I. Isupova, I.V. Kharina and Yu.Yu. Tanashev Publicly Available Download PDF	279
Study of nanoalloys formation mechanism from single-source precursors [M(NH₃)₅Cl](ReO₄)₂, M = Rh, Ir E. Yu. Filatov, Yu. V. Shubin and S. V. Korenev Publicly Available Download PDF	283
Synthesis and thermal decomposition of the oxalatho cuprates(II) – [M(NH₃)₄][Cu(C₂O₄)₂]*3H₂O, M = Pt, Pd K. V. Yusenko, E. Yu. Filatov, D. B. Vasilchenko, I. A. Baidina, A. V. Zadesenez and Yu. V. Shubin Publicly Available Download PDF	289
IV.3 Metals and Alloys
IV.3.1 General
HT-XRD in the study of Cu-Li-Mg M. H. Braga, J. Ferreira, L. F. Malheiros and M. Hämäläinen Publicly Available Download PDF	299
Phase distribution of friction welded Ti6Al4V/γ-TAB H.-G. Brokmeier, S.-J. Jin, V. Ventzke, S. Riekehr, M. Kocak and J. Homeyer Publicly Available Download PDF	305
Mixed site occupancies in μ-Zr-Nb-Al by resonant powder diffraction J.-M. Joubert, R. Černý and H. Emerich Publicly Available Download PDF	311
Gold leaf decoration on medieval islamic glazed ceramics – in search of technological features with XRD C. Pacheco, R. Chapoulie, E. Dooryhee and Ph. Goudeau Publicly Available Download PDF	317
IV.3.2 Microstructure, Stress and Texture
Use of generalised pole figures in the X-ray study of textured metal materials Yu. Perlovich, M. Isaenkova and V. Fesenko Publicly Available Download PDF	327
Reconstruction of high-temperature deformation process by texture of the low-temperature phase as applied to Zrbased alloys M. Isaenkova, Yu. Perlovich, V. Fesenko and M. Grekhov Publicly Available Download PDF	333
X-ray studies of nanostructured metals processed by severe plastic deformation A.R. Kilmametov, A.V. Khristoforov, G. Wilde and R.Z. Valiev Publicly Available Download PDF	339
Microstructure evolution of nanocrystalline HITPERM and NANOPERM alloys: Insight from in-situ synchrotron radiation experiments R. Nicula, V.D. Cojocaru, J. Bednarcik, M. Stir and E. Burkel Publicly Available Download PDF	345
Time resolved in-situ synchrotron radiation diffraction investigation of grain-growth kinetics in magnetic nanocomposites J. Bednarčík, R. Nicula, V.D. Cojocaru, M. Stir and E. Burkel Publicly Available Download PDF	351
Triaxial residual stresses in composite tube from austenitic stainless steel with welded ferritic steel cladding Yu.V. Taran, J. Schreiber, A.M. Balagurov, U. Stuhr, H. Kockelmann and V.B. Zlokazov Publicly Available Download PDF	355
Neutron diffraction investigation of the residual stress gradient near stainless steel – zirconium alloy interface A.V. Tamonov, V.V. Sumin and U. Stuhr Publicly Available Download PDF	361
IV.4 Minerals and Inorganics
IV.4.1 Structural Changes, In-situ and Non-Ambient Investigations
High temperature X-ray diffraction investigation of an aluminium-siliconcorundum system D. Garipoli, P. Bergese, E. Bontempi, M. Minicucci, A. Di Cicco and L. E. Depero Publicly Available Download PDF	369
Investigation of the βʹ to α-phase transformation temperature of (Ca_1-xMg_x)₃(PO₄)₂ solid solutions F. Goetz-Neunhoeffer, J. Neubauer, R. Enderle and M. Göbbels Publicly Available Download PDF	375
Vacancies ordering in La³⁺_1-xBa²⁺_xFeO_3-δ perovskites A.N. Nadeev, S.V. Tsybulya, G.N. Kryukova, I.S. Yakovleva and L.A. Isupova Publicly Available Download PDF	381
In-situ investigations of LiMn₂O₄ at high pressure Paweł Piszora Publicly Available Download PDF	387
Structural study of pure silica and Gecontaining zeolite ITQ-24 J.L. Jordá, A. Cantín, A. Corma, M.J. Diaz-Cabañas, S. Leiva, M. Moliner, F. Rey, M.J. Sabater and S. Valencia Publicly Available Download PDF	393
Structure properties of chemisorbed methyl groups in the framework of faujasite zeolitic catalysts S. Vratislav, M. Dlouhá and V. Bosáček Publicly Available Download PDF	399
Synchrotron radiation XRPD study on the early hydration of cements M. Merlini, C. Meneghini, G. Artioli and T. Cerulli Publicly Available Download PDF	411
Effect of interlayer cation and relative humidity on the hydration properties of a dioctahedral smectite W. Oueslati, M. S. Karmous, H. Ben Rhaiem, B. Lanson and A. Ben Haj Amara Publicly Available Download PDF	417
Time-resolved synchrotron X-ray powder diffraction study of biogenic nanomagnetite A.M.T. Bell, V.S. Coker, C.I. Pearce, R.A.D. Pattrick, G. van der Laan and J.R. Lloyd Publicly Available Download PDF	423
Utilizing total scattering to study the Jahn-Teller transition in La_1-xCa_xMnO₃ E. S. Božin, X. Qiu, R. J. Worhatch, G. Paglia, M. Schmidt, P. G. Radaelli, J. F. Mitchell, T. Chatterji, Th. Proffen and S. J. L. Billinge Publicly Available Download PDF	429
Neutron diffraction study of Pr_0.5Ca_0.5CoO_3-γ (γ=0 and 0.07) A. Chichev, M. Dlouhá, S. Vratislav, J. Hejtmánek, Z. Jirák, K. Knížek and M. Maryško Publicly Available Download PDF	435
Advances in the characterisation of domain switching in ferroelectric ceramics J. L. Jones, J. E. Daniels and E. Üstündag Publicly Available Download PDF	441
The nature of special points on unit cell parameters temperature dependences for crystal substances Stanislav K. Filatov and Rimma S. Bubnova Publicly Available Download PDF	447
IV.4.2 Determination of Crystal Structure; Structure Refinement
Combined high resolution powder and single-crystal diffraction to determine the structure of Li^1+xCe^III_xCe^IV_6-xF₂₅ G. Renaudin, E. Mapemba, M. El-Ghozzi, M. Dubois and R. Černý Publicly Available Download PDF	455
Crystal Structure of the Ba₃MgSi₂O₈:Mn²⁺,Eu²⁺ phosphor for white light emitting diodes T. Aitasalo, A. Hietikko, J. Hölsä, M. Lastusaari, J. Niittykoski and T. Piispanen Publicly Available Download PDF	461
Rietveld refinements of SnO₂ ceramic powders doped with ZnO, WO₃, CoO, Nb₂O₅ and MoO₃ J. A. G. Carrió, T. J. Masson, A. H. Munhoz, M. M. de Jesus, L. Perazolli, U. Coleto, S. Gutierrez-Antonio, R. F. C. Marques and C. O. Paiva-Santos Publicly Available Download PDF	467
Synchrotron X-ray powder diffraction studies of solubility limits in the LiFe₅O₈-LiAl₅O₈ spinel solid solutions J. Darul, W. Nowicki, P. Piszora and E. Wolska Publicly Available Download PDF	471
Synchrotron X-ray diffraction study on the cation distribution in quaternary Li-Fe-Mn spinel oxides W. Nowicki, J. Darul, P. Piszora, C. Baehtz and E. Wolska Publicly Available Download PDF	477
Diffraction analysis of the lithium battery cathode material Li_1.2Mn_0.4Ni_0.3Co_0.1O₂ P.S. Whitfield, I.J. Davidson, P.W. Stephens, L.M.D. Cranswick and I.P. Swainson Publicly Available Download PDF	483
Defect structure examination of Sn-doped indium oxide (ITO) J. Popović, E. Tkalčec, B. Gržeta, C. Goebbert, V. Ksenofontov and M. Takeda Publicly Available Download PDF	489
Modulation of Cu-O chain length in SmBa₂Cu₃O_6+δ, by Al doping and clustering M. Scavini, M. Daldosso, M. Brunelli, C. Ferrero and C. Oliva Publicly Available Download PDF	495
Simulation of the XRD patterns, structural properties of a synthetic Na-Hectorite exchanged Cu²⁺ and Ca²⁺ M.S. Karmous, W. Oueslati, H. Ben Rhaiem, J. L. Robert and A. Ben Haj Amara Publicly Available Download PDF	503
IV.4.3 Determination of Magnetic Structure, Magnetic Materials
Intermediate phase in the oxidative hydrothermal synthesis of potassium jarosite, a model kagomé antiferromagnet W. Bisson and A. S. Wills Publicly Available Download PDF	511
Neutron powder diffraction study on the magnetic ordering and structure of Li_xMn_3-x-yFe_yO₄ spinels E. Wolska, W. Nowicki, J. Darul, M. Tovar, O. Prokhnenko and P. Piszora Publicly Available Download PDF	517
IV.4.4 Microstructure, Phase Analysis
Phase composition and thermal expansion behaviour of zirconium tungstate prepared by rapid sintering E. Neubauer and P. Angerer Publicly Available Download PDF	525
X-ray phase analysis in leucite systems J. Maixner, A. Kloužková, M. Mrázová and M. Kohoutková Publicly Available Download PDF	531
Structural analysis by the Rietveld method and SEM of irradiated pseudoboehmite and Al₂O₃ J. A. G. Carrió, S. B. Faldini, L. F. de Miranda, P. K. Kiyohara, L. G. A. Silva and A. H. Munhoz Publicly Available Download PDF	537
Rietveld refinement of ZrSiO₄: Application of a phenomenological model of anisotropic peak width A. Sarkar, P. Mukherjee and P. Barat Publicly Available Download PDF	543
X-ray diffraction line broadening in dry grinding of kaolinite P. Pardo, J. Bastida, M.A. Kojdecki, R. Ibáñez and M. Zbik Publicly Available Download PDF	549
IV.5 Organic Materials
Microstructure of energetic crystals – grain by grain via rocking curve M. Herrmann, P. B. Kempa and S. Doyle Publicly Available Download PDF	557
The presence of polymorphism in oxytetracycline hydrochloride shown by X-ray powder diffraction techniques R. Toro, G. Díaz de Delgado, A. Bahsas and J.M. Delgado Publicly Available Download PDF	563
Synthesis and structural characterization of mixed transition metal derivatives of maleic acid: (M²⁺_0.5Fe²⁺_0.5)(C₄H₃O₄)^-₂·4H₂O (with M²⁺=Mn, Co, Ni, and Zn) using powder diffraction data T. González, A. Briceño, G. Díaz de Delgado and J.M. Delgado Publicly Available Download PDF	569
Structure determination and phase transition behaviour of mesitylene R.M. Ibberson, S. Parsons, I. Natkaniec and K. Hołderna-Natkaniec Publicly Available Download PDF	575
Structures of transition metal hydroxyterephthalates A. Carton, A. Mesbah, M. François and P. Rabu Publicly Available Download PDF	581
Analysis of intra- and intermolecular hydrogen bonding in androstane derivatives: A case study of steroids Rajnikant, Dinesh and Bhavnaish Publicly Available Download PDF	587
Structures of magnesium and zinc long aliphatic chains carboxylates A. Mesbah, C. Juers, M. François, E. Rocca and J. Steinmetz Publicly Available Download PDF	593
The crystal structures of the β1 and β2 polymorphs of mono-unsaturated triacylglycerols and cocoa butter determined from high resolution powder diffraction data J.B. van Mechelen, R. Peschar and H. Schenk Publicly Available Download PDF	599
Microphase separation in semifluorinated polyesters D. Jehnichen, D. Pospiech, L. Häußler, P. Friedel, S.S. Funari, J. Tsuwi and F. Kremer Publicly Available Download PDF	605
Powder diffraction studies of organoammonium polymolibdates B. Gaweł and W. Łasocha Publicly Available Download PDF	611
Author Index Publicly Available Download PDF	XXIX

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eBook published on:

October 29, 2015

eBook ISBN:

9783486992540

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October 29, 2015

Paperback ISBN:

9783486992533

Pages and Images/Illustrations in book

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36

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220

https://doi.org/10.1524/9783486992540

eBook ISBN: 9783486992540

Paperback ISBN: 9783486992533

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Tenth European Powder Diffraction Conference

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