Ninth European Powder Diffraction Conference: Prague, September 2-5, 2004

$book: Ninth European Powder Diffraction Conference$

Book Open Access

Ninth European Powder Diffraction Conference

Prague, September 2-5, 2004

Language: English

Published/Copyright: 2006

Published by

Become an author with De Gruyter Brill

Explore this Subject How to publish with us

This book is in the series

Volume 23 | Zeitschrift für Kristallographie / Supplemente

About this book

Zeitschrift für Kristallographie. Supplement Volume 23 presents the complete Proceedings of all contributions to the IX European Powder Diffraction Conference in Prague 2004:

Method Development and Application
Instrumental
Software Development
Materials

Supplement Series of Zeitschrift für Kristallographie publishes Proceedings and Abstracts of international conferences on the interdisciplinary field of crystallography.

Topics

Frontmatter Publicly Available Download PDF	I
Preface: Condensation of Scientific Knowledge on Powder Diffraction Publicly Available Download PDF	VII
Editorial Notes Publicly Available Download PDF	XIII
European Powder Diffraction Conference Award Publicly Available Download PDF	XV
Table of Contents Publicly Available Download PDF	XVII
I. METHOD DEVELOPMENT AND APPLICATION
I.1 Determination of Crystal Structure
Protein polycrystallography R. B. Von Dreele, P. L. Lee and Y. Zhang Publicly Available Download PDF	3
Using the parallel tempering algorithm to overcome complex problems in structure determination of inorganic materials with laboratory X-rays T. Bataille, N. Mahé, E. Le Fur, J.-Y. Pivan and D. Louër Publicly Available Download PDF	9
Molecular crystal structures from powder X-ray diffraction techniques Eugene Y. Cheung and Kenneth D.M. Harris Publicly Available Download PDF	15
On the uncertainty of lattice parameters refined from neutron diffraction data B. Peplinski, D. M. Többens, W. Kockelmann and R. M. Ibberson Publicly Available Download PDF	21
I.2 Qualitative and Quantitative Phase Analysis
Application of the Rietveld method to the severely superimposed diffraction patterns of technical products containing a large number of solid solution phases B. Peplinski, P. Köcher and G. Kley Publicly Available Download PDF	29
Application of X-ray diffraction in forensic science Marek Kotrlý Publicly Available Download PDF	35
I.3 Analysis of Microstructure and Macrostress
I.3.1 Residual Stresses
Diffraction stress analysis of grain interaction in polycrystalline materials U. Welzel, S. Fréour, A. Kumar and E. J. Mittemeijer Publicly Available Download PDF	43
Accurate absolute peak positions for multiple {hkl} residual stress analysis by means of misalignment corrections Arnold C. Vermeulen Publicly Available Download PDF	49
Diffraction stress analysis of strongly fibre-textured gold layers A. Kumar, U. Welzel and E.J. Mittemeijer Publicly Available Download PDF	55
Residual stress measurement of gold artefacts by Debye ring analysis P. Zanola, D. Benedetti, E. Bontempi, V. Villa, G. Baronio, M. Tosti, R. Roberti and L. E. Depero Publicly Available Download PDF	61
X-ray residual stress measurement in titanium nitride thin films M. Dopita and D. Rafaja Publicly Available Download PDF	67
I.3.2 Line Broadening Analysis
Dislocation line broadening R. Kužel Publicly Available Download PDF	75
Considerations concerning Wilkens’ theory of dislocation line-broadening N. Armstrong, M. Leoni and P. Scardi Publicly Available Download PDF	81
Momentum method applied to evaluation of size and strain in ball-milled iron A. Borbély, A. Révész and I. Groma Publicly Available Download PDF	87
Microstructure of severely deformed metals from X-ray line profile analysis J. Gubicza, N. H. Nam, K. Máthis and V. V. Stolyarov Publicly Available Download PDF	93
Burgers Vector Populations in hot rolled titanium determined by X-ray Peak Profile Analysis I. C. Dragomir, G. A. Castello-Branco, G. Ribarik, H. Garmestani, T. Ungar and R. L. Snyder Publicly Available Download PDF	99
Spatial fluctuations of the microstructure during deformation of Cu single crystals M. Kerber, E. Schafler, P. Hanak, G. Ribàrik, S. Bernstorff, T. Ungàr and M. Zehetbauer Publicly Available Download PDF	105
Analysis of polydisperse ball-milled fluorite powders using a full pattern technique M. Leoni, G. De Giudici, R. Biddau, M. D'Incau and P. Scardi Publicly Available Download PDF	111
Anisotropic microstrain broadening due to compositional inhomogeneities and its parametrisation A. Leineweber and E. J. Mittemeijer Publicly Available Download PDF	117
X-ray diffraction from epitaxial thin films: an analytical expression of the line profiles accounting for microstructure A. Boulle, R. Guinebretière and A. Dauger Publicly Available Download PDF	123
Microstructure of post-deformed ECAPTi investigated by Multiple X-Ray Line Profile Analysis E. Schafler, K. Nyilas, S. Bernstorff, L. Zeipper, M. Zehetbauer and T. Ungàr Publicly Available Download PDF	129
The Dislocation-Structure and Crystallite- Size in Forsterite (Olivine) Deformed at 1400 °C by 11 GPa Krisztián Nyilas, Hélène Couvy, Patrick Cordier and Tamás Ungár Publicly Available Download PDF	135
Diffuse X-ray scattering from GaN/SiC (0001) thin films S. Daniš and V. Holý Publicly Available Download PDF	141
Test of applicability of some powder diffraction tools to nanocrystals Z. Kaszkur Publicly Available Download PDF	147
Influence of coherent connection of crystalline blocks on the diffraction pattern of nanostructured materials S.V. Cherepanova and S.V. Tsybulya Publicly Available Download PDF	155
I.4 Texture
Automated Crystal Orientation Measurement by backscatter Kikuchi diffraction Robert A. Schwarzer Publicly Available Download PDF	163
A simple technique for correcting diffraction intensities for the effects of preferred orientation in calcite samples S. Battaglia and L. Leoni Publicly Available Download PDF	169
Influence of extinction phenomenon on determination of the orientation distribution function G. Gómez-Gasga, T. Kryshtab, J. Palacios-Gómez and A. de Ita de la Torre Publicly Available Download PDF	175
II. INSTRUMENTAL
First test measurements at the new structure powder diffractometer (SPODI) at the FRM-II R. Gilles, M. Hoelzel, M. Schlapp, F. Elf, B. Krimmer, H. Boysen and H. Fuess Publicly Available Download PDF	183
EXED – the new Extreme Environment Diffractometer at the Hahn-Meitner-Institut Berlin J. Peters, K. Lieutenant, D. Clemens and F. Mezei Publicly Available Download PDF	189
R2D2: a new neutron powder diffractometer at NFL A. Wannberg, M. Grönros, A. Mellergård, L-E. Karlsson, R. G. Delaplane and B. Lebech Publicly Available Download PDF	195
Bent perfect crystal monochromator at the monochromatic focusing condition Y. N. Choi, S. A. Kim, S. K. Kim, S. B. Kim, C. H. Lee, P. Mikula and M. Vrána Publicly Available Download PDF	199
Multiple-reflection neutron bent-perfect-crystal (BPC) monochromator P. Mikula, M. Vrána and V. Wagner Publicly Available Download PDF	205
Wavelength calibration in conventional SANS setup with a mechanical velocity selector L. Almásy, A. Len, M. Markó and E. Rétfalvi Publicly Available Download PDF	211
Neutron RTOF diffractometer FSD for residual stress investigation A. M. Balagurov, G. D. Bokuchava, E. S. Kuzmin, A. V. Tamonov and V. V. Zhuk Publicly Available Download PDF	217
III. SOFTWARE DEVELOPMENT
Indexing with the successive dichotomy method, DICVOL04 D. Louër and A. Boultif Publicly Available Download PDF	225
Powder3D: An easy to use program for data reduction and graphical presentation of large numbers of powder diffraction patterns B. Hinrichsen, R. E. Dinnebier and M. Jansen Publicly Available Download PDF	231
BRASS, the Bremen Rietveld analysis and structure suite J. Birkenstock, R.X. Fischer and T. Messner Publicly Available Download PDF	237
FAULTS, a new program for refinement of powder diffraction patterns from layered structures M. Casas-Cabanas, J. Rodríguez-Carvajal and M.R. Palacín Publicly Available Download PDF	243
PM2K: a flexible program implementing Whole Powder Pattern Modelling M. Leoni, T. Confente and P. Scardi Publicly Available Download PDF	249
Calculating the peak shape of axially focussing powder diffractometers D. M. Többens Publicly Available Download PDF	255
IV. MATERIALS
IV.1 Thin Layers
X-ray scattering from interface dislocations in highly mismatched oxide epitaxial films R. Guinebretière, A. Boulle, O. Masson and A. Dauger Publicly Available Download PDF	263
Influence of magnetron sputtering conditions on the parameters of TiN coatings on steel substrates R. Mirchev, V. Antonov, I. Iordanova and P. J. Kelly Publicly Available Download PDF	269
Structural and microstructural characterisation of ZrN coatings for decorative applications P. Zanola, E. Bontempi, M. Gelfi, M. Tosti, R. Roberti and L. E. Depero Publicly Available Download PDF	275
Chalcogenide films on glass substrate as attenuators of X-ray radiation S. R. Lukić, D. M. Petrović, G. R. Štrbac and D. D. Štrbac Publicly Available Download PDF	281
Effect of annealing conditions on structural transformation of ZnS thin film T. Kryshtab, J. Palacios Gómez and M. Mazin Publicly Available Download PDF	287
Electrocrystallization of Pt layers onto Au substrates; an X-ray diffraction study I. Yu. Molina, L. M. Plyasova, S. V. Cherepanova, E. R. Savinova and G. A. Tsirlina Publicly Available Download PDF	293
Residual stress mapping in the zirconia electrolyte layer of a high-temperature solid oxide fuel cell Werner Fischer and Günther Blass Publicly Available Download PDF	299
Ultrashort period Cu/Si and Ni/C multilayers for X-ray mirrors M. Jergel, M. Ožvold, R. Senderák, Š. Luby and E. Majková Publicly Available Download PDF	305
IV.2 Nanocrystalline Materials
Microstructure of nanocrystalline materials studied by powder diffraction Publicly Available Download PDF	313
Preparation and characterization of isometric gold nanoparticles with pre-calculated size M. Šlouf, R. Kužel and Z. Matěj Publicly Available Download PDF	319
Bulk characterization of multiwall carbon nanotubes Jette Oddershede and Kenny Ståhl Publicly Available Download PDF	325
Neutron diffraction studies of the atomic vibrations of bulk and surface atoms of nanocrystalline SiC S. Stel’makh, E. Grzanka, Y. Zhao, W. Palosz and B. Palosz Publicly Available Download PDF	331
Phase transition in nanocrystalline ZnO E. Grzanka, S. Gierlotka, S. Stelmakh, B. Palosz, T. Strachowski, A. Swiderska-Sroda, G. Kalisz, W. Lojkowski and F. Porsch Publicly Available Download PDF	337
IV.3 Metals and Alloys
Study of martensitic transformation in fatigued stainless steel by neutron diffraction stress analysis Yu. V. Taran, M. R. Daymond, E. C. Oliver and J. Schreiber Publicly Available Download PDF	345
The evaluation of the kinetics of ordering processes in Ni_1+δSn (δ = 0.35, 0.50) by X-ray powder diffraction A. Leineweber and E.J. Mittemeijer Publicly Available Download PDF	351
In situ neutron diffraction study of the low cycle fatigue of the α−γ duplex stainless steel P. Lukáš, O. Muránsky, J. Polák and P. Jenčuš Publicly Available Download PDF	357
SANS investigation of precipitate microstructure in nickel-base superalloys Waspaloy and DT750 P. Strunz, J. Zrník, T. Seliga and H. J. Penkalla Publicly Available Download PDF	363
Diffraction analysis of iron materials after surface machining M. Čerňanský, N. Ganev, J. Barcal, J. Drahokoupil and K. Kolařík Publicly Available Download PDF	369
Non-destructive phase analysis and residual stresses measurement using grazing angle X-ray diffraction geometry S. J. Skrzypek, J. Jeleńkowski, T. Borowski, W. Ratuszek and T. Wierzchoń Publicly Available Download PDF	375
Thermal stability of the microstructure of severely deformed copper L. Balogh, J. Gubicza, R. J. Hellmig, Y. Estrin and T. Ungár Publicly Available Download PDF	381
Archaeometric study of Dutch Tin-Lead spoon fragments from Amsterdam: 1500–1775 AD. A neutron diffraction study D. Visser, W. Kockelmann, P. Hallebeek, J. Veerkamp and W. Krook Publicly Available Download PDF	387
Characterisation of radiation-induced precipitates in reactor pressure vessel steels J. Šaroun, J. Kočík, E. Garcia-Matres, O. Muraňský and P. Strunz Publicly Available Download PDF	393
Structure analysis of NiZr₂ in reciprocal and real space N. Mattern, J. Sakowski and C. Baehtz Publicly Available Download PDF	399
In situ high temperature XRD studies of the crystallisation of melt-spun Mg₇₇Ni₁₈Y₅ A. Teresiak, A. Gebert, M. Savyak, N. Mattern and M. Uhlemann Publicly Available Download PDF	405
Complex intermetallic compounds in the Mg-Ir system solved by powder diffraction Radovan Černý, Guillaume Renaudin, Yaroslav Tokaychuk and Vincent Favre-Nicolin Publicly Available Download PDF	411
IV.4 Minerals and Inorganics
IV.4.1 Structural Changes, Non-Ambient Conditions
Low temperature SR-XRPD study of åkermanite-gehlenite solid solution M. Merlini, M. Gemmi and G. Artioli Publicly Available Download PDF	419
Study of the structural evolution and selectivity of Wyoming montmorillonite in relation with the concentration of Cu²⁺ and Ni²⁺ W. Oueslati, H. Ben Rhaiem, M.S. Karmous, S. Naaman and A. Ben Haj Amara Publicly Available Download PDF	425
The interlayer structure and thermal behavior of Cu and Ni montmorillonites M. S. Karmous, H. Ben Rhaiem, S. Naamen, W. Oueslati and A. Ben Haj Amara Publicly Available Download PDF	431
Structural characterisation of hightemperature K-exchanged sodalite M. Dapiaggi, G. Artioli, C. Mazzocchia and M. Merlini Publicly Available Download PDF	437
A time-resolved X-ray powder diffraction method to trace the decomposition of PdB_y solid solutions T. G. Berger, A. Leineweber, E. J. Mittemeijer and M. Knapp Publicly Available Download PDF	443
γʹ-Fe₄N formation in decomposing ε-Fe₃N: A powder diffraction study using synchrotron radiation T. Liapina, A. Leineweber, E. J. Mittemeijer, M. Knapp, C. Baehtz, Z. Q. Liu, K. Mitsuishi and K. Furuya Publicly Available Download PDF	449
X – ray powder diffraction study of leucite crystallisation M. Novotna and J. Maixner Publicly Available Download PDF	455
Neutron diffraction structure study of borosilicate based matrix glasses M. Fábián, E. Sváb, Gy. Mészáros, L. Kőszegi, L. Temleitner and E. Veress Publicly Available Download PDF	461
Neutron diffraction studies of temperature induced phase transitions in Rb₂KFeF₆ elpasolite S. G. Vasilovsky, V. V. Sikolenko, A. I. Beskrovny, A. V. Belushkin, I. N. Flerov, A. Tressaud and A. M. Balagurov Publicly Available Download PDF	467
IV.4.2 Determination of Crystal Structure
Cation distribution in Li₂M(II)Sn₃O₈, M(II) = Mg, Co, Fe T. Trendafilova, D. Kovacheva, K. Petrov and A. Hewat Publicly Available Download PDF	475
Crystal structure of the monoclinic Ba₂MgSi₂O₇ persistent luminescence material T. Aitasalo, J. Hölsä, T. Laamanen, M. Lastusaari, L. Lehto, J. Niittykoski and F. Pellé Publicly Available Download PDF	481
Cation distributions in fully hydrated Sr-and Rb- bicationic zeolites: an X-ray anomalous powder diffraction study H. Palancher, C. Pichon, J. L. Hodeau, J. F. Bérar, J. Lynch, B. Rebours and J. Rodriguez-Carvajal Publicly Available Download PDF	487
Model of structure disorder of illite: preliminary results S. Ferrari, A. F. Gualtieri, G. H. Grathoff and M. Leoni Publicly Available Download PDF	493
XRD study of the stacking mode of the nacrite/alkali halides complexes S. Naamen, H. Ben Rhaïem, M. S. Karmous and A. Ben Haj Amara Publicly Available Download PDF	499
Crystal structure determination and Rietveld refinement of rosasite and mcguinnessite N. Perchiazzi Publicly Available Download PDF	505
Rietveld analysis of polytypic Zn_1−xMg_xSe and Zn_1−x−yMg_xBeySe solid solutions R. Minikayev, W. Paszkowicz, F. Firszt, H. Męczyńska and A. Marasek Publicly Available Download PDF	511
A proposition for the structure of ammonium hydrogen (acid) urate from uroliths P. Friedel, J. Bergmann, R. Kleeberg and G. Schubert Publicly Available Download PDF	517
X-ray powder diffraction data of synthetic ß- Tricalcium Phosphate M. Ermrich and F. Peters Publicly Available Download PDF	523
Distribution of sodium cations and chemisorbed methyl groups in the structure of NaX and NaLSX zeolite catalysts by powder neutron diffraction and ¹³C NMR S. Vratislav, M. Dlouhá and V. Bosáček Publicly Available Download PDF	529
IV.4.3 Determination of Magnetic Structure, Magnetic Materials
Structural and magnetic study of magnetoelectric perovskite Sr₂CoMoO₆ S. A. Ivanov, S.-G. Eriksson, R. Tellgren, H. Rundlöf and M. Tssegai Publicly Available Download PDF	537
Crystal structure and magnetism of Pr[Fe(CN)₆]·4D₂O V. Kavečanský, M. Mihalik, S. Maťaš, Z. Mitróová and M. Lukáčová Publicly Available Download PDF	543
IV.4.4 Microstructure, Phase Analysis
Microstructure of crystalline phases in electrotechnical porcelains J. M. Amigó, F. J. Serrano, M. A. Kojdecki, J. Bastida, V. Esteve and M. M. Reventós Publicly Available Download PDF	551
Micro(nano)structure of the glacial state in triphenyl phosphite (TPP) P. Derollez, A. Hédoux, Y. Guinet, J. Lefebvre, M. Descamps and O. Hernandez Publicly Available Download PDF	557
Correlation between texture and tabletting properties of some pharmaceutical tablets M. Koivisto, E. Suihko and V.-P. Lehto Publicly Available Download PDF	563
Incrustation of precious stones in dental apatite L. Bucio, I. A. Belío-Reyes, J. A. Rodríguez, M. N. Orta, J. Arenas-Alatorre, C. Magaña and R. Velázquez Publicly Available Download PDF	569
Microstructural analysis of ZnO from different aqueous synthesis routes G. Vanhoyland, D. Mondelaers, H. Van den Rul, J. D'Haen, L.C. Van Poucke and J. Mullens Publicly Available Download PDF	575
The effect of Al and Gd doping on the structure, microstructure and thermal expansion of gallium nitride (GaN) Z. K. Heiba, Sameh Ahmed, Ali Abo-Shama and Karimat El-Sayed Publicly Available Download PDF	581
Quantitative phase analysis of ordinary Portland cements using synchrotron radiation powder diffraction A. G. De la Torre, A. Cabeza, E. R. Losilla and M. A. G. Aranda Publicly Available Download PDF	587
IV.5 Organic Materials
Ab initio structure determination of two anhydrous forms of α-lactose by powder X-ray diffraction C. Platteau, J. Lefebvre, S. Hemon, F. Affouard, J. F. Willart and P. Derollez Publicly Available Download PDF	595
Structure determination of 1-pentanol (C₅H₁₂O) at 183 K M. Ramírez-Cardona, J. C. Escamilla-Casas, M. A. Cuevas-Diarte and I. Barajas-Rosales Publicly Available Download PDF	601
Crystallographic texture changes of wood due to air parameter variations J. T. Bonarski and W. Olek Publicly Available Download PDF	607
Poly(ethylene glycol) interactions with proteins J. Hašek Publicly Available Download PDF	613
Author Index Publicly Available Download PDF	xxvii

Publishing information

Pages and Images/Illustrations in book

eBook published on:

October 29, 2015

eBook ISBN:

9783486992526

Paperback published on:

November 13, 2015

Paperback ISBN:

9783486992519

Pages and Images/Illustrations in book

Front matter:

36

Main content:

618

https://doi.org/10.1524/9783486992526

eBook ISBN: 9783486992526

Paperback ISBN: 9783486992519

Safety & product resources

Manufacturer information:
Walter de Gruyter GmbH
Genthiner Straße 13
10785 Berlin
productsafety@degruyterbrill.com

Ninth European Powder Diffraction Conference

Overview

About this book

Topics

Table of contents

Bibliographic data