Abstract
Microwave enhanced gold nanoparticles (Au NPs) were synthesized using gum Arabic as both reducing and stabilizing agents. Response surface methodology was applied to study effects of the Au NPs synthesized parameters, namely, microwave exposure time (90–180 s) and the amount of AgNO3 solution (1–10 mL) on the mean particle size, mixture solution color and concentration of the synthesized Au NPs. The colloidal solution containing well-dispersed and spherical fabricated Au NPs with mean particle size (22 nm) and maximum concentration (159 ppm) and color (1.12 absorbance unit, a.u.), were obtained at the optimal synthesis conditions, using 8.17 mL of HAuCl4 (1 mM) and 2 mL of gum Arabic solution (4% w/v) during microwave exposure time of 180 s. The physico-chemical properties of the synthesized Au NPs at obtained optimum synthesis conditions were characterized by Fourier transform-infrared spectroscopy, UV-Vis spectroscopy, dynamic light scattering, X-ray diffraction, transmission electron microscopy and field emission scanning electron microscopy.
Acknowledgements
The authors would like to acknowledge the Iran Nanotechnology Initiatives Council (INIC) for funding the development of an innovative methodology for safety assessment of industrial nanomaterials (grant no. 84465).
Conflict of interest statement: The authors declare that they have no conflict of interest.
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Articles in the same Issue
- Frontmatter
- Uniform Airy Approximation for Nonadiabatic Transitions in a Curve-Crossing Weak-Coupling Case
- Microwave Accelerated Green Synthesis of Gold Nanoparticles Using Gum Arabic and their Physico-Chemical Properties Assessments
- Electrochemical Sensor for the Determination of Paracetamol at Carbamazepine Film Coated Carbon Paste Electrode
- Green Synthesis of CoFe2O4 and Investigation of its Catalytic Efficiency for Degradation of Dyes in Aqueous Medium
- A Rational Study of the Origin and Generality of Anti-Enthalpy–Entropy Compensation (AEEC) Phenomenon
- Molecular Interactions Investigation of L-Histidine in Water and in Aqueous Citric Acid at Different Temperatures Using Volumetric and Acoustic Methods
- Effect of Acid on Surface Hydroxyl Groups on Kaolinite and Montmorillonite
- In situ Synthesis of Reduced Graphene Oxide Supported CoMo Nanoparticles as Efficient Catalysts for Hydrogen Generation from NH3BH3
Articles in the same Issue
- Frontmatter
- Uniform Airy Approximation for Nonadiabatic Transitions in a Curve-Crossing Weak-Coupling Case
- Microwave Accelerated Green Synthesis of Gold Nanoparticles Using Gum Arabic and their Physico-Chemical Properties Assessments
- Electrochemical Sensor for the Determination of Paracetamol at Carbamazepine Film Coated Carbon Paste Electrode
- Green Synthesis of CoFe2O4 and Investigation of its Catalytic Efficiency for Degradation of Dyes in Aqueous Medium
- A Rational Study of the Origin and Generality of Anti-Enthalpy–Entropy Compensation (AEEC) Phenomenon
- Molecular Interactions Investigation of L-Histidine in Water and in Aqueous Citric Acid at Different Temperatures Using Volumetric and Acoustic Methods
- Effect of Acid on Surface Hydroxyl Groups on Kaolinite and Montmorillonite
- In situ Synthesis of Reduced Graphene Oxide Supported CoMo Nanoparticles as Efficient Catalysts for Hydrogen Generation from NH3BH3