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Indentation creep behavior of Fe–8Ni–xZr oxide dispersion strengthened alloys

  • Mustafa Tekin

    Mustafa Tekin completed his BSc degree at İstanbul Technical University, İstanbul, in 2014 and MSc degree at İstanbul Technical University, İstanbul, in 2017. He received his PhD degree in Mechanical Engineering from Necmettin Erbakan University, Konya, Turkey, in 2022. He is working as an Assistant Professor at KTO Karatay University in Konya. His research interests are mechanical alloying, thermal stability, high entropy alloys, material testing, nanoindentation, and nanocrystalline metals.

     ORCID logo     , Faiz Muhaffel

    Faiz Muhaffel completed his BSc degree at İstanbul Technical University, İstanbul, in 2008 and MSc degree at İstanbul Technical University, İstanbul, in 2010. He received his PhD degree in Materials Science and Engineering at İstanbul Technical University, İstanbul, Turkey, in 2021. His research interests are metallurgical engineering, wear behavior of materials, micro arc oxidation, nanoindentation, and material testing.

     ORCID logo     , Hasan Kotan

    Professor Hasan Kotan completed his BSc degree at Sakarya University, Sakarya, in 2006 and MSc degree at University of Pittsburgh, Pennsylvania, in 2010. He received his PhD degree in Materials Science and Engineering from North Carolina State University, North Carolina, USA, in 2013. His research interests are nanocrystalline metals, stainless steel, thermal stability, mechanical alloying, and thermal stability.

     ORCID logo     and Murat Baydoğan

    Professor Murat Baydoğan completed his BSc degree at İstanbul Technical University, Sakarya Engineering Faculty, Sakarya, in 1992 and MSc degree at İstanbul Technical University, İstanbul, in 1996. He received his PhD degree in Materials Science and Engineering at İstanbul Technical University, İstanbul, Turkey, in 2003. He is working as a professor at Istanbul Technical University. His research interests are metallurgical and materials engineering, wear behavior of materials, micro arc oxidation, microstructural characterization of materials, nanoindentation, and material testing.

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Published/Copyright: July 20, 2023
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Materials Testing
From the journal Materials Testing Volume 65 Issue 9

Abstract

This study was conducted to understand the creep behavior of two oxide dispersion strengthened alloys containing Zr as the alloying addition by performing indentation creep tests at room temperature. The oxide dispersion strengthened alloys were Fe–8Ni–xZr (x = 1 and 4 at.%, i.e., Zr-1 and Zr-4 alloys, respectively), which had been previously fabricated by mechanical alloying; followed by consolidation via equal channel angular extrusion at 1000 °C. The indentation tests were conducted under a maximum load of 100 mN with the loading rates at 300 and 400 mN min−1. The hardness was calculated by the Oliver–Pharr method, and the creep properties, such as the creep displacement, creep strain rate, creep stress, and stress exponent n, were determined. The results showed that the Zr-4 alloy was harder than the Zr-1 alloy. However, the creep resistance of the Zr-1 alloy was better than that of the Zr-4 alloy. It was further demonstrated that both the hardness and creep resistance depended on the loading rate. Moreover, a possible creep mechanism was proposed. Although the tests were performed at room temperature, they can provide insight into the effect of an oxide dispersion strengthened alloys microstructure on creep at higher temperatures.

Keywords: creep mechanism; equal channel angular extrusion; indentation creep; oxide dispersion strengthened alloys; powder metallurgy; Zr content
Corresponding author: Murat Baydoğan, Department of Metallurgical and Materials Engineering, Istanbul Technical University, 34469 Maslak, İstanbul, Türkiye, E-mail:

About the authors

Mustafa Tekin

Mustafa Tekin completed his BSc degree at İstanbul Technical University, İstanbul, in 2014 and MSc degree at İstanbul Technical University, İstanbul, in 2017. He received his PhD degree in Mechanical Engineering from Necmettin Erbakan University, Konya, Turkey, in 2022. He is working as an Assistant Professor at KTO Karatay University in Konya. His research interests are mechanical alloying, thermal stability, high entropy alloys, material testing, nanoindentation, and nanocrystalline metals.

Faiz Muhaffel

Faiz Muhaffel completed his BSc degree at İstanbul Technical University, İstanbul, in 2008 and MSc degree at İstanbul Technical University, İstanbul, in 2010. He received his PhD degree in Materials Science and Engineering at İstanbul Technical University, İstanbul, Turkey, in 2021. His research interests are metallurgical engineering, wear behavior of materials, micro arc oxidation, nanoindentation, and material testing.

Hasan Kotan

Professor Hasan Kotan completed his BSc degree at Sakarya University, Sakarya, in 2006 and MSc degree at University of Pittsburgh, Pennsylvania, in 2010. He received his PhD degree in Materials Science and Engineering from North Carolina State University, North Carolina, USA, in 2013. His research interests are nanocrystalline metals, stainless steel, thermal stability, mechanical alloying, and thermal stability.

Murat Baydoğan

Professor Murat Baydoğan completed his BSc degree at İstanbul Technical University, Sakarya Engineering Faculty, Sakarya, in 1992 and MSc degree at İstanbul Technical University, İstanbul, in 1996. He received his PhD degree in Materials Science and Engineering at İstanbul Technical University, İstanbul, Turkey, in 2003. He is working as a professor at Istanbul Technical University. His research interests are metallurgical and materials engineering, wear behavior of materials, micro arc oxidation, microstructural characterization of materials, nanoindentation, and material testing.

Acknowledgment

The authors are particularly indebted to Dr. Kris A. Darling for conducting ECAE.

  1. Author contributions: All the authors have accepted responsibility for the entire content of this submitted manuscript and approved submission.

  2. Research funding: None declared.

  3. Competing interests: On behalf of all authors, the corresponding author states that there is no conflict of interest.

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Published Online: 2023-07-20
Published in Print: 2023-09-26

© 2023 Walter de Gruyter GmbH, Berlin/Boston

Articles in the same Issue

  1. Frontmatter
  2. Experimental evidence of hydrogen evolution from local anodic corrosion sites and its consequences for corrosion cracking mechanisms
  3. Weldability and mechanical behavior of CMT welded AISI 430 and HARDOX 500 steels
  4. Mechanical properties and microstructural features of rotary friction welded UNS S42000 martensitic stainless-steel joints
  5. Decarburization effects on high-cycle fatigue of uncoated press hardened steels
  6. Non-destructive detection for mosaic ceramic surface defects based on convolutional neural networks
  7. Low-velocity impact behaviours of sandwiches manufactured from fully carbon fiber composite for different cell types and compression behaviours for different core types
  8. Microstructural and numerical variation of friction spot welded AA7075 couples
  9. Crushing performance and optimization of bio-inspired multi-cell columns
  10. Collapse of a honeycomb sandwich composite in an aircraft radome
  11. A multi-strategy boosted prairie dog optimization algorithm for global optimization of heat exchangers
  12. Indentation creep behavior of Fe–8Ni–xZr oxide dispersion strengthened alloys
  13. Mechanical and tribological behavior of a hybrid WC and Al2O3 reinforced Al–4Gr composite
  14. Effect of vibration and cutting zone temperature on surface topography during hybrid cooling/lubrication assisted machining of Vanadis 10
  15. Thermal and mechanical properties of a new insulation composite material
https://doi.org/10.1515/mt-2023-0030
Keywords for this article
creep mechanism; equal channel angular extrusion; indentation creep; oxide dispersion strengthened alloys; powder metallurgy; Zr content

Articles in the same Issue

  1. Frontmatter
  2. Experimental evidence of hydrogen evolution from local anodic corrosion sites and its consequences for corrosion cracking mechanisms
  3. Weldability and mechanical behavior of CMT welded AISI 430 and HARDOX 500 steels
  4. Mechanical properties and microstructural features of rotary friction welded UNS S42000 martensitic stainless-steel joints
  5. Decarburization effects on high-cycle fatigue of uncoated press hardened steels
  6. Non-destructive detection for mosaic ceramic surface defects based on convolutional neural networks
  7. Low-velocity impact behaviours of sandwiches manufactured from fully carbon fiber composite for different cell types and compression behaviours for different core types
  8. Microstructural and numerical variation of friction spot welded AA7075 couples
  9. Crushing performance and optimization of bio-inspired multi-cell columns
  10. Collapse of a honeycomb sandwich composite in an aircraft radome
  11. A multi-strategy boosted prairie dog optimization algorithm for global optimization of heat exchangers
  12. Indentation creep behavior of Fe–8Ni–xZr oxide dispersion strengthened alloys
  13. Mechanical and tribological behavior of a hybrid WC and Al2O3 reinforced Al–4Gr composite
  14. Effect of vibration and cutting zone temperature on surface topography during hybrid cooling/lubrication assisted machining of Vanadis 10
  15. Thermal and mechanical properties of a new insulation composite material
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