Oxidation Behavior at 1173 K of Modified P/M Stainless Steel 316 L by Addition of Cr, Ni, and Cr with Ni
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Yada Polsen
Yada Polsen, born in 1987, received her Bachelor’s and Master’s degrees from the Department of Metallurgical Engineering, Chulalongkorn University, Bangkok, Thailand in 2010 and 2013, respectively. She joined the TTCL Public Company Limited, Bangkok, Thailand as a quality control engineer and has been working now as a Quality Assurance Assistant for the Sumitomo Corporation. Her research interest focuses on the development and characterization of nickel-based superalloys.
Dr. Panyawat Wangyao, born in 1971, is an Assistant Professor and a Member of the Innovative Metals Research Unit, Department of Metallurgical Engineering, Chulalongkorn University, Bangkok, Thailand. He served as Head of the Department of Metallurgical Engineering, Faculty of Engineering, Chulalongkorn University, Bangkok, Thailand from 2011 to 2015. He received his Ph.D. in Physical Metallurgy from the Technical University of Kosice, Slovakia, in 2002. His research areas of expertise include high temperature materials such as superalloys, super stainless steel as well as powder metallurgy of alloys.
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Nutthita Chuankrerkkul
Dr. Nutthita Chuankrerkkul, Ph.D., born in 1975, is an Associate Professor at the Metallurgy and Materials Science Research Institute, Chulalongkorn University, Thailand. She received her Bachelor’s degree in Materials Science and a Master’s degree in Ceramic Technology both from Chulalongkorn University and received a Ph.D. in Engineering Materials from the University of Sheffield, United Kingdom. Her research interest is particulate materials processing, especially in powder injection molding of metals, ceramics, and composites.
Dr. Patama Visuttipitukul, born in 1977, is an Associate Professor at the Department of Metallurgical Engineering, Faculty of Engineering, Chulalongkorn University, Bangkok, Thailand. She received her Doctoral degree from the Department of Metallurgical Engineering, University of Tokyo, Japan. Her expertise includes materials characterization and surface engineering.
Dr. Ruangdaj Tongsri, born in 1966, is a Principal Researcher and Lab Head at the Particulate Materials Processing Technology (PMPT) group of the National Metal and Materials Technology Center (MTEC), Pathum Thani, Thailand. He received his Ph.D. from Department of Materials at the Imperial College of London, UK in 2000. His expertise areas include powder metallurgy and physical metallurgy.
Dr.-Ing. Gobboon Lothongkum, born in 1960, is a Professor and a Member of the Innovative Metals Research Unit, Department of Metallurgical Engineering, Faculty of Engineering, Chulalongkorn University, Bangkok, Thailand. He received a Dr.-Ing. degree from the Helmut Schmidt-University/ University of the Federal Armed Forces Hamburg, Germany, and an International Welding Engineer Certificate from the International Institute of Welding in 1994 and 2006, respectively. He served as Head of Department from 2015 to 2019. His areas of expertise include corrosion of metals and alloys, welding and metal joining, stainless steel.
Abstract
Specimens of P/M 316 L stainless steel and modified P/M 316 L stainless steel with various amounts of Cr, Ni, and Cr along with Ni additions were compressed by a 500 MPa-hydraulic press for a duration of 30 s and then sintered at 1573 K in a hydrogen atmosphere for 2.7 ks. The oxidation resistance tests of those specimens were carried out at 1173 K in air for 360 ks. The 5 wt.-% Cr-added specimen resulted in the best oxidation resistance with the lowest oxidation rate constant of 1.54 × 10-7 kg2 × m-4 × s-1. The oxidation products which formed inside the pores and on the surfaces of all specimens were analyzed using scanning electron microscope/energy dispersive spectroscopic (SEM/EDS) and X-ray diffraction (XRD) analysis techniques. The results show that the oxides forming on both inside pores and surfaces were identified as Cr2O3, Fe2O3, (Fe0.6Cr0.4)2O3, NiFe2O4 and NiCr2O4 in all tested conditions. The measured hardness of the modified specimens was in the range of 87-92 HRB, compared to the hardness of the 316 L specimen, which was 93 HRB. Increasing the amount of powder added provided a slightly lower hardness value due to increased porosity.
About the authors
Yada Polsen, born in 1987, received her Bachelor’s and Master’s degrees from the Department of Metallurgical Engineering, Chulalongkorn University, Bangkok, Thailand in 2010 and 2013, respectively. She joined the TTCL Public Company Limited, Bangkok, Thailand as a quality control engineer and has been working now as a Quality Assurance Assistant for the Sumitomo Corporation. Her research interest focuses on the development and characterization of nickel-based superalloys.
Dr. Panyawat Wangyao, born in 1971, is an Assistant Professor and a Member of the Innovative Metals Research Unit, Department of Metallurgical Engineering, Chulalongkorn University, Bangkok, Thailand. He served as Head of the Department of Metallurgical Engineering, Faculty of Engineering, Chulalongkorn University, Bangkok, Thailand from 2011 to 2015. He received his Ph.D. in Physical Metallurgy from the Technical University of Kosice, Slovakia, in 2002. His research areas of expertise include high temperature materials such as superalloys, super stainless steel as well as powder metallurgy of alloys.
Dr. Nutthita Chuankrerkkul, Ph.D., born in 1975, is an Associate Professor at the Metallurgy and Materials Science Research Institute, Chulalongkorn University, Thailand. She received her Bachelor’s degree in Materials Science and a Master’s degree in Ceramic Technology both from Chulalongkorn University and received a Ph.D. in Engineering Materials from the University of Sheffield, United Kingdom. Her research interest is particulate materials processing, especially in powder injection molding of metals, ceramics, and composites.
Dr. Patama Visuttipitukul, born in 1977, is an Associate Professor at the Department of Metallurgical Engineering, Faculty of Engineering, Chulalongkorn University, Bangkok, Thailand. She received her Doctoral degree from the Department of Metallurgical Engineering, University of Tokyo, Japan. Her expertise includes materials characterization and surface engineering.
Dr. Ruangdaj Tongsri, born in 1966, is a Principal Researcher and Lab Head at the Particulate Materials Processing Technology (PMPT) group of the National Metal and Materials Technology Center (MTEC), Pathum Thani, Thailand. He received his Ph.D. from Department of Materials at the Imperial College of London, UK in 2000. His expertise areas include powder metallurgy and physical metallurgy.
Dr.-Ing. Gobboon Lothongkum, born in 1960, is a Professor and a Member of the Innovative Metals Research Unit, Department of Metallurgical Engineering, Faculty of Engineering, Chulalongkorn University, Bangkok, Thailand. He received a Dr.-Ing. degree from the Helmut Schmidt-University/ University of the Federal Armed Forces Hamburg, Germany, and an International Welding Engineer Certificate from the International Institute of Welding in 1994 and 2006, respectively. He served as Head of Department from 2015 to 2019. His areas of expertise include corrosion of metals and alloys, welding and metal joining, stainless steel.
Acknowledgement
This work was supported by THE 90th ANNIVERSARY OF CHULALONGKORN UNIVERSITY FUND (Ratchadaphiseksomphot Endowment Fund). The authors express their gratitude to M. Morakotjinda, National Metal and Materials Technology Center (MTEC), A. Thueploy, Metallurgy and Materials Science Research Institute, Chulalongkorn University and O. Srihakulung, Defense Technology Institute (DTI), Thailand, for their assistance and use of equipment.
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Articles in the same Issue
- Frontmatter
- Mechanical testing
- Application of 3D digital image correlation for the measurement of the tensile mechanical properties of high-strength steel
- Mechanical testing/production-oriented testing/materialography
- Comparative study of thermoplastic liner materials with regard to mechanical and permeation barrier properties before and after cyclic thermal aging
- Oxidation Behavior at 1173 K of Modified P/M Stainless Steel 316 L by Addition of Cr, Ni, and Cr with Ni
- Mechanical testing/Analysis of physical properties
- Effect of graphene nanoplatelet filling on mechanical properties of natural fiber reinforced polymer composites
- Fatigue testing/Numerical simulations
- Fatigue life evaluation of an electrically driven shuttle frame using finite element analysis
- Component-oriented testing and simulation
- Conceptual comparison of the ecogeography-based algorithm, equilibrium algorithm, marine predators algorithm and slime mold algorithm for optimal product design
- Fracture mechanics testing/numerical simulations
- Thermo-mechanical analysis of a FGM plate subjected to thermal shock – A new numerical approach considering real time temperature dependent material properties
- Mechanical testing/materialography/chemical resistance testing
- Mechanical properties of Al-Cu/B4C and Al-Mg/B4C metal matrix composites
- Component-oriented testing and simulation
- Comparision of the political optimization algorithm, the Archimedes optimization algorithm and the Levy flight algorithm for design optimization in industry
- Materialography
- Surface modification of a magnesium alloy by electrical discharge coating with a powder metallurgy electrode
- Materialography
- Characterization of mechanically alloyed Fe based and MoNiAl+Al2O3 reinforced composites
- Mechanical testing/Chemical resistance testing
- Optimization of flexural and impact properties of r-LDPE-DPWF composite for printer parts production
- Component-oriented testing and simulation
- Evaluation methods for estimation of Weibull parameters used in Monte Carlo simulations for safety analysis of pressure vessels
- Materials testing for welding and additive manufacturing applications
- Comparison of ANN and RSM modeling approaches for WEDM process optimization
