Home Physical Sciences Process optimization of chili flavor beef tallow and analysis of its volatile compounds by GC-IMS
Article
Licensed
Unlicensed Requires Authentication

Process optimization of chili flavor beef tallow and analysis of its volatile compounds by GC-IMS

  • , , , , , , , and EMAIL logo
Published/Copyright: June 11, 2021

Abstract

With chili and liquid beef tallow as the main raw materials, the processing conditions of chili flavor beef tallow were explored. Gas chromatograpy-ion mobility spectrometry (GC-IMS) was used to determine the volatile compounds in chili flavor beef tallow. The capsaicin and dihydrocapsaicin in chili flavor beef tallow were determined by high performance liquid chromatography (HPLC). The optimum technological conditions were determined, and the index of chromatic aberration, cholesterol was also determined. Based on GC-IMS analysis, 102 kinds of volatile compounds were detected, and the sample III (the ratio of solid–liquid was 1:5, the frying temperature was 120 °C, and the frying time was 15 min) performed better than other samples. The preparation of chili beef tallow improves its antioxidant activity and makes its aroma more intense and more in line with the taste of Chinese people, which provides a theoretical and practical basis for the development of spice beef tallow in the future.


Corresponding author: Xinyi He, College of Food Science and Biological Engineering, Tianjin Agricultural University, Tianjin300392, China, E-mail:
Hang Li and Jiamin Liu contributed to the work equally and are regarded as co-first authors.

Funding source: Foundation of Tianjin Science and Technology Major Project

Award Identifier / Grant number: 18ZXYENC00120

Funding source: Tianjin Technical Expert Project

Award Identifier / Grant number: 19JCTPJC59900

Award Identifier / Grant number: 2020KJ090

Acknowledgments

The project supported by the Foundation of Tianjin Science and Technology Major Project (No. 18ZXYENC00120), Tianjin Technical Expert Project (No. 19JCTPJC59900), and Tianjin Municipal Education Commission Research Project (No.2020KJ090) are gratefully acknowledged.

  1. Author contributions: Xinyi He conducted the research. Zhanzhong Wang, Xiaodong Liu, Xichun Yan analyzed the data, Shoushan Liu, Xu Li, and Zhenyu Liao provided the formal analysis.

  2. Research funding: The project was supported by the Foundation of Tianjin Science and Technology Major Project (No. 18ZXYENC00120), Tianjin Technical Expert Project (No. 19JCTPJC59900), and Tianjin Municipal Education Commission Research Project (No. 2020KJ090).

  3. Conflict of interest statement: The authors declare no conflicts of interest regarding this article.

References

1. Baba, VY, Powell, AF, Ivamoto-Suzuki, ST, Pereira, LF, Vanzela, AL, Giacomin, RM, et al.. Capsidiol-related genes are highly expressed in response to Colletotrichum scovillei during Capsicum annuum fruit development stages. Sci Rep 2020;10:1267–74. https://doi.org/10.1038/s41598-020-68949-5.Search in Google Scholar PubMed PubMed Central

2. Shah, NA, Prasad, RV, Patel, BB. Optimization of supercritical fluid extraction of Paprika (cv. Reshampatti) oil, capsaicin and pigments. Flavour Fragrance J 2020;35:469–77. https://doi.org/10.1002/ffj.3579.Search in Google Scholar

3. Xie, JH, Ye, WW, Pang, J, Cai, XH. Research progress of deep processing technology of chili. J Chin Capsicum 2004;2:28–31.Search in Google Scholar

4. Sun, J, Sun, BG, Ren, FZ, Chen, H, Zhang, V, Zhang, Y. Characterization of key odorants in Hanyuan and Hancheng fried pepper (Zanthoxylum bungeanum) oil. J Agric Food Chem 2020;68:6403–11. https://doi.org/10.1021/acs.jafc.0c02026.Search in Google Scholar PubMed

5. Zhang, HX, Liu, H, Chen, GJ, Kan, J. Study on the quality of chili oil products from different chili varieties different chili oil products. Food Ferment Ind 2019;45:190–8.Search in Google Scholar

6. Liu, YM, Wu, YJ, Wang, YJ, Tang, X. Analysis of volatile compounds in Guizhou oil chili. Food Sci 2013;34:221–7.Search in Google Scholar

7. Chen, D, Huang, YQ, He, XM, Shi, ZG, Feng, YQ. Coupling carbon nanotube film microextraction with desorption corona beam ionization for rapid analysis of Sudan dyes (I–IV) and rhodamine B in chili oil. Analyst 2015;140:1731–8. https://doi.org/10.1039/c4an02044h.Search in Google Scholar PubMed

8. An, ZL. Research status of chili oil processing and production. chili J 2006;3:45–8.Search in Google Scholar

9. Fei, WY. Solvent extraction for the 21st century. Chem Ind Eng Prog 2001;19:11–3.Search in Google Scholar

10. Abdalla Adel, A, Afify, AS, Hasaan, IE. Studying the effect of household-type treatment and processing on the residues of ethion and profenofos pesticides and on the contents of capsaicinoids in green chili pepper using GC-MS/MS and HPLC. Food Anal Methods 2018;11:382–93. https://doi.org/10.1007/s12161-017-1009-9.Search in Google Scholar

11. Xue, M, He, XY, Yan, XC. Study on the preparation of chili chicken oil. Food Res Dev 2019;40:120–4. https://doi.org/10.1177/0379572118811442.Search in Google Scholar PubMed

12. Schwolow, S, Gerhardt, N, Rohn, S, Weller, P. Data fusion of GC-IMS data and FT-MIR spectra for the authentication of olive oils and honeys—is it worth to go the extra mile? Anal Bioanal Chem 2019;411:6005–19. https://doi.org/10.1007/s00216-019-01978-w.Search in Google Scholar PubMed

13. Wang, WG, Liang, XX, Cheng, SS, Chen, C, Wen, M, Peng, L, et al.. Development of ion mobility spectrometry and its application for detection trace explosives. Chin Sci Bull 2014;59:1079–86. https://doi.org/10.1007/s11434-014-0671-1.Search in Google Scholar

14. Zhou, CX, Zheng, FP, Sun, BG. Application of ion mobility spectrometry in food flavor analysis. Food Ind Sci Technol 2019;40:309–18.Search in Google Scholar

15. Wang, YY, Zhang, ZY, Sun, J, Chang, YF, Lv, F, Ding, YT, et al.. Analysis of flavor changes of brown rice during storage based on gas chromatography-ion mobility spectrometry. Food Ferment Ind 2020;46:250–5.Search in Google Scholar

16. Meng, XT, Qiao, X, Pan, Y, Zou, SP, Zhang, T, Zhang, Q. Characteristic flavor compounds fingerprinting of mutton from different producing regions of Xinjiang, China by gas chromatography-ion mobility spectrometry. Food Sci 2020;41:218–26.Search in Google Scholar

17. Du, P, Chen, ZJ, Yang, F, Li, XL, Yang, J, Liu, CX, et al.. A rapid method for the discrimination of different varieties of green coffee beans by headspace-gas chromatography-ion mobility spectrometry. Food Sci 2019;40:228–33.Search in Google Scholar

18. Yang, F, Yang, L, Xu, LD. Flavor analysis of Capsicum frutescens L. sauce based on electronic nose and gas chromatograph-ion mobility spectrometer (GC-IMS). Sci Tech Food Ind 2019;40:193–8.Search in Google Scholar

19. Chen, T, Lu, DL, Chen, B. Application of headspace/gas chromatography-tandem ion mobility spectrometry with chemometrics in classification of edible vegetable oils. J Instrum Anal 2017;36:1235–9.Search in Google Scholar

20. Yang, L, Li, Y. The research for nutritional value and application of refining pure chicken fat. China Con 2012;37:60–3. https://doi.org/10.1111/oet.12022_7.Search in Google Scholar

21. Yao, D. Research on the preparation of Chili flavor blending Tallow and its Quality analysis. Tianjin: Tianjin Agricultural University; 2018.Search in Google Scholar

22. Liu, JM. Research of beef tallow fractionation and preparation of low-melting Chili flavor oil. Tianjin: Tianjin Agricultural University; 2020.Search in Google Scholar

23. Zhang, XR. Determination of cholesterol content in Inner Mongolia Livestock meat and comparison of two detection methods. Hohhot: Inner Mongolia Agricultural University; 2017.Search in Google Scholar

24. Zhang, QB. Study on Determination of cholesterol content in food by gas chromatography mass spectrometry. Changchun: Jilin University; 2013.Search in Google Scholar

25. Wang, GL, Zhang, SX, Pan, NK, Luo, Q. Clinical research progress of small and dense low density lipoprotein cholesterol. Lab Med Clin 2015;12:1804–6.Search in Google Scholar

26. Pino, JA, Barzola-Miranda, SE. Characterization of odor-active compounds in pechiche (Vitex cymosa Berteo ex Speng) fruit. J Raw Mater Process Foods 2020;1:33–9.Search in Google Scholar

Received: 2020-09-29
Accepted: 2021-05-29
Published Online: 2021-06-11

© 2021 Walter de Gruyter GmbH, Berlin/Boston

Downloaded on 31.3.2026 from https://www.degruyterbrill.com/document/doi/10.1515/ijfe-2020-0246/html
Scroll to top button