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Biodiesel production from waste cooking oil using Indion-140 catalyst: optimization studies

  • Mallaiah Mekala EMAIL logo , Prasad Babu Koorla , Ramesh Kola , Bhavani Pokala , Anwar Shaik , Sai Mani Yogesh Kosuru and Yashraj Delhiwala
Published/Copyright: July 31, 2025
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Abstract

Heterogeneous transesterification of Waste Cooking Palm Oil (WCPO) to biodiesel over ion exchange resin solid acid catalyst, Indion-140 in a batch reactor and the optimization of the process conditions have been investigated. The reaction is conducted under various parameters like temperature in the range of 40 °C–80 °C, catalyst loading in the range of 1 g/cc – 5 g/cc based on volume of reaction mixture and mole ratios of reactants in the range of 1:1 – 1:10. The experimental design of the influencing parameters is modeled by using Central Composite Design (CCD) with Response Surface Methodology (RSM). The experiments are performed as per the combinations of influencing parameters designed by aforementioned CCD methodology. The experimental data used the power law regression in a quadratic model. An ANN was trained on the experimental data. ANOVA is used to test the regression model for biodiesel yield. The maximum biodiesel yield achieved was 86.63 % experimentally, while the model predicted a yield of 79.243 % under optimal conditions.


Corresponding author: Mallaiah Mekala, Department of Chemical Engineering, Chaitanya Bharathi Institute of Technology, Hyderabad 500075, India, E-mail:

Award Identifier / Grant number: IH/1048/Chemical/D008/2024

Acknowledgments

The authors would like acknowledge Chaitanya Bharathi Institute of Technology, Hyderabad for providing the funding to carry out the research work at Institute.

  1. Research ethics: Not applicable.

  2. Informed consent: Not applicable.

  3. Author contributions: The authors have accepted responsibility for the entire content of this manuscript and approved its submission.

  4. Use of Large Language Models, AI and Machine Learning Tools: No.

  5. Conflict of interest: The authors declare no conflict of interests.

  6. Research funding: This work was supported by Chaitanaya Bharthi Institute of Technology, Hyderabad Project No. CBIT/PROJ-IH/1048/Chemical/D008/2024 under grant IH/1048/Chemical/D008/2024.

  7. Data availability: None declared.

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Received: 2025-02-28
Accepted: 2025-06-23
Published Online: 2025-07-31

© 2025 Walter de Gruyter GmbH, Berlin/Boston

Downloaded on 11.9.2025 from https://www.degruyterbrill.com/document/doi/10.1515/cppm-2025-0040/pdf
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