Analytical chemistry of engineered nanomaterials: Part 2. analysis in complex samples (IUPAC Technical Report)
Ján Labuda, Jiří Barek, Zuzana Gajdosechova, Silvana Jacob, Linda Johnston, Petra Krystek, Zoltan Mester, Josino Moreira, Veronika Svitkova and Kevin J. Wilkinson
Pure and Applied Chemistry, 2023
Vol. 95, no. 11, pp. 1159-1196
https://doi.org/10.1515/pac-2022-0401
Recently, the scope, regulation, legislation, and metrology of the analytical chemistry of engineered nanomaterials (ENMs) have been reviewed in the Part 1 of the IUPAC Technical Report (PAC vol. 95, no. 2, 2023, pp. 133-163). Chemical analysis of nanomaterials in complex sample matrices presents a substantial challenge for analytical science and regulatory agencies. The purpose of the present Part 2 is to discuss the detection, characterization, and quantification of nanomaterials in samples of complex matrices including methods for sample preparation and fitness for purpose. Analytical methods applied to analysis in matrices of environmental samples, food, cosmetics, and biological samples as well as those used to monitor the fate of ENMs in the environment and biological systems are reported. Tables of numerous recently published works on analyses of typical ENMs with detailed protocols and conclusive comments are presented. There is a rapid development in the field mostly in the stage of accumulation of factual material. The single-particle inductively coupled plasma mass spectrometry is already widely used at the chemical analysis of metal-containing nanoparticles.
© 2024 IUPAC & De Gruyter
This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International License.
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