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Synthesis, crystal structure and electrochemical behaviour of [2,6-bis(3,5-dimethylpyrazolyl)pyridine](dithiocyanato)cobalt(II)
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C. Arıcı
Published/Copyright:
September 25, 2009
Abstract
A mononuclear cobalt(II) complex, [Co(dmpp)(SCN)2], was synthesized using 2,6-bis (3,5-dimethylpyrazolyl)pyridine (dmpp) and thiocyanate anion (SCN), and characterized by IR spectroscopy and single-crystal X-ray diffraction. In addition, cyclic voltammetric studies have been performed. The complex crystalizes in monoclinic space group C 2/c, with unit cell dimensions a = 15.2469(15), b = 9.1120(9), c = 14.0302(11) Å, β = 95.823(3)°. The cell containes 4 molecules.
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Published Online: 2009-9-25
Published in Print: 2003-7-1
© 2003 Oldenbourg Wissenschaftsverlag GmbH
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