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Synthesis, structural and spectral studies of N-p-methylbenzyliden-N-phenyl-p,p′-dimethoxybenzoyl acetic acid hydrazide
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D. Ülkü
Published/Copyright:
September 25, 2009
Abstract
The structure of the organic derivative of N-p-methylbenzyliden-N-phenyl-p,p′-dimethoxybenzoyl acetic acid hydrazide, [C32H28N2O5], has been determined by X-ray diffraction. The structure derived from the NMR spectroscopy, the IR spectra and elemental analysis is consistent with that of the X-ray diffraction. The compound crystalizes in the monoclinic system with space group P21/c, a = 16.234(1), b = 9.399(2), c = 19.389(1), β = 110.924(3)°, V = 2763.3(5) Å3 and Z = 4. In the crystal, there is one weak C—H…O type intermolecular hydrogen bond interaction.
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Published Online: 2009-9-25
Published in Print: 2003-5-1
© 2003 Oldenbourg Wissenschaftsverlag GmbH
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Articles in the same Issue
- Solution of the structure and disorder of Ln13Br18B3 (Ln = Gd, Tb)
- Anomalous thermal expansion behaviour of Na8[AlSiO4]6(NO3)2-sodalite: P4̅3n to Pm3̅n phase transition by untilting and contraction of TO4 units
- Crystal structure of new hexahydrate dicobalt pyrophosphate Co2P2O7·6H2O: comparison with Co2P2O72H2O, α-, β- and γ-Co2P2O7
- Crystal structures and Raman spectra of Cu(OH)F and Cu3(OH)2F4
- Crystal chemistry of lead oxide phosphates: crystal structures of Pb4O(PO4)2, Pb8O5(PO4)2 and Pb10(PO4)6O
- Structural distortion of the α, β, and γ polymorphs of glycine on cooling
- Synthesis, structural and spectral studies of N-p-methylbenzyliden-N-phenyl-p,p′-dimethoxybenzoyl acetic acid hydrazide
- Crystal structure of an inclusion complex between chiral monoaza-15-crown-5 and S(–)-1-phenyl-ethyl ammonium percholorate
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