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Synthesis, structural and spectral studies of N-p-methylbenzyliden-N-phenyl-p,p′-dimethoxybenzoyl acetic acid hydrazide

  • D. Ülkü , C. Arıcı , F. Ercan , M. Saçmacı , E. Sarıpınar and Y. Akçamur
Published/Copyright: September 25, 2009

Abstract

The structure of the organic derivative of N-p-methylbenzyliden-N-phenyl-p,p′-dimethoxybenzoyl acetic acid hydrazide, [C32H28N2O5], has been determined by X-ray diffraction. The structure derived from the NMR spectroscopy, the IR spectra and elemental analysis is consistent with that of the X-ray diffraction. The compound crystalizes in the monoclinic system with space group P21/c, a = 16.234(1), b = 9.399(2), c = 19.389(1), β = 110.924(3)°, V = 2763.3(5) Å3 and Z = 4. In the crystal, there is one weak C—H…O type intermolecular hydrogen bond interaction.

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Published Online: 2009-9-25
Published in Print: 2003-5-1

© 2003 Oldenbourg Wissenschaftsverlag GmbH

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