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Crystal growth of KPb2Cl5 by Bridgeman method with pressure control system
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Gang Cheng
Published/Copyright:
May 13, 2013
Abstract
⊙15 mm Single crystals of potassium lead chloride (KPb2Cl5) have been grown by a novel modified Bridgman method under protect of N2 and CCl4 with a pressure control system. It could make vacuum or protect atmosphere according to the need of raw materials composition and crystals growth. So the process of preparation of crystal would be simplified. Measurements of the transmission of crystal in the mid-infrared were also made.
Published Online: 2013-05-13
Published in Print: 2013-05
© by Oldenbourg Wissenschaftsverlag, München, Germany
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Articles in the same Issue
- Clathrates and semiclathrates of Type-I: crystal structure and superstructures
- Crystal growth of KPb2Cl5 by Bridgeman method with pressure control system
- Structures of a co-crystal of tautomers of (E)-N-7-chloro-4-(2-methoxycinnamolyhydrazinyl)quinoline and a single tautomer of the 4-methoxy analogue
- Amino acid hexafluorosilicates – an overview
- Association of combined features of amino acid and protein withcrystallization propensity of proteins from Cytophaga Hutchinsonii
- Crystal structure of 2-(4-methylphenyl)-2-oxo-1-(phenyliodonio)-1-(triphenylarsonio)ethanid tetrafluoroborate solved from X-ray powder data
