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Crystal structure of phenyl 1-hydroxy-2-naphthoate, an unexpected product from an attempted aryl aryl coupling reaction1

Published/Copyright: July 28, 2010
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Zeitschrift für Kristallographie - Crystalline Materials
From the journal Zeitschrift für Kristallographie - Crystalline Materials Volume 210 Issue 3

Abstract

The title compound was obtained as an unexpected by-product in the attempted biaryl coupling of phenyl 1-methoxy-2-naphthoate with 2-methoxy-1-naphthyl magnesium bromide. From ether/petroleum ether it crystallizes from the purified reaction mixture as colorless plates of the space group P21/a; a = 1258.7(5) pm, b = 1791.1(8) pm, c = 583.8(2) pm, and β = 93.68(3)°. The most characteristic feature of the structure is an intramolecular hydrogen bond quasi forming a fourth 6-membered nearly planar ring system.

Published Online: 2010-7-28
Published in Print: 1995-3-1

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Articles in the same Issue

  1. A new method for measuring absolute optical path differences without external compensation
  2. The crystallographic calculation of the elements of mechanical twinning in crystals
  3. Edge-bicolorings of regular polyhedra
  4. A comparison of powder diffraction studies of kaolin group minerals
  5. Crystal growth and reinvestigation of the crystal structure of crednerite, CuMnO2
  6. Die Kristallstruktur des Bleigermanats Pb11Ge3O17
  7. Hydrogen bonding in crystalline L-His H+ · H2PO4− · H2O
  8. The crystal structure of calcium glutarate monohydrate
  9. Structures cristallines du 4-bromo-2-méthoxy-1-méthyl-5-nitro et du 4-bromo-2-cyano-1-méthyl-5-nitroimidazoles obtenus par substitution nucléophile à partir du 2,4-dibromo-1-méthyl-5-nitroimidazole
  10. Crystal structures of 2-[bis(triphenylphosphine)silver(I)]benzisothiazol-3(2H)-one 1,1-dioxide and 2-[bis(triphenylphosphine)silver(I)]-4,5-dimethylisothiazol-3(2H)-one 1,1-dioxide · ethanol
  11. Crystal structure of phenyl 1-hydroxy-2-naphthoate, an unexpected product from an attempted aryl aryl coupling reaction1
  12. Polytypism of vapor grown PbI2 crystals
  13. Efficient use of measuring time on conventional diffractometers: a discussion document for practising crystallographers
  14. Redetermination of the crystal structure of manganese ultraphosphate, MnP4O11
  15. Crystal structure of tripotassium diselenoaurate(I), K3AuSe2
  16. Crystal structure of 2,3,4-triphenyl-5,7-difluor-8-(trans-stilbenyl)-2,3-dihydrocinnoline, C40H28F2N2
  17. Crystal structure of p-bis(tert-butyl-trimethylsiloxyl-methyliden-phosphino)-benzene,(C4H9C((CH3)3SiO)P)2C6H4
  18. Crystal structure of 7,8-dihydro-6H-dipyrido[1,2-a;2,1-c]-[1,4]-diazepinium bis(cis-1,2-dicyanoethene-1,2-dithiolato)nickelate, (C5H4N)2(CH2)3)(Ni(S2C2(CN)2)2
  19. Crystal structure of methyl-3-bis(trimethylsilyl)-amino-indolizine-2-carboxylate, CO2CH3(C8NH5)N(Si(CH3)3)2
  20. Crystal structure of tris(2,2′-bipyridyl)-zinc(II) Perchlorate, (Zn(C10H8N2)3)(ClO4)2
  21. Crystal structure of 1,8-bis(4-trifluoromethylphenyl)naphthalene, C24H14F6
  22. Crystal structure of α-amino-α-(2,6-dichlorophenyl)-cyclohexane-2,6-dione, C13H11Cl2NO2
  23. Crystal structure of (Z)-N-phthaloyl-2,3-dehydrophenylalanine methyl ester, C18H13NO4
  24. Crystal structure of (S)-2-pivaloylamino-3-(4′-hydroxyphenyl)-propionohydrazide, C14H21N3O3
  25. Crystal structure of 1-methoxycarbonyl-4-oxo-2-methyl-2-pentylidene-triphenylphosphorane, C26H25O3P
  26. Crystal structure of 1-acyl-4-oxo-hexylidene-triphenylphosphorane, C26H27O2P
  27. Crystal structure of 2,3,4,5-tetraphenyl-6-benzylidene-pyran, C36H26O
https://doi.org/10.1524/zkri.1995.210.3.210

Articles in the same Issue

  1. A new method for measuring absolute optical path differences without external compensation
  2. The crystallographic calculation of the elements of mechanical twinning in crystals
  3. Edge-bicolorings of regular polyhedra
  4. A comparison of powder diffraction studies of kaolin group minerals
  5. Crystal growth and reinvestigation of the crystal structure of crednerite, CuMnO2
  6. Die Kristallstruktur des Bleigermanats Pb11Ge3O17
  7. Hydrogen bonding in crystalline L-His H+ · H2PO4− · H2O
  8. The crystal structure of calcium glutarate monohydrate
  9. Structures cristallines du 4-bromo-2-méthoxy-1-méthyl-5-nitro et du 4-bromo-2-cyano-1-méthyl-5-nitroimidazoles obtenus par substitution nucléophile à partir du 2,4-dibromo-1-méthyl-5-nitroimidazole
  10. Crystal structures of 2-[bis(triphenylphosphine)silver(I)]benzisothiazol-3(2H)-one 1,1-dioxide and 2-[bis(triphenylphosphine)silver(I)]-4,5-dimethylisothiazol-3(2H)-one 1,1-dioxide · ethanol
  11. Crystal structure of phenyl 1-hydroxy-2-naphthoate, an unexpected product from an attempted aryl aryl coupling reaction1
  12. Polytypism of vapor grown PbI2 crystals
  13. Efficient use of measuring time on conventional diffractometers: a discussion document for practising crystallographers
  14. Redetermination of the crystal structure of manganese ultraphosphate, MnP4O11
  15. Crystal structure of tripotassium diselenoaurate(I), K3AuSe2
  16. Crystal structure of 2,3,4-triphenyl-5,7-difluor-8-(trans-stilbenyl)-2,3-dihydrocinnoline, C40H28F2N2
  17. Crystal structure of p-bis(tert-butyl-trimethylsiloxyl-methyliden-phosphino)-benzene,(C4H9C((CH3)3SiO)P)2C6H4
  18. Crystal structure of 7,8-dihydro-6H-dipyrido[1,2-a;2,1-c]-[1,4]-diazepinium bis(cis-1,2-dicyanoethene-1,2-dithiolato)nickelate, (C5H4N)2(CH2)3)(Ni(S2C2(CN)2)2
  19. Crystal structure of methyl-3-bis(trimethylsilyl)-amino-indolizine-2-carboxylate, CO2CH3(C8NH5)N(Si(CH3)3)2
  20. Crystal structure of tris(2,2′-bipyridyl)-zinc(II) Perchlorate, (Zn(C10H8N2)3)(ClO4)2
  21. Crystal structure of 1,8-bis(4-trifluoromethylphenyl)naphthalene, C24H14F6
  22. Crystal structure of α-amino-α-(2,6-dichlorophenyl)-cyclohexane-2,6-dione, C13H11Cl2NO2
  23. Crystal structure of (Z)-N-phthaloyl-2,3-dehydrophenylalanine methyl ester, C18H13NO4
  24. Crystal structure of (S)-2-pivaloylamino-3-(4′-hydroxyphenyl)-propionohydrazide, C14H21N3O3
  25. Crystal structure of 1-methoxycarbonyl-4-oxo-2-methyl-2-pentylidene-triphenylphosphorane, C26H25O3P
  26. Crystal structure of 1-acyl-4-oxo-hexylidene-triphenylphosphorane, C26H27O2P
  27. Crystal structure of 2,3,4,5-tetraphenyl-6-benzylidene-pyran, C36H26O
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