Home Structure of 2,6-di-(4-tert-butylphenyl)-4,4′-biphenyl-4H-pyran
Article
Licensed
Unlicensed Requires Authentication

Structure of 2,6-di-(4-tert-butylphenyl)-4,4′-biphenyl-4H-pyran

Published/Copyright: July 28, 2010
Become an author with De Gruyter Brill
Submit Manuscript Author Information
Zeitschrift für Kristallographie - Crystalline Materials
From the journal Zeitschrift für Kristallographie - Crystalline Materials Volume 209 Issue 4

Abstract

The title compound (C37H38O) belongs to the family 1-hetero-2,5-cyclohexadienes. The structure is triclinic, space group P[unk], with a = 11.576(5), b = 12.229(5), c = 12.305(5) Å, α = 68.52(3), β = 71.50(3), γ = 77.54(3)° and Z = 2. Three-dimensional intensity data collected on the SYNTEX P21 diffractometer using CuKα radiation at room temperature used for the structure determination and refinement. The final R value is 0.082 for 3713 observed reflections. Both tert-butyl groups are disordered as a result of their rotation around the C(phenyl)-C(tertbutyl) bond.

Published Online: 2010-7-28
Published in Print: 1994-4-1

© 2015 Oldenbourg Wissenschaftsverlag GmbH, Rosenheimer Str. 145, 81671 München

Articles in the same Issue

  1. Investigations on the directional solidification of the eutectic LiF–LiBaF3
  2. Electrostatic lattice-site energies of alkali feldspars in relation with Si/Al ordering
  3. Determination of the distribution coefficients of the rare earth ions Er3+ and Nd3+ in yttria-stabilized c-ZrO2 single crystals
  4. Videographic reconstructions and simulations of the real Cu3Au structure at various temperatures
  5. Structural phase transitions of rubidiumpolyphosphate, Rb2{∞1} [P2O6]
  6. Structure refinements of β-Si3N4 at temperatures up to 1360°C by X-ray powder investigation
  7. X-ray diffraction studies elucidating high temperature superconducting properties of YBa2Cu3O7−x thin films
  8. Positional and thermal disorder in the trigonal bipyramid of magnetoplumbite structure type SrGa12O19
  9. The crystal structure and changes of (NH4)1.4[Cu(NH3)2]0.3Br2 composition
  10. Crystal structure of FeAlPO5
  11. Synthesis, crystal growth and structure of KEu2[Si4O10]F
  12. Crystal structure of the bis(3-methyl-orotato)dimanganese(II) hexahydrate [Mn2(C6H4N2O4)2(H2O)6]
  13. Metal-betaine interactions. XVIII. Crystal structure of tetraaqua(trimethylammonioacetato)copper(III) sulfate trihydrate, [Cu(Me3NCH2CO2)(H2O)4](SO4) · 3H2O
  14. Structure of 2,6-di-(4-tert-butylphenyl)-4,4′-biphenyl-4H-pyran
  15. The crystal structure of 2-(5,7-dichloro-1-methyloxoindol)-3-spiro-1′(2′-benzoylhexahydropyrrolizin)-3′-spiro-2″-indian-1″,3″-dione
  16. The crystal and molecular structure of lisuride hydrogen maleate
  17. Structures of 6,9-dimethyl- and 6,9-diisopropyl-[2.2] (1,4)phenanthrenoparacyclophane
  18. Crystal structure of zirconium diphosphide, ZrP2
  19. Crystal structure of digadolinium monocarbide dichloride (1T type), Gd2CCl2
  20. Crystal structure of η5-cyclopentadienyl-1-titana-1-chloro-2,5-bis(p-methoxyphenyl)-2,5-diaza-cyclopent-3-ene, C21H21ClN2O2Ti
  21. Crystal structure of η5-cyclopentadienyl-1-titana-1-chloro-2,5-di(p-tolyl)-3,4-diphenyl-2,5-diaza-cyclopent-3-ene, C33H29ClN2Ti
  22. Crystal structure of 5-amino-3H-[1,3,4]thiadiazole-2-thione, C2H3N3S2
  23. Crystal structure of 4H,8H-2,3,6,7-tetrakis(methoxycarbonyl)thiopyrano-[3,2-b]thiopyrane-4,8-dione, C16H12O10S2
  24. Crystal structure of tetraethylammonium O-methyldithiocarbonate, C10H23NOS2
  25. Crystal structure of μ-N,N′-malodinitrile-bis(pentacarbonyltungsten) methylene chloride, C13H4Cl2N2O10W
  26. Crystal structure of ethylenediammonium hexafluorosilicate, [H3N(CH2)2NH3]SiF6
  27. Crystal structure of ethylenediammonium sulphate, [H3N(CH2)2NH3]SO4
  28. Crystal structure of ethylenediammonium copper sulphate, [H3N(CH2)2NH3]Cu(SO4)2(H2O)4
  29. Crystal structure of copper strontium (5/1), Cu5Sr
https://doi.org/10.1524/zkri.1994.209.4.357

Articles in the same Issue

  1. Investigations on the directional solidification of the eutectic LiF–LiBaF3
  2. Electrostatic lattice-site energies of alkali feldspars in relation with Si/Al ordering
  3. Determination of the distribution coefficients of the rare earth ions Er3+ and Nd3+ in yttria-stabilized c-ZrO2 single crystals
  4. Videographic reconstructions and simulations of the real Cu3Au structure at various temperatures
  5. Structural phase transitions of rubidiumpolyphosphate, Rb2{∞1} [P2O6]
  6. Structure refinements of β-Si3N4 at temperatures up to 1360°C by X-ray powder investigation
  7. X-ray diffraction studies elucidating high temperature superconducting properties of YBa2Cu3O7−x thin films
  8. Positional and thermal disorder in the trigonal bipyramid of magnetoplumbite structure type SrGa12O19
  9. The crystal structure and changes of (NH4)1.4[Cu(NH3)2]0.3Br2 composition
  10. Crystal structure of FeAlPO5
  11. Synthesis, crystal growth and structure of KEu2[Si4O10]F
  12. Crystal structure of the bis(3-methyl-orotato)dimanganese(II) hexahydrate [Mn2(C6H4N2O4)2(H2O)6]
  13. Metal-betaine interactions. XVIII. Crystal structure of tetraaqua(trimethylammonioacetato)copper(III) sulfate trihydrate, [Cu(Me3NCH2CO2)(H2O)4](SO4) · 3H2O
  14. Structure of 2,6-di-(4-tert-butylphenyl)-4,4′-biphenyl-4H-pyran
  15. The crystal structure of 2-(5,7-dichloro-1-methyloxoindol)-3-spiro-1′(2′-benzoylhexahydropyrrolizin)-3′-spiro-2″-indian-1″,3″-dione
  16. The crystal and molecular structure of lisuride hydrogen maleate
  17. Structures of 6,9-dimethyl- and 6,9-diisopropyl-[2.2] (1,4)phenanthrenoparacyclophane
  18. Crystal structure of zirconium diphosphide, ZrP2
  19. Crystal structure of digadolinium monocarbide dichloride (1T type), Gd2CCl2
  20. Crystal structure of η5-cyclopentadienyl-1-titana-1-chloro-2,5-bis(p-methoxyphenyl)-2,5-diaza-cyclopent-3-ene, C21H21ClN2O2Ti
  21. Crystal structure of η5-cyclopentadienyl-1-titana-1-chloro-2,5-di(p-tolyl)-3,4-diphenyl-2,5-diaza-cyclopent-3-ene, C33H29ClN2Ti
  22. Crystal structure of 5-amino-3H-[1,3,4]thiadiazole-2-thione, C2H3N3S2
  23. Crystal structure of 4H,8H-2,3,6,7-tetrakis(methoxycarbonyl)thiopyrano-[3,2-b]thiopyrane-4,8-dione, C16H12O10S2
  24. Crystal structure of tetraethylammonium O-methyldithiocarbonate, C10H23NOS2
  25. Crystal structure of μ-N,N′-malodinitrile-bis(pentacarbonyltungsten) methylene chloride, C13H4Cl2N2O10W
  26. Crystal structure of ethylenediammonium hexafluorosilicate, [H3N(CH2)2NH3]SiF6
  27. Crystal structure of ethylenediammonium sulphate, [H3N(CH2)2NH3]SO4
  28. Crystal structure of ethylenediammonium copper sulphate, [H3N(CH2)2NH3]Cu(SO4)2(H2O)4
  29. Crystal structure of copper strontium (5/1), Cu5Sr
Sign up now to receive a 20% welcome discount
Institutional Access
How does access work?
Have an idea on how to improve our website?
Please write us.
© 2025 De Gruyter Brill
Downloaded on 12.10.2025 from https://www.degruyterbrill.com/document/doi/10.1524/zkri.1994.209.4.357/html
Scroll to top button