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Crystal and molecular structure of the complex N-(8-quinolyl) pyridine-2-carbaldimine, 8-aminoquinoline monohydrate, nickel(II)-di-perchlorate. [Ni(C9H8N2)(C15H11N3)(H2O)]2+[(CIO4)2]2−
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August 25, 2010
Abstract
The crystal structure of the title compound M = 653.07 has been determined. Crystals are orthorhombic, space group Pbca with a = 22.320(9), b = 16.257(7), c = 14.503(7) A, Z = 8, Dx = 1.649(4), Dm = 1.70 Mg/m3. The crystal structure was determined by the heavy-atom method and refined to R = 0.065 and Rw = 0.066. Nickel(II) atom is surrounded by five nitrogen atoms and one oxygen atom of the water molecule forming an irregular octahedron.
Published Online: 2010-8-25
Published in Print: 1985-2-1
© 2015 Oldenbourg Wissenschaftsverlag GmbH, Rosenheimer Str. 145, 81671 München
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