Article
Open Access
Structural Phase Transition of N,N-Dimethylnitramine as Studied by 14N Nuclear Quadrupole Resonance
-
Tetsuo Asaji
Published/Copyright:
June 2, 2014
Received: 1993-8-10
Published Online: 2014-6-2
Published in Print: 1994-2-1
© 1946 – 2014: Verlag der Zeitschrift für Naturforschung
Articles in the same Issue
- Titelei
- Preface
- The story of the frustrated NQR physicist
- Low Frequency Nuclear Quadrupole Resonance with SQUID Amplifiers
- Determination of the Sign of Nuclear Quadrupole Interaction by Laser-Radiofrequency Double-Resonance Determination of the Sign of Nuclear Quadrupole Interaction by Laser-Radiofrequency Double-Resonance
- Wideline 2H -NMR Spectroscopy and Imaging of Solids
- β-Radiation Detected NMR in Solid and Liquid Neon
- 1H -14N Nuclear Quadrupole Double Resonance with Multiple Frequency Sweeps
- On the Reconstruction of NQR Nutation Spectra in Solids with Powder Geometry
- Automatically Tuned Probe Head System for Pulsed NQR Spectroscopy in Extreme Thermodynamic Conditions
- Investigation of Intrinsic Point Defects in Metals by Nuclear Quadrupole Double Resonance
- A New Pulsed Nuclear Quadrupole Resonance Spectrometer
- Theory of NQR Pulses
- Numerical Simulation of Magnetic Resonance Experiments: Concepts and Applications to Static, Rotating and Double Rotating Experiments
- Solomon Echoes Extended to Soft Pulse Excitation
- Nitrogen-14 NQR Multiple-Pulse Spin-locking in the Axial Electric Field Gradient
- Calculation of Quadrupole Coupling Constants: From Gas to Liquid
- Theoretical Investigation on the Nuclear Quadrupole Interaction of CH3Cl, CH2Cl2 and CHCl3
- Sternheimer Factors and Electric-Field-Gradient Hyperpolarisabilities for Ions in Crystals
- The Breathing Mode of BaBiO3: Electric Field Gradient and Total Energy Calculations
- A Theoretical Study of the Vibrational Dependence of the Nuclear Quadrupole Coupling Constants of some Diatomic Molecules
- Quadrupole Coupling Assignments in Inorganic Periodic Systems by ab initio Calculation of Electric Field Gradients
- Quadrupole Coupling in some H-bonded Organic Systems by ab initio Lattice Calculations of Electric Field Gradients
- The Nuclear Quadrupole Resonance of the 63, 65Cu Nuclei in Copper (I) Complexes
- A 35Cl NQR and MNDO study of 3,5-dichloro-1,2,4-triazole and its ionic forms
- 35Cl NQR of 1,5,2-Diazaphosphorine Derivatives
- Halogen NQR and Crystal Structure of Ammonium Halides (R-NH3)+X- and (X–) (+H3NR´NH3+) (X–). R = (HOCH2)3C, R´ = CH2C(CH3)2CH2; X = I,Br
- Structure and Bonding of Bromoantimonate (III) Complexes with Unusual Valency by Means of NQR and Powder X-Ray Diffraction
- Crystal Structure and NQR of Two Copper (I) Complexes of 4,6-Dimethylpyrimidine-2-thione
- 63,65Cu and 79,81Br NQR Studies of Halogenocuprate Complexes of Triphenylphosphine
- 81Br NQR and Crystal Structure of Ethylammonium Tribromomercurate(II), CH3CH2NH3HgBr3
- 81Br NQR for Uncoordinated Br ions in trans-[CoBr2(en)2][H5O2]Br2 and trans-[CoBr2(en)2] [D5O2]Br2
- Bromine NQR and Crystal Structures of Tetraanilinium Decabromotricadmate and 4-Methylpyridinium Tribromocadmate
- Tetraguanidium Hexabromocadmate, [C(NH2)3]4[CdBr6]. Crystal Structure and Bromine Nuclear Quadrupole Resonance
- Effect of Deuteration on the Phase Transitions and on the Critical Dynamics in Ammonium Hexachlorometallates
- Ionic Dynamics in Plastic Crystal KNO2 Studied by 39K and 15N NMR
- Structural Phase Transition of N,N-Dimethylnitramine as Studied by 14N Nuclear Quadrupole Resonance
- Successive Phase Transitions and High Ionic Conductivity of Trichlorogermanate (II) Salts as Studied by 35C1 NQR and Powder X-Ray Diffraction
- Phase Transitions in 4,4´-Dichlorobenzophenone as Studied by 35Cl FT-NQR
- Inequivalent Reorientation of the Trichloromethyl Groups in 1,4-Bis(TrichloromethyI) Benzene as Studied by Pulsed 35Cl NQR
- 35Cl NQR Relaxation and Hydrogen Bond in Some Chloral Hemiacetals
- 35Cl NQR Spin-Lattice Relaxation Mechanism in Ni(H2O)6SnCl6 and Mg(H2O)6SnCl6 Crystals
- Ionic motion and Disordered Structure in the Rotator Phase of Butylammonium Chloride Studied by Temperature Dependences of 35Cl and 2H NMR
- Low Temperature Isotope Effect in Ammonium Hexachloroselenate(IV) Studied by 35Cl NQR
- NQR Spin-Lattice Relaxation of Re in Perrhenates
- Study of the Molecular Dynamics from Deuterium Zeeman and Quadrupolar NMR Relaxation of 4,4´-di-n-Heptylazoxybenzene in the Nematic and Smectic A Phases
- Materials Characterisation by Nuclear Quadrupole Interaction
- Dynamics of Deuteron Glasses as Probed by 2 D Exchange NMR
- Nuclear Quadrupole Interaction and Ionic Dynamics in Sodium Superionic Conductors
- 17O Quadrupole Dips in Ammonium Persulphate
- The Zeeman Effect in Quadrupole Double Resonance Spectra: Dependence of the Line Shapes on the Orientation of the Electric Field Gradient Tensor
- Temperature Dependence of Impurity Induced EFG's in Extremely Diluted CuB
- Systematic Investigation of MF3 Crystalline Compounds (M = Al, Cr, Fe, Ga, In, Sc, Ti, and V) and Fe1-xMxF3 Mixed Series (M = Ga, Cr, V)
- Dehydration of Solid SnCl2(OH2)· H2O to SnCl2
- 43Ca NMR Study of Bismuth-Based High-Tc Superconductors
- The Energy Dispersion of the Chain Band in YBa2Cu3O6+x and Its Effect on the Cu(2) NQR Frequency
- Why is the Cu(2) Asymmetry Parameter of NQR Spectra in HTSC so Small?
- Internal Magnetic Field at Ba Site in Antiferromagnetic YBa2Cu3O6 Determined by 137Ba NQR
- Nuclear Quadrupole Resonance Study of Copper in Electron-Irradiated YBa2Cu3O6.95
- Calculated Spin-lattice Relaxation of 103Ru Compared with Low Temperature Quadrupole Orientation Measurements
- Hydrogen-doped Antiferromagnetic YBa2Cu3O7-δHx as Studied by Proton NMR and Cu NQR
- Quadrupole Interaction at Surfaces -Nuclear Methods
- Local Magnetic Fields in some Bismuth Compounds. A Survey of Experimental Evidences
- 209Bi NQR Powder Spectra Influenced by Local and Applied Magnetic Fields
- Investigation of the Phase Transition at 67.17 K in the Thiourea-CCl4 Inclusion Compound. As Studied by 14N NQR
- Positronium Quadrupole Interactions in Crystals
Keywords for this article
Molecular crystal;
Phase transition;
Soft mode;
NQR;
Spin-lattice relaxation
Creative Commons
BY-NC-ND 3.0
Articles in the same Issue
- Titelei
- Preface
- The story of the frustrated NQR physicist
- Low Frequency Nuclear Quadrupole Resonance with SQUID Amplifiers
- Determination of the Sign of Nuclear Quadrupole Interaction by Laser-Radiofrequency Double-Resonance Determination of the Sign of Nuclear Quadrupole Interaction by Laser-Radiofrequency Double-Resonance
- Wideline 2H -NMR Spectroscopy and Imaging of Solids
- β-Radiation Detected NMR in Solid and Liquid Neon
- 1H -14N Nuclear Quadrupole Double Resonance with Multiple Frequency Sweeps
- On the Reconstruction of NQR Nutation Spectra in Solids with Powder Geometry
- Automatically Tuned Probe Head System for Pulsed NQR Spectroscopy in Extreme Thermodynamic Conditions
- Investigation of Intrinsic Point Defects in Metals by Nuclear Quadrupole Double Resonance
- A New Pulsed Nuclear Quadrupole Resonance Spectrometer
- Theory of NQR Pulses
- Numerical Simulation of Magnetic Resonance Experiments: Concepts and Applications to Static, Rotating and Double Rotating Experiments
- Solomon Echoes Extended to Soft Pulse Excitation
- Nitrogen-14 NQR Multiple-Pulse Spin-locking in the Axial Electric Field Gradient
- Calculation of Quadrupole Coupling Constants: From Gas to Liquid
- Theoretical Investigation on the Nuclear Quadrupole Interaction of CH3Cl, CH2Cl2 and CHCl3
- Sternheimer Factors and Electric-Field-Gradient Hyperpolarisabilities for Ions in Crystals
- The Breathing Mode of BaBiO3: Electric Field Gradient and Total Energy Calculations
- A Theoretical Study of the Vibrational Dependence of the Nuclear Quadrupole Coupling Constants of some Diatomic Molecules
- Quadrupole Coupling Assignments in Inorganic Periodic Systems by ab initio Calculation of Electric Field Gradients
- Quadrupole Coupling in some H-bonded Organic Systems by ab initio Lattice Calculations of Electric Field Gradients
- The Nuclear Quadrupole Resonance of the 63, 65Cu Nuclei in Copper (I) Complexes
- A 35Cl NQR and MNDO study of 3,5-dichloro-1,2,4-triazole and its ionic forms
- 35Cl NQR of 1,5,2-Diazaphosphorine Derivatives
- Halogen NQR and Crystal Structure of Ammonium Halides (R-NH3)+X- and (X–) (+H3NR´NH3+) (X–). R = (HOCH2)3C, R´ = CH2C(CH3)2CH2; X = I,Br
- Structure and Bonding of Bromoantimonate (III) Complexes with Unusual Valency by Means of NQR and Powder X-Ray Diffraction
- Crystal Structure and NQR of Two Copper (I) Complexes of 4,6-Dimethylpyrimidine-2-thione
- 63,65Cu and 79,81Br NQR Studies of Halogenocuprate Complexes of Triphenylphosphine
- 81Br NQR and Crystal Structure of Ethylammonium Tribromomercurate(II), CH3CH2NH3HgBr3
- 81Br NQR for Uncoordinated Br ions in trans-[CoBr2(en)2][H5O2]Br2 and trans-[CoBr2(en)2] [D5O2]Br2
- Bromine NQR and Crystal Structures of Tetraanilinium Decabromotricadmate and 4-Methylpyridinium Tribromocadmate
- Tetraguanidium Hexabromocadmate, [C(NH2)3]4[CdBr6]. Crystal Structure and Bromine Nuclear Quadrupole Resonance
- Effect of Deuteration on the Phase Transitions and on the Critical Dynamics in Ammonium Hexachlorometallates
- Ionic Dynamics in Plastic Crystal KNO2 Studied by 39K and 15N NMR
- Structural Phase Transition of N,N-Dimethylnitramine as Studied by 14N Nuclear Quadrupole Resonance
- Successive Phase Transitions and High Ionic Conductivity of Trichlorogermanate (II) Salts as Studied by 35C1 NQR and Powder X-Ray Diffraction
- Phase Transitions in 4,4´-Dichlorobenzophenone as Studied by 35Cl FT-NQR
- Inequivalent Reorientation of the Trichloromethyl Groups in 1,4-Bis(TrichloromethyI) Benzene as Studied by Pulsed 35Cl NQR
- 35Cl NQR Relaxation and Hydrogen Bond in Some Chloral Hemiacetals
- 35Cl NQR Spin-Lattice Relaxation Mechanism in Ni(H2O)6SnCl6 and Mg(H2O)6SnCl6 Crystals
- Ionic motion and Disordered Structure in the Rotator Phase of Butylammonium Chloride Studied by Temperature Dependences of 35Cl and 2H NMR
- Low Temperature Isotope Effect in Ammonium Hexachloroselenate(IV) Studied by 35Cl NQR
- NQR Spin-Lattice Relaxation of Re in Perrhenates
- Study of the Molecular Dynamics from Deuterium Zeeman and Quadrupolar NMR Relaxation of 4,4´-di-n-Heptylazoxybenzene in the Nematic and Smectic A Phases
- Materials Characterisation by Nuclear Quadrupole Interaction
- Dynamics of Deuteron Glasses as Probed by 2 D Exchange NMR
- Nuclear Quadrupole Interaction and Ionic Dynamics in Sodium Superionic Conductors
- 17O Quadrupole Dips in Ammonium Persulphate
- The Zeeman Effect in Quadrupole Double Resonance Spectra: Dependence of the Line Shapes on the Orientation of the Electric Field Gradient Tensor
- Temperature Dependence of Impurity Induced EFG's in Extremely Diluted CuB
- Systematic Investigation of MF3 Crystalline Compounds (M = Al, Cr, Fe, Ga, In, Sc, Ti, and V) and Fe1-xMxF3 Mixed Series (M = Ga, Cr, V)
- Dehydration of Solid SnCl2(OH2)· H2O to SnCl2
- 43Ca NMR Study of Bismuth-Based High-Tc Superconductors
- The Energy Dispersion of the Chain Band in YBa2Cu3O6+x and Its Effect on the Cu(2) NQR Frequency
- Why is the Cu(2) Asymmetry Parameter of NQR Spectra in HTSC so Small?
- Internal Magnetic Field at Ba Site in Antiferromagnetic YBa2Cu3O6 Determined by 137Ba NQR
- Nuclear Quadrupole Resonance Study of Copper in Electron-Irradiated YBa2Cu3O6.95
- Calculated Spin-lattice Relaxation of 103Ru Compared with Low Temperature Quadrupole Orientation Measurements
- Hydrogen-doped Antiferromagnetic YBa2Cu3O7-δHx as Studied by Proton NMR and Cu NQR
- Quadrupole Interaction at Surfaces -Nuclear Methods
- Local Magnetic Fields in some Bismuth Compounds. A Survey of Experimental Evidences
- 209Bi NQR Powder Spectra Influenced by Local and Applied Magnetic Fields
- Investigation of the Phase Transition at 67.17 K in the Thiourea-CCl4 Inclusion Compound. As Studied by 14N NQR
- Positronium Quadrupole Interactions in Crystals