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Fatigue and fracture-induced defect structures of metals investigated by positron microscopy

  • W. Egger , G. Kögel , P. Sperr , W. Triftshäuser , J. Bär , S. Rödling and H.-J. Gudladt EMAIL logo
Published/Copyright: February 16, 2022
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Abstract

Defect distributions close to cracks from monotonic and fatigue fractures have been investigated for the first time by positron lifetime studies. The positron beams probe either the depth profile of defects at sub-μm resolution or the lateral distribution of defects at a few μm spatial resolution. Both in pure Cu and in the precipitation-hardened alloy Al 6013, in addition to dislocations, large clusters of up to 30 vacancies were detected close to a fatigue crack exclusively, whereas at monotonic fractures only the annihilation characteristics of dislocations were observed. If this characteristic difference holds as a general rule, then positron lifetime microscopy will provide a simple, quantitative method to distinguish a posteriori monotonic fractures from fatigue fractures without any further fractographic studies.


Prof. Dr. H-J. Gudladt Institut für Werkstoffkunde D-85577 Neubiberg, Germany Tel.: +49 89 6004 2534 Fax: +49 89 6004 3295

Dedicated to Professor Dr. Otmar Vöhringer on the occasion of his 65th birthday


References

[1] W. Triftshäuser, in: U. Gonser (Ed.), Topics in Current Physics, Vol. 40: Microscopic Methods in Metals, Springer, Berlin (1986) 249.10.1007/978-3-642-46571-0_9Search in Google Scholar

[2] R. Krause –Rehberg, H.S. Leipner: Positron Annihilation in Semiconductors: Defect Studies, Springer, Berlin (1999).10.1007/978-3-662-03893-2Search in Google Scholar

[3] T.E.M. Staab, R. Krause –Rehberg, B. Kieback: J. Mat. Sci. 34 (1999) 3833.10.1023/A:1004666003732Search in Google Scholar

[4] M.J. Puska, R.M. Nieminen: Rev. Mod. Phys. 68 (1994) 841.10.1103/RevModPhys.66.841Search in Google Scholar

[5] P. Sperr, G. Kögel: Mater. Sci. Forum 255–257 (1997) 109.10.4028/www.scientific.net/MSF.255-257.109Search in Google Scholar

[6] R. Suzuki, Y. Kobayashi, T. Mikado, H. Ohgaki, M. Chiwaki, T. Yamazaki, T. Tomimasu: Jpn. J. Appl. Phys. 30 (1991) L 532.10.1143/JJAP.30.L532Search in Google Scholar

[7] J. Gebauer, R. Krause –Rehberg, S. Eichler, W. Bauer –Kugelmann, G. Kögel,W. Triftshäuser,M. Luysberg, H. Sohn, E.R. Weber: Mater. Sci. Forum 255–257 (1997) 204.10.4028/www.scientific.net/MSF.255-257.204Search in Google Scholar

[8] T. Aruga, S. Takamura, K. Nakata, Y. Ito: Appl. Surf. Sci. 85 (1995) 229.10.1016/0169-4332(94)00336-XSearch in Google Scholar

[9] H. Greif, M. Haaks, U. Holzwarth, U. Männig, M. Thongbhoyai, T. Wider, K. Maier, J. Bihr, B. Huber: Appl. Phys. Lett. 71 (1997) 2115.10.1063/1.120451Search in Google Scholar

[10] A. David, G. Kögel, P. Sperr, W. Triftshäuser: Phys. Rev. Lett. 87 (2001) 067402.10.1103/PhysRevLett.87.067402Search in Google Scholar PubMed

[11] W.A.Wood, S. McGourland, K.R. Sargent: Acta metall. 11 (1963) 643.10.1016/0001-6160(63)90002-6Search in Google Scholar

[12] P.O. Kettunen, T. Lepistö, G. Kostorz, G. Göltz: Acta metall. 29 (1981) 963.10.1016/0001-6160(81)90050-XSearch in Google Scholar

[13] T. Lepistö, J. Yli –Kauppila, P. Kettunen, P. Hautojärvi: phys. stat. sol. (a) 67 (1983) K93.10.1002/pssa.2210670248Search in Google Scholar

[14] R. Page, J.R. Weertman, M. Roth: Acta metall. 30 (1982) 1357.10.1016/0001-6160(82)90155-9Search in Google Scholar

[15] H. Mughrabi, F. Ackermann, K. Herz, in: J.T. Fong (Ed.), Fatigue Mechanisms, ASTM-STP 675, Kansas City (1979) 69.10.1520/STP35885SSearch in Google Scholar

[16] Z.S. Basinski, A.S. Korbel, S.J. Basinsky: Acta metall. 28 (1980) 191.10.1016/0001-6160(80)90068-1Search in Google Scholar

[17] J. Bär, Th. Volpp: MP Materialprüfung 43 (2001) 242.10.1515/mt-2001-430610Search in Google Scholar

[18] L. Diaz, R. Pareja, M.A. Pedrosa, R. Gonzalez: phys. stat. sol. (a) 92 (1985) 159.10.1002/pssa.2210920114Search in Google Scholar

[19] M. Eldrup, J.H. Evans, D.E. Mogensen, B.N. Singh: Radiat. Eff. 54 (1981) 65.10.1080/00337578108207128Search in Google Scholar

[20] H.E. Hansen, R.M. Nieminen, M.J. Puska: J. Phys. F: Met. Phys. 14 (1984) 1299.10.1088/0305-4608/14/5/025Search in Google Scholar

[21] G. Kögel: Appl. Phys. A 63 (1996) 227.10.1007/BF01567874Search in Google Scholar

[22] E. Soininen, H. Huomo, P.A. Huttunen, J. Mäkinen, A. Vehanen, P. Hautojärvi: Phys. Rev. B 41 (1990) 6227.10.1103/PhysRevB.41.6227Search in Google Scholar

[23] W. Egger, G. Kögel, P. Sperr, W. Triftshäuser, S. Rödling, J. Bär, H.-J. Gudladt: Appl. Surf. Sci. 194 (2002) 214.10.1016/S0169-4332(02)00106-XSearch in Google Scholar

[24] A. Somoza: Mater. Sci. Forum 363 –365 (2001) 9.10.4028/www.scientific.net/MSF.363-365.9Search in Google Scholar

[25] G. Dlubek, P. Lademann, H. Krause, S. Krause, R. Unger: Scripta mater. 39 (1998) 893.10.1016/S1359-6462(98)00250-4Search in Google Scholar

[26] C. Zamponi: Ph. D. Thesis, University of Bonn (2002).Search in Google Scholar

[27] H. Häkkinen, S. Mäkinen, M. Manninen: Phys. Rev. B 41 (1990) 12441.10.1103/PhysRevB.41.12441Search in Google Scholar

[28] H.E. Schäfer, in: P.G. Coleman, S.C. Sharma, L.M. Diana (Eds.), Positron Annihilation, North Holland, Amsterdam (1982) 369.Search in Google Scholar

[29] C. Hidalgo, G. Gonzales –Doncel, S. Linderoth, J. San Juan: Phys. Rev. B 45 (1992) 7017.10.1103/PhysRevB.45.7017Search in Google Scholar

[30] H. Murakami: Phys. Rev. B 47 (1993) 6114.10.1103/PhysRevB.47.6114Search in Google Scholar

[31] E. Hashimoto, M. Iwami, Y. Ueda: J. Phys.: Cond. Matter 6 (1994) 1611.10.1088/0953-8984/6/8/019Search in Google Scholar

[32] M. Springer, G. Kögel, B. Strasser, W. Triftshäuser, K. Schreckenbach: Mater. Sci. Forum 255 –257 (1997) 695.10.4028/www.scientific.net/MSF.255-257.695Search in Google Scholar

[33] G. Kögel: Appl. Surface Sci. 194 (2002) 200.10.1016/S0169-4332(02)00102-2Search in Google Scholar

Received: 2002-10-21
Published Online: 2022-02-16

© 2003 Carl Hanser Verlag, München

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