Abstract
Defect distributions close to cracks from monotonic and fatigue fractures have been investigated for the first time by positron lifetime studies. The positron beams probe either the depth profile of defects at sub-μm resolution or the lateral distribution of defects at a few μm spatial resolution. Both in pure Cu and in the precipitation-hardened alloy Al 6013, in addition to dislocations, large clusters of up to 30 vacancies were detected close to a fatigue crack exclusively, whereas at monotonic fractures only the annihilation characteristics of dislocations were observed. If this characteristic difference holds as a general rule, then positron lifetime microscopy will provide a simple, quantitative method to distinguish a posteriori monotonic fractures from fatigue fractures without any further fractographic studies.
References
[1] W. Triftshäuser, in: U. Gonser (Ed.), Topics in Current Physics, Vol. 40: Microscopic Methods in Metals, Springer, Berlin (1986) 249.10.1007/978-3-642-46571-0_9Search in Google Scholar
[2] R. Krause –Rehberg, H.S. Leipner: Positron Annihilation in Semiconductors: Defect Studies, Springer, Berlin (1999).10.1007/978-3-662-03893-2Search in Google Scholar
[3] T.E.M. Staab, R. Krause –Rehberg, B. Kieback: J. Mat. Sci. 34 (1999) 3833.10.1023/A:1004666003732Search in Google Scholar
[4] M.J. Puska, R.M. Nieminen: Rev. Mod. Phys. 68 (1994) 841.10.1103/RevModPhys.66.841Search in Google Scholar
[5] P. Sperr, G. Kögel: Mater. Sci. Forum 255–257 (1997) 109.10.4028/www.scientific.net/MSF.255-257.109Search in Google Scholar
[6] R. Suzuki, Y. Kobayashi, T. Mikado, H. Ohgaki, M. Chiwaki, T. Yamazaki, T. Tomimasu: Jpn. J. Appl. Phys. 30 (1991) L 532.10.1143/JJAP.30.L532Search in Google Scholar
[7] J. Gebauer, R. Krause –Rehberg, S. Eichler, W. Bauer –Kugelmann, G. Kögel,W. Triftshäuser,M. Luysberg, H. Sohn, E.R. Weber: Mater. Sci. Forum 255–257 (1997) 204.10.4028/www.scientific.net/MSF.255-257.204Search in Google Scholar
[8] T. Aruga, S. Takamura, K. Nakata, Y. Ito: Appl. Surf. Sci. 85 (1995) 229.10.1016/0169-4332(94)00336-XSearch in Google Scholar
[9] H. Greif, M. Haaks, U. Holzwarth, U. Männig, M. Thongbhoyai, T. Wider, K. Maier, J. Bihr, B. Huber: Appl. Phys. Lett. 71 (1997) 2115.10.1063/1.120451Search in Google Scholar
[10] A. David, G. Kögel, P. Sperr, W. Triftshäuser: Phys. Rev. Lett. 87 (2001) 067402.10.1103/PhysRevLett.87.067402Search in Google Scholar PubMed
[11] W.A.Wood, S. McGourland, K.R. Sargent: Acta metall. 11 (1963) 643.10.1016/0001-6160(63)90002-6Search in Google Scholar
[12] P.O. Kettunen, T. Lepistö, G. Kostorz, G. Göltz: Acta metall. 29 (1981) 963.10.1016/0001-6160(81)90050-XSearch in Google Scholar
[13] T. Lepistö, J. Yli –Kauppila, P. Kettunen, P. Hautojärvi: phys. stat. sol. (a) 67 (1983) K93.10.1002/pssa.2210670248Search in Google Scholar
[14] R. Page, J.R. Weertman, M. Roth: Acta metall. 30 (1982) 1357.10.1016/0001-6160(82)90155-9Search in Google Scholar
[15] H. Mughrabi, F. Ackermann, K. Herz, in: J.T. Fong (Ed.), Fatigue Mechanisms, ASTM-STP 675, Kansas City (1979) 69.10.1520/STP35885SSearch in Google Scholar
[16] Z.S. Basinski, A.S. Korbel, S.J. Basinsky: Acta metall. 28 (1980) 191.10.1016/0001-6160(80)90068-1Search in Google Scholar
[17] J. Bär, Th. Volpp: MP Materialprüfung 43 (2001) 242.10.1515/mt-2001-430610Search in Google Scholar
[18] L. Diaz, R. Pareja, M.A. Pedrosa, R. Gonzalez: phys. stat. sol. (a) 92 (1985) 159.10.1002/pssa.2210920114Search in Google Scholar
[19] M. Eldrup, J.H. Evans, D.E. Mogensen, B.N. Singh: Radiat. Eff. 54 (1981) 65.10.1080/00337578108207128Search in Google Scholar
[20] H.E. Hansen, R.M. Nieminen, M.J. Puska: J. Phys. F: Met. Phys. 14 (1984) 1299.10.1088/0305-4608/14/5/025Search in Google Scholar
[21] G. Kögel: Appl. Phys. A 63 (1996) 227.10.1007/BF01567874Search in Google Scholar
[22] E. Soininen, H. Huomo, P.A. Huttunen, J. Mäkinen, A. Vehanen, P. Hautojärvi: Phys. Rev. B 41 (1990) 6227.10.1103/PhysRevB.41.6227Search in Google Scholar
[23] W. Egger, G. Kögel, P. Sperr, W. Triftshäuser, S. Rödling, J. Bär, H.-J. Gudladt: Appl. Surf. Sci. 194 (2002) 214.10.1016/S0169-4332(02)00106-XSearch in Google Scholar
[24] A. Somoza: Mater. Sci. Forum 363 –365 (2001) 9.10.4028/www.scientific.net/MSF.363-365.9Search in Google Scholar
[25] G. Dlubek, P. Lademann, H. Krause, S. Krause, R. Unger: Scripta mater. 39 (1998) 893.10.1016/S1359-6462(98)00250-4Search in Google Scholar
[26] C. Zamponi: Ph. D. Thesis, University of Bonn (2002).Search in Google Scholar
[27] H. Häkkinen, S. Mäkinen, M. Manninen: Phys. Rev. B 41 (1990) 12441.10.1103/PhysRevB.41.12441Search in Google Scholar
[28] H.E. Schäfer, in: P.G. Coleman, S.C. Sharma, L.M. Diana (Eds.), Positron Annihilation, North Holland, Amsterdam (1982) 369.Search in Google Scholar
[29] C. Hidalgo, G. Gonzales –Doncel, S. Linderoth, J. San Juan: Phys. Rev. B 45 (1992) 7017.10.1103/PhysRevB.45.7017Search in Google Scholar
[30] H. Murakami: Phys. Rev. B 47 (1993) 6114.10.1103/PhysRevB.47.6114Search in Google Scholar
[31] E. Hashimoto, M. Iwami, Y. Ueda: J. Phys.: Cond. Matter 6 (1994) 1611.10.1088/0953-8984/6/8/019Search in Google Scholar
[32] M. Springer, G. Kögel, B. Strasser, W. Triftshäuser, K. Schreckenbach: Mater. Sci. Forum 255 –257 (1997) 695.10.4028/www.scientific.net/MSF.255-257.695Search in Google Scholar
[33] G. Kögel: Appl. Surface Sci. 194 (2002) 200.10.1016/S0169-4332(02)00102-2Search in Google Scholar
© 2003 Carl Hanser Verlag, München
Articles in the same Issue
- Frontmatter
- Articles/Aufsätze
- Bedeutung von Eigenspannungsabbau und mikrostrukturellen Veränderungen für die Lebensdauervorhersage schwingbeanspruchter Schweißverbindungen
- Factors affecting cyclic lifetime of EB-PVD thermal barrier coatings with various bond coats
- Depth-resolved X-ray residual stress analysis in PVD (Ti, Cr) N hard coatings
- Crystal orientation and residual stress in TiN film by synchrotron radiation
- Characterization of thermal and anodic oxide layers on β- and on near-β-titanium alloys for biomedical application
- Micromechanisms and modelling of crack initiation and growth in tool steels: role of primary carbides
- Fatigue crack nucleation at grain boundaries – experiment and simulation
- Fatigue and fracture-induced defect structures of metals investigated by positron microscopy
- Deformation and fracture of Nb/α-Al2O3 composites in compression and bending studied by optical methods
- Dislocation microstructures of single crystal ⟨001⟩ CMSX-4 specimens tensile tested at 700 and 1000°C
- Influence of mechanical surface treatments on the HCF performance of the Ni-superalloy Udimet 720 LI
- Precipitation of β-phase and twinning during deformation of Mg–Al alloy AZ91 at 150 °C after solution treatment
- Nanograin size, high-nitrogen austenitic stainless steels
- Der dynamische SD-Effekt und der Einfluss auf die Fließortkurve
- Einfluss der Umformgeschwindigkeit und -temperatur auf das Fließverhalten metallischer Werkstoffe
- Mean stress sensitivity of sintered iron and steel
- Thermozyklisches Kriechen einer kurzfaserverstärkten Aluminium-Kolbenlegierung
- Strength and ductility of thin Cu wires
- Modeling of deformation behavior of copper under equal channel angular pressing
- Reaktionssintern von AlMg–MgO zur Herstellung von Bauteilen auf Spinellbasis
- Determination of the local oxygen distribution in a commercial titanium alloy by 3-dimensional atom probe
- Phase diagram of the Al–Cu–Fe quasicrystal-forming alloy system
- Notifications/Mitteilungen
- Personal/Personelles
- Books/Bücher
- Conferences/Konferenzen
Articles in the same Issue
- Frontmatter
- Articles/Aufsätze
- Bedeutung von Eigenspannungsabbau und mikrostrukturellen Veränderungen für die Lebensdauervorhersage schwingbeanspruchter Schweißverbindungen
- Factors affecting cyclic lifetime of EB-PVD thermal barrier coatings with various bond coats
- Depth-resolved X-ray residual stress analysis in PVD (Ti, Cr) N hard coatings
- Crystal orientation and residual stress in TiN film by synchrotron radiation
- Characterization of thermal and anodic oxide layers on β- and on near-β-titanium alloys for biomedical application
- Micromechanisms and modelling of crack initiation and growth in tool steels: role of primary carbides
- Fatigue crack nucleation at grain boundaries – experiment and simulation
- Fatigue and fracture-induced defect structures of metals investigated by positron microscopy
- Deformation and fracture of Nb/α-Al2O3 composites in compression and bending studied by optical methods
- Dislocation microstructures of single crystal ⟨001⟩ CMSX-4 specimens tensile tested at 700 and 1000°C
- Influence of mechanical surface treatments on the HCF performance of the Ni-superalloy Udimet 720 LI
- Precipitation of β-phase and twinning during deformation of Mg–Al alloy AZ91 at 150 °C after solution treatment
- Nanograin size, high-nitrogen austenitic stainless steels
- Der dynamische SD-Effekt und der Einfluss auf die Fließortkurve
- Einfluss der Umformgeschwindigkeit und -temperatur auf das Fließverhalten metallischer Werkstoffe
- Mean stress sensitivity of sintered iron and steel
- Thermozyklisches Kriechen einer kurzfaserverstärkten Aluminium-Kolbenlegierung
- Strength and ductility of thin Cu wires
- Modeling of deformation behavior of copper under equal channel angular pressing
- Reaktionssintern von AlMg–MgO zur Herstellung von Bauteilen auf Spinellbasis
- Determination of the local oxygen distribution in a commercial titanium alloy by 3-dimensional atom probe
- Phase diagram of the Al–Cu–Fe quasicrystal-forming alloy system
- Notifications/Mitteilungen
- Personal/Personelles
- Books/Bücher
- Conferences/Konferenzen