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Microwave-Assisted Extraction of Phenolic Compounds from Dried Waste Grape Skins

  • Miguel A. Pedroza , Danila Amendola , Luana Maggi , Amaya Zalacain , Dante M. De Faveri und Giorgia Spigno EMAIL logo
Veröffentlicht/Copyright: 11. April 2015
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Abstract

Microwave-assisted extraction (MAE) was investigated for recovering of total phenolic compounds from dried waste grape skins using a domestic microwave oven. Influence of vessel geometry, irradiation cycles, irradiation power and time was investigated. The results in terms of phenolics yield, antioxidant capacity and energy consumption were compared with a reference solid–liquid extraction (SLE) carried out for 2 h at 60°C. Equivalent yield of total phenolics as in SLE was achieved with a MAE extraction time of 1,033 sec (corresponding to 83 sec of irradiation at 900 W, 83% saving in extraction time compared to SLE and with a 70% energetic efficiency). Pre-maceration of samples and solvent pre-heating are proposed for large-scale industrial processes to enhance phenolics extraction and process efficiency.

Funding statement: Funding: This work received funding from Progetto Ager (grant no 2010–2222). M.A.P. is grateful for the CONACYT fellowship (207976) received from the Mexican government.

Abbreviations

ABTS

2,2′-azino-bis(3-ethylbenzothiazoline-6-sulphonic acid) diammonium salt

AOC/AOC

antioxidant capacity/specific antioxidant capacity

DWGS

dried waste grape skins

MAE

microwave-assisted extraction

GAE-TPI/GAE-FI

gallic acid equivalents based on total phenolics index/Folin index

SLE

solvent–liquid extraction

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Published Online: 2015-4-11
Published in Print: 2015-6-1

©2015 by De Gruyter

Heruntergeladen am 12.11.2025 von https://www.degruyterbrill.com/document/doi/10.1515/ijfe-2015-0009/html
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